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Preparation method and preparation device of choline chloride powder

A choline chloride water agent and choline chloride technology, which are applied in botany equipment and methods, biocides, animal repellants, etc., can solve the problems of long production cycle, affecting product quality, and high energy consumption for drying , to achieve the effect of increasing the price period

Pending Publication Date: 2016-08-24
SHANDONG AOCTER CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the existence of small wrinkle openings or small channel holes on the carrier will consume a lot of energy and time for drying, and the production cycle will be longer
[0009] Second, the product shelf life is short
When the carrier is dried, there is still a small amount of water in the openings of small wrinkles or small pores and caves that have not been dried, and the powder may deteriorate during long-term storage, affecting product quality
In particular, the choline chloride powder using plant-based carriers will also produce moisture absorption and deterioration, which will affect product quality.

Method used

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  • Preparation method and preparation device of choline chloride powder
  • Preparation method and preparation device of choline chloride powder
  • Preparation method and preparation device of choline chloride powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0069] Example 1. A preparation method for choline chloride powder, is characterized in that, comprises the steps:

[0070] Step 1: obtaining the choline chloride aqueous solution whose weight percentage of choline chloride is 50%;

[0071] Step 2: Adding a spray auxiliary agent to the choline chloride aqueous solution, the amount of the spray auxiliary agent added is 2 to 15% of the weight of the choline chloride aqueous solution, and mixing and stirring evenly;

[0072] Step 3: Pump the choline chloride water agent added with spray aid into the spray drying equipment for spray drying. The pressure of the nozzle is controlled at 3.5Mpa, the inlet air temperature is 210°C, and the outlet air temperature is 100°C, and the choline chloride is dried. powder;

[0073] Step 4: Send the choline chloride dry powder into a mixing tank, add potassium ferrocyanide whose weight is 3% of the choline chloride dry powder to the mixing tank, stir and mix to obtain the choline chloride powd...

Embodiment 2

[0076] Example 2. A preparation method for choline chloride powder, is characterized in that, comprises the steps:

[0077] Step 1: obtaining the choline chloride aqueous solution whose weight percent of choline chloride is 75%;

[0078] Step 2: Adding a spray auxiliary agent to the choline chloride aqueous solution, the amount of the spray auxiliary agent added is 2 to 15% of the weight of the choline chloride aqueous solution, and mixing and stirring evenly;

[0079] Step 3: Pump the choline chloride water agent added with spray aid into the spray drying equipment for spray drying. The nozzle pressure is controlled at 4Mpa, the air inlet temperature is 260°C, and the air outlet temperature is 120°C to obtain dry choline chloride powder ;

[0080] Step 4: send the choline chloride dry powder into the mixing tank, add 5% calcium stearate with a weight of 5% of the choline chloride dry powder to the mixing tank, stir and mix to obtain the choline chloride powder.

[0081] Th...

Embodiment 3

[0083] Example 3. A preparation method for choline chloride powder, is characterized in that, comprises the steps:

[0084] Step 1: obtaining a choline chloride aqueous solution with a weight percentage of 50% to 80% of choline chloride;

[0085] Step 2: Adding a spray auxiliary agent to the choline chloride aqueous solution, the amount of the spray auxiliary agent added is 2 to 15% of the weight of the choline chloride aqueous solution, and mixing and stirring evenly;

[0086] Step 3: Pump the choline chloride water agent added with spray aid into the spray drying equipment for spray drying. The pressure of the nozzle is controlled at 5.0Mpa, the inlet air temperature is 300°C, and the outlet air temperature is 150°C, and the choline chloride is dried. powder;

[0087] Step 4: Send the dry choline chloride powder into a mixing tank, add silicon dioxide whose weight is 30% of the dry choline chloride powder to the mixing tank, stir and mix to obtain the choline chloride powd...

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Abstract

The invention discloses a preparation method and a preparation device of choline chloride powder. The preparation method includes: obtaining choline chloride water of 50-80% in weight percentage of choline chloride; adding a spray auxiliary into the choline chloride water, and mixing and stirring well, wherein adding quantity of the spray auxiliary is 2-15% of weight of the choline chloride water; pumping the choline chloride water added with the spray auxiliary into spray drying equipment for spray drying; step 4, feeding choline chloride dried powder into a mixing tank, adding one of or a mixture of multiple of potassium ferrocyanide, sodium silicoaluminate, tricalcium phosphate, silica, microcrystalline cellulose and calcium stearate accounting for 3-30% of weight of the choline chloride dried powder, and stirring and mixing to obtain the choline chloride powder. The preparation device comprises an air feeding system, a liquid feeding system, a spray drying system, a mixing system, a tail gas treatment system and a pipeline. The preparation method and the preparation device have the advantages of quickness in drying and low energy consumption.

Description

technical field [0001] The invention relates to the field of food additives, in particular to a method and device for preparing choline chloride powder. Background technique [0002] Choline (scientific name 2-hydroxyethyl-trimethylcholine hydroxide), a kind of vitamin B. Choline can promote fat metabolism in the liver and kidney; choline is also the basis for the body to synthesize acetylcholine, thereby affecting the transmission of nerve signals. In addition, choline is also one of the methyl sources required for the synthesis of methionine in the body. Natural choline is contained in many foods, but its concentration is not enough to meet the needs of the modern feed industry for the rapid growth of animals, so synthetic choline should be added to the feed to meet its needs. Lack of choline can lead to fatty liver, slow growth and increased death in poultry and livestock. Choline chloride is the hydrochloride of choline. In general animal rations, it has been widely u...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23K20/105A23K40/10A01N33/12A01N25/12A01P21/00
CPCA01N25/12A01N33/12A23N17/00A01N2300/00
Inventor 曹俊山郝秀利赵士辉王淑华
Owner SHANDONG AOCTER CHEM
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