Tobacco extract, extracting method and application

A technology of tobacco extract and extraction method, which is applied in the field of tobacco additives, can solve the problems of loss of acidic and neutral aroma components, incomplete dissolution of aroma components, loss of medium and small polar aroma components, etc., to achieve improved baking aroma, Suitable for industrial production and application, the effect of strong aroma of tobacco

Active Publication Date: 2017-01-11
ZHENGZHOU TOBACCO RES INST OF CNTC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most commercially available tobacco extracts are prepared by ethanol continuous extraction method, which has two major disadvantages: ① part of the natural aroma is lost during the extraction process, and the aroma of the product is weak; ② in addition to aroma components, there are also pectin in the product , protein, and hemicellulose substances, these substances will be cracked during the smoking process of cigarettes to produce some harmful components, and at the same time increase the irritation and miscellaneous gas of smoking, and affect the sensory quality (Song Peng. Microbial fermentation reduces harmful substances in cigarette smoke Composition and research on improving cigarette quality [D]. Xi'an: Northwest University, 2008.; Chi Jingji, et al. Correlation analysis between main chemical indicators of tobacco leaves and smoking quality [J]. Journal of Agricultural Sciences of Yanbian University, 2006, 28(3):208-210.)
However, when water is used as the extraction solvent, small and medium polar aroma components cannot be fully dissolved. On the contrary, components that are unfavorable to cigarette smoking such as pectin, protein, and polysaccharides are extracted, and the enzymatic hydrolysis is carried out under acidic conditions....

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  • Tobacco extract, extracting method and application
  • Tobacco extract, extracting method and application
  • Tobacco extract, extracting method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] In this embodiment, the tobacco extract is prepared by the following steps:

[0041] 1) Weigh 1 kg of flue-cured tobacco raw material, put the raw material in a SY-III-A experimental tobacco processor, evenly spray 5% propylene glycol of the raw material mass, place it in a sealed place for 12 hours to fully absorb the tobacco leaves, and then heat it to 80°C for baking 1.5h;

[0042] 2) Grind the roasted raw materials to 200 mesh, add 95% ethanol for extraction, the mass ratio of solid to liquid is 1:10, the extraction temperature is 40°C, and the extraction time is 4 hours; after the extraction, filter out with 400 mesh filter cloth Extraction solution, filter residue plus solvent and extract again;

[0043] 3) Combine the two extracts, first pass through a microfiltration membrane with a pore size of 200nm, then pass through an ultrafiltration membrane with a molecular weight cut-off of 10kD, collect the ultrafiltration permeate, and distill under reduced pressure u...

Embodiment 2

[0046] In this embodiment, the tobacco extract is prepared by the following steps:

[0047] 1) Weigh 1 kg of flue-cured tobacco raw material, put the raw material in a SY-III-A experimental tobacco processor, evenly spray 15% propylene glycol of the raw material mass, place it in a sealed place for 6 hours to fully absorb the tobacco leaves, and then heat it to 120°C for baking 0.5h;

[0048] 2) Grind the roasted raw materials to 20 mesh, add absolute ethanol for extraction, the mass ratio of solid to liquid is 1:10, the extraction temperature is 20°C, and the extraction time is 8 hours; after the extraction, use a 400-mesh filter cloth to filter out Extract the liquid, add solvent to the filter residue and extract again;

[0049] 3) Combine the two extracts, first pass through a microfiltration membrane with a pore size of 50nm, then pass through an ultrafiltration membrane with a molecular weight cut-off of 5kD, collect the ultrafiltration permeate, and distill under reduce...

Embodiment 3

[0052] In this embodiment, the tobacco extract is prepared by the following steps:

[0053] 1) Weigh 1 kg of flue-cured tobacco raw material, place the raw material in a SY-III-A experimental tobacco processor, evenly spray 7% propylene glycol of the raw material mass, place it in a sealed place for 10 hours to fully absorb the tobacco leaves, and then heat it to 100°C for baking 1h;

[0054] 2) Grind the roasted raw materials to 40 mesh, add 95% ethanol for extraction, the mass ratio of solid to liquid is 1:8, the extraction temperature is 10°C, and the time is 10h; after the extraction, filter out with 400 mesh filter cloth Extraction solution, filter residue plus solvent and extract again;

[0055] 3) Combine the two extracts, first pass through a microfiltration membrane with a pore size of 100nm, then pass through an ultrafiltration membrane with a molecular weight cut-off of 8kD, collect the ultrafiltration permeate, and distill under reduced pressure until there is no ...

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Abstract

The invention discloses a tobacco extract, an extracting method and application and belongs to the field of tobacco additives. The tobacco extract is extracted with the method including the following steps that firstly, propylene glycol is added into tobacco raw materials, and then baking is carried out after standing; secondly, smashing is carried out, and a solvent is added into powder materials for extraction; thirdly, extract liquid passes through an ultrafiltrtion membrane, penetrating liquid is obtained and subjected to reduced pressure distillation, and concentrate is obtained; fourthly, the concentrate is subjected to secondary separation with a molecule distillation method, light components are collected, and the tobacco extract is obtained. The extract contains rich megastigmatrienone, Damascone, neophytadiene, phenylcarbinol, phenethyl alcohol, farnesylacetone and pyrone and furanone aroma components, and the tobacco extract is thick in baking aroma and tobacco aroma, good in penetration, small in irritation and miscellaneous gas, high in satisfaction, capable of improving the smoking quality of cigarettes and providing a certain amount of nicotine to meet the physiological needs of consumers when used.

Description

technical field [0001] The invention relates to a tobacco extract, and also relates to an extraction method and application, belonging to the field of tobacco additives. Background technique [0002] Tobacco stems, the main veins of tobacco leaves, account for about 25% to 30% of the weight of tobacco leaves. my country is a big tobacco producing country, producing about hundreds of thousands of tons of tobacco stems every year. Among them, some tobacco stems are manufactured by expansion technology into expanded stems and added to the leaf group formula, and some tobacco stems and waste tobacco leaves (fragments, tobacco powder) are added with wood pulp as raw materials to make reconstituted tobacco leaves. Using a certain proportion of expanded cut stems and reconstituted tobacco leaves in the cigarette leaf group formula can reduce the tar release and increase the filling value of cigarettes. However, shredded stems and reconstituted tobacco leaves have heavy miscellane...

Claims

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Application Information

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IPC IPC(8): A24B15/24
CPCA24B15/24
Inventor 张文娟徐秀娟屈展孙世豪马骥霍现宽杨伟平张启东柴国璧姬凌波张建勋
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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