Method for extracting lipid component

A lipid and extraction tank technology, which is applied in chemical instruments and methods, fat production, and fat substance recovery, can solve problems such as high equipment requirements, flammability and explosion, and limited production scale, and achieve stable chemical properties and extraction efficiency. High, good product quality effect

Active Publication Date: 2013-05-08
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In recent years, some new oil extraction processes have also been developed. There is a method of using water instead of solvent to simultaneously produce oil and protein with the help of enzymes. This method is still in the experimental stage in the world. Although the reaction conditions Mild, the main quality indicators of the product are similar to those of the solvent extraction method, but the yield of oil is only 75%~90%, and the yield of protein is about 65%; with supercritical CO 2 The extraction method has the highest product quality, high oil yield, and low temperature during processing, but this method requires high equipment, limited production scale, and high production cost, which is not suitable for industrial production; there is also a method called The method of subcritical fluid extraction is a new method of extracting target components from natural products by using the fluid in the subcritical state as the solvent, and successively undergoing processes such as leaching, evaporation, desolventization, compression, and condensation recovery with the solute in the system. When applied to oil extraction, propane or butane is mainly used. It is non-toxic, non-thermally processed, and the active product that retains raw materials is not damaged or oxidized. It can be used for industrialized large-scale production, energy saving, and low operating cost. It has the advantages of easy separation from the product, etc., but the solvent is volatile, flammable and explosive, and has high requirements on production equipment, environment and daily operation, and there are extremely serious safety hazards, which limit its large-scale application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Take peanuts with an oil content of 43% by weight, go through impurity removal, shelling, drying, and embryo pressing (the temperature of the material should be kept ≤50°C during the process), and then put the embryo flakes into the extraction tank, and vacuumize to below 0.01MPa Finally, add liquefied perfluorocyclobutane that is 1.5 times the weight of the raw material, operate at a temperature of 30°C (operating pressure is the corresponding vapor pressure), and extract a mixture of oil and solvent for 60 minutes each time and 3 times in total; The mixture with the solvent is gasified under reduced pressure, and the gauge pressure reaches 0MPa, and then vacuumizes for precipitation. When the gauge pressure is -0.09MPa and the temperature is 40~50°C, keep for 30 minutes to obtain the precipitated peanut crude oil, which contains residual solvent ≤ 30mg / kg, impurity ≤0.3%.

[0019] The defatted peanut meal containing solvent is decompressed and gasified, and the gauge ...

Embodiment 2

[0021] Take soybeans with an oil content of 19% by weight, remove impurities, peel, dry, crush, soften, and press embryos (the temperature of soybeans should be kept ≤ 60°C during the process), and then put the embryo flakes into the extraction tank and vacuumize to 0.01 When it is below MPa, add liquefied chloroheptafluorobutane twice the weight of the raw material at an operating temperature of 60°C (operating pressure is the corresponding vapor pressure), and extract oil and solvent for 30 minutes each time for a total of 3 extractions The mixture; the oil and solvent mixture is gasified under reduced pressure, and the gauge pressure reaches 0MPa, and then vacuumizes for precipitation. When the gauge pressure is -0.09MPa and the temperature is 50~60°C, keep for 50 minutes to obtain the crude soybean oil containing Residual solubility ≤ 50mg / kg, impurity ≤ 0.3%.

[0022] The solvent-containing defatted soybean meal is decompressed and gasified, and the gauge pressure reaches...

Embodiment 3

[0024] Take hemp seeds with an oil content of 28% by weight, after screening to remove organic and inorganic impurities and magnetic separation to remove metal impurities, dry them with hot air at a temperature of 40~50°C until the water content drops to ≤8% by weight, and use shelling Machine crushing (keep the temperature of the hemp seeds ≤ 50°C during the crushing process), and then screen the crushed hemp seeds with a sieve, the hemp seeds pass through the sieve, and the shells are blocked by the sieve to obtain shelled hemp Seed kernels; use the embryo pressing machine to press the hemp seed kernels into embryo flakes; put the embryo flakes into the extraction tank, vacuumize to below 0.01MPa, add liquefied perfluorocyclopropane twice the weight of the raw materials, and operate at a temperature of 40 ℃ (the operating pressure is the corresponding vapor pressure), after 20 minutes each time, a total of 4 extractions, the oil and solvent mixture is obtained; the oil and so...

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Abstract

The invention discloses a method for extracting lipid components, which performs lipid components extraction in various raw materials by adopting subcritical extraction technology with fluorine-containing napthene low-pressure liquified gas as an extraction medium; by using the characteristics of stable chemical properties, safety, no toxicity, nonflammability, and lipid component solubility after liquefaction for fluorine-containing napthene, the method extracts lipid components (grease, lipoid, oil-soluble pigments, essential oil, wax, etc) in some raw materials at a low temperature and pressure; the energy consumption is low; the extraction efficiency is high; the product quality is good; normal temperature or low temperature operation of the whole process is realized; various functional components in the raw materials are ensured to not be destroyed thermally to a maximum extent; degreased meal can be used for secondary deep development; the invention facilitates the realization of the comprehensive utilization and high added value processing of raw materials, and has important application value.

Description

technical field [0001] The invention relates to lipid processing technology, in particular to a method for extracting lipid components. Background technique [0002] Lipids are a class of natural organic compounds that contain alkyd esterification structures, are soluble in organic solvents but not in water, are essential nutrients for the human body, and are important components of the human body, including fats and lipids. Commonly referred to as fats include fats and oils, those that are in a solid state at room temperature are called "fat"; those that are in a liquid state are called "oil". Daily edible animal and vegetable oils, such as lard, vegetable oil, soybean oil, and sesame oil, are all fats and oils, that is to say, daily edible oils are fats. Lipids are substances very similar to fats and oils. There are many types, mainly including: lecithin, neurophospholipids, cholesterol and lipoproteins. The so-called lipid components also include some fat-soluble pigmen...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B1/10C11B1/00C11B1/04C11B9/02C11B11/00C07C49/255C07C45/79C09B61/00C07C33/02C07C29/76
CPCY02W30/74
Inventor 杨继国
Owner SOUTH CHINA UNIV OF TECH
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