Nickel ferrite nanoparticles and green synthesis method and application thereof
A technology of nano-particles and nickel ferrite, which is applied in the fields of nano-magnetism, nickel compounds, nano-technology, etc., can solve the problems that have not been reported in the research, and achieve the effects of uniform particle size, simple synthesis method, and low cost
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Embodiment 1
[0050] A green synthesis method for nickel ferrite nanoparticles, comprising the following steps:
[0051] 1) Take 10g of fresh water hyacinth lotus stems and leaves and wash them with tap water and distilled water successively, place them in a mortar and grind them into mud, add distilled water to wash the extract 3 times, share 50 mL of distilled water, and combine precipitation each time, three precipitations, and merge and transfer. Put it into a beaker, further place it in a 95-100°C water bath for heating and extraction for 10 minutes, cool it to room temperature, filter it with suction, take the supernatant and dilute to 50mL to obtain the water hyacinth lotus extract;
[0052] 2) take nickel chloride and ferric nitrate and be dissolved in 100mL deionized water, make its final concentration be respectively 0.15mol / L and 0.30mol / L; placed on a magnetic stirrer and stirred continuously for 20 min; the obtained mixture was placed in a 60°C water bath and heated at constant...
Embodiment 2
[0057] A green synthesis method for nickel ferrite nanoparticles, comprising the following steps:
[0058] 1) Take 10g of fresh water hyacinth lotus leaves and wash them with tap water and distilled water successively, place them in a mortar and grind them into mud, add distilled water to wash the extract 3 times, share 50mL of distilled water, keep the precipitation each time, combine the precipitation three times, and further Place in a 95-100°C water bath for heating and extraction for 10min, cool to room temperature, filter with suction and dilute to 50mL to obtain water hyacinth lotus extract;
[0059] 2) Weigh nickel acetate and ferric chloride and dissolve them in 100mL deionized water, so that their final concentrations are respectively 0.15mol / L and 0.30mol / L; at room temperature, the prepared 50mL water hyacinth extract is added to the above-mentioned salt solution , placed on a magnetic stirrer and continuously stirred for 20 min; the obtained mixture was placed in ...
Embodiment 3
[0062] A green synthesis method for nickel ferrite nanoparticles, comprising the following steps:
[0063] 1) Take 10g of fresh water hyacinth lotus stems and wash them with tap water and distilled water successively, place them in a mortar and grind them into mud, add distilled water to wash the extract 3 times, share 50 mL of distilled water, retain the precipitation each time, and combine the precipitations for three times, then further. Place in a 95-100°C water bath for heating and extraction for 10min, cool to room temperature, filter with suction and dilute to 50mL to obtain water hyacinth lotus extract;
[0064] 2) Weigh nickel acetate and ferric chloride and dissolve them in 100mL deionized water, so that their final concentrations are respectively 0.15mol / L and 0.30mol / L; at room temperature, the prepared 50mL water hyacinth extract is added to the above-mentioned salt solution , placed on a magnetic stirrer and continuously stirred for 20 min; the obtained mixture w...
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