Dry powder reflective thermal insulation coating
A heat insulation and coating technology, applied in the direction of reflection/signal coating, cement coating, coating, etc., can solve the problems of reducing the thermal conductivity coefficient of heat insulation coating, weak UV resistance of coating, short service life, etc., and achieve relative solution Capacitance and processing problems, suppression of efflorescence, and improvement of wear resistance
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[0033] H1: Polymer-modified graphene oxide, prepared by the following method:
[0034] (1) Synthesis of NTDA-terminated polypyrrolene prepolymer
[0035] In a 100 mL dry three-necked flask, add 10 mmol of 3,3'-diaminobenzidine DAB, 11 mmol of 1,4,5,8-naphthalene tetracarboxylic anhydride NTDA, 22 mmol of benzoic acid, 3 mL of isoquinoline and 40 mL of m -cresol, under nitrogen protection and magnetic stirring; after 2 hours, heat up to 85°C for 6h, 190°C for 21h, after the reaction, cool down to 70°C and quickly pour it into 150mL methanol to obtain a large amount of solid precipitation; wash the product repeatedly with methanol Finally, filter and collect the polymer, and dry it in a vacuum oven at 160°C for 20 hours for use;
[0036] (2) Synthesis of amino-terminated sulfonated polyimide prepolymer
[0037] In a 100mL dry three-neck flask, add 1.6mmol 2,2'-bis(4-sulfophenoxy)biphenyldiamine, 12.5mL m-creso1 and 0.8mL triethylamine successively, and protect with nitrogen ga...
Embodiment 1
[0059] In parts by weight, add 30 parts of A1, 8 parts of B1, 8 parts of C1, 7 parts of D1, 8 parts of E1, 3 parts of F1, 7 parts of G1, 25 parts of H1 and 5 parts of I1 into the mixer and mix well for 10 minutes , and the output is dry powder coating. According to the weight ratio, mix the powder and water according to the ratio of 1:0.5, and then apply it on the wall to complete the construction.
Embodiment 2
[0061] In parts by weight, add 30 parts of A1, 8 parts of B1, 8 parts of C1, 7 parts of D1, 8 parts of E1, 3 parts of F1, 7 parts of G1, 25 parts of H2 and 5 parts of I1 into the mixer and mix well for 10 minutes , and the output is dry powder coating. According to the weight ratio, mix the powder and water according to the ratio of 1:0.5, and then apply it on the wall to complete the construction.
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