Purifier and preparation method thereof
A purifier and alumina powder technology, applied in ceramic products, other household utensils, applications, etc., can solve the problems of complex synthesis process, high brittleness, strong ionic bond, etc., and achieve simple and efficient preparation method, small thermal expansion coefficient, The effect of high compressive strength
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[0035] The preparation method of the purifier of the present invention comprises the following steps:
[0036] 1) Preparation of ceramic slurry: Mix the alumina powder, sintering aids, rare earth oxides and binders evenly to obtain mixed powder, and mix the mixed powder with water in a mass ratio of (80-85):100. Mixing, then adding carbon fiber, dispersing evenly to obtain ceramic slurry;
[0037] 2) forming a blank to obtain a blank;
[0038] 3) Sintering: a. After sintering the green body at 1100-1200℃ for 60-90min under normal pressure, b. Adjust the pressure to 20MPa, adjust the temperature to 800-1000℃ and continue sintering for 30-60min, c. Heat preservation at 700°C for 90-120min to obtain a honeycomb ceramic carrier;
[0039] 4) carrier coating and dipping: the slurry solution is coated on the surface of the prepared honeycomb ceramic carrier, and after drying treatment, the carrier is put into the active component solution containing palladium, platinum and rhodium ...
Embodiment 1
[0043] The purifier of this embodiment includes a housing and a honeycomb ceramic carrier. The honeycomb ceramic carrier is arranged in the housing. The porous structure of the honeycomb ceramic carrier includes a curved serpentine channel and a straight channel. The straight channel is connected to the serpentine channel. The components of the carrier and their mass fractions include: sintering aid: 6%, rare earth oxide: 5%, methyl cellulose: 4%, carbon fiber: 2%, and the remaining 83% is alumina powder. The sintering aids are MgO and CaO with a mass ratio of 1:1, and the rare earth oxides can be one or two of rare earth oxides such as lanthanum oxide, cerium oxide, rubidium oxide, praseodymium oxide, dysprosium oxide, promethium oxide, etc. A mixture of two or more. The length ratio of the straight channel to the serpentine channel is 5:3, and the average wall thickness of the honeycomb ceramic is 1mm.
Embodiment 2
[0045] The purifier of this embodiment includes a housing and a honeycomb ceramic carrier. The honeycomb ceramic carrier is arranged in the housing. The porous structure of the honeycomb ceramic carrier includes a curved serpentine channel and a straight channel. The straight channel is connected to the serpentine channel. The components of the carrier and their mass fractions include: sintering aid: 7%, rare earth oxide: 4%, methyl cellulose: 2%, carbon fiber: 2%, and the remaining 85% is alumina powder. The sintering aids are MgO and SiO with a mass ratio of 2:1:1 2 and Fe 2 O 3 The rare earth oxide can be one or a mixture of two or more rare earth oxides such as lanthanum oxide, cerium oxide, rubidium oxide, praseodymium oxide, dysprosium oxide, and promethium oxide. The length ratio of the straight channel and the serpentine channel is 5:2, and the average wall thickness of the honeycomb ceramic is 1.5mm.
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Abstract
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