Modified floating bead calcium silicate, preparation method thereof and thermal insulation and decoration integrated board
A technology of calcium silicate and floating beads, applied in the field of thermal insulation of construction projects, can solve the problems of affecting thermal insulation effect, cracking of foam cement board surface, poor waterproof performance, etc.
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[0027] The invention provides a kind of preparation method of calcium silicate of modified floating beads, comprising the following steps:
[0028] Mix the floating beads, surfactant, water repellent and water to obtain the floating beads dispersion;
[0029] The floating beads dispersion and lime milk are mixed for hydrothermal reaction to obtain xonotlite slurry; the mass ratio of calcium hydroxide in the floating beads and lime milk is (5~20):(1~5 );
[0030] The hard calcium silicate slurry stone and the reinforcing fiber are mixed and then pressed into shape to obtain the modified calcium silicate calcium silicate.
[0031] In the present invention, unless otherwise specified, the raw materials used are commercially available products well known to those skilled in the art.
[0032] The present invention mixes the floating beads, surfactant, water repellent and water (hereinafter referred to as the first mixing) to obtain the floating beads dispersion.
[0033] In the ...
Embodiment 1
[0121] Take 5 parts of floating beads and 80 parts of deionized water, prepare water-based slurry, ball mill for 30 minutes, add 0.5 parts of polyvinyl alcohol, 0.5 parts of silane coupling agent KH-5700, and mix evenly with a magnetic stirrer to obtain floating beads Dispersions;
[0122] Mix the floating bead dispersion with milk of lime, wherein the mass of calcium hydroxide base is 1 part, the obtained mixture is subjected to hydrothermal reaction, the stirring speed is 200r / min, and the temperature is raised to 150°C for 8 hours to obtain xonotlite slurry;
[0123] Wash the xonotlite slurry and mix it with pulp, press molding and drying to obtain modified calcium silicate beads with a pore size of 2-10nm, a compressive strength of 1MPa, and a thermal conductivity of 0.03W / (m·K) , bulk density is 70kg / m 3 , Hydrophobic rate of 98%.
Embodiment 2
[0125] Take 20 parts of floating beads and 75 parts of deionized water, prepare water-based slurry, ball mill for 30 minutes, add 2.5 parts of sodium dodecylbenzenesulfonate, 3 parts of silane coupling agent KH-5703, and mix with a magnetic stirrer Evenly, get the floating bead dispersion;
[0126] Mix the floating bead dispersion with milk of lime, wherein the mass of calcium hydroxide is 5 parts, and the obtained mixture is subjected to hydrothermal reaction, the stirring speed is 500r / min, and the temperature is raised to 250°C for 72 hours to obtain xonotlite slurry;
[0127] Wash the xonotlite slurry and mix it with glass fiber, press and dry to obtain modified calcium silicate beads with a pore size of 30-100nm, a compressive strength of 20MPa, and a thermal conductivity of 0.08W / (m·K ), the bulk density is 800~1000kg / m 3 , Hydrophobic rate of 90%.
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