A kind of preparation technology of β-carotene microcapsule
A technology of carotene and preparation process, which is applied in food coating, radioactive physical shape, food science, etc., can solve the problems of failing to meet product safety and hygiene standards, affecting product use effect, unfavorable cold water diffusion, etc., and achieve good Embedding effect, avoiding moisture absorption and adhesion, and good solubility
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Embodiment 1
[0021] (1) Add 200kg of hydroxypropyl etherified-octenyl succinic esterified starch into 500kg of water at 60-80°C, and stir to dissolve it. Add 5kg trehalose and 5kg EDTA-Na into the dissolved composite modified starch (hydroxypropyl etherified-octenyl succinic esterified starch), and stir while adding to make it evenly mixed, 50-70 ℃ heat preservation and standing for later use to obtain an aqueous phase.
[0022] (2) 4.5kg β-carotene (content is 96%), 0.1kg microporous octenyl succinic acid corn starch, 0.1kg natural vitamin E, 0.1kg propyl gallate (PG) are added in 50kg sunflower oil , under a nitrogen atmosphere, an oil bath at 120-180° C. for 3-10 minutes to obtain an oil phase.
[0023] (3) Discharge the dissolved water phase and oil at the same time, control the flow rate separately, according to the water phase: oil phase = 13:1 (mass ratio), mix online with a pipeline shearer, and the number of revolutions is 10000-16000 rpm 5 to 10 minutes, 19000 to 28000 rpm for ...
Embodiment 2
[0026] (1) Add 200kg of hydroxypropyl etherified-octenyl succinic esterified starch into 800kg of water at 60-80°C, and stir to dissolve it. Add 5kg trehalose and 5kg sodium ascorbate into the dissolved composite modified starch (hydroxypropyl etherified-octenyl succinic esterified starch), stir while adding, make it evenly mixed, 50~70℃ Heat preservation and stand for later use to obtain an aqueous phase.
[0027] (2) 3.7kg β-carotene (content 96%), 0.1kg microporous octenyl succinic acid cornstarch, 0.1kg natural vitamin E, 0.1kg tert-butylhydroquinone (TBHQ) are added to 50kg corn oil , in a nitrogen atmosphere, in an oil bath at 120-180° C. for 3-10 minutes, to obtain an oil phase.
[0028] (3) Discharge the dissolved water phase and oil at the same time, control the flow rate separately, according to the water phase: oil phase = 20:1 (mass ratio), mix online with a pipeline shearer, and the number of rotations is 10,000 to 16,000 rpm 5 to 10 minutes, 19000 to 28000 rpm ...
Embodiment 3
[0031] (1) Add 100kg of hydroxypropyl etherified-octenyl succinic esterified starch into 400kg of water at 60-80°C, and stir to dissolve it. Add 5kg trehalose and 5kg tea polyphenols into the dissolved composite modified starch (hydroxypropyl etherified-octenyl succinic esterified starch), and stir while adding to make it evenly mixed, 50-70 ℃ heat preservation and standing for later use to obtain an aqueous phase.
[0032](2) 2.1kg beta-carotene (content 96%), 0.1kg microporous octenyl succinic acid corn starch, 0.1kg natural vitamin E, 0.1kg butylated hydroxytoluene (BHT) are added in 50kg sunflower oil, Under nitrogen environment, oil bath at 120-180° C. for 3-10 minutes to obtain an oil phase.
[0033] (3) Discharge the dissolved water phase and oil at the same time, control the flow rate separately, according to the water phase: oil phase = 10:1 (mass ratio), mix online with a pipeline shearing machine, and the number of rotations is 10,000 to 16,000 rpm 5 to 10 minutes...
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