Method for producing nitroalkane and co-producing ketoxime

A technology of nitroalkane and nitropropane, which is applied in the field of producing nitroalkane and co-producing ketoxime, can solve the problems that do not involve high-selectivity nitroalkane and co-produce ketoxime, and achieve high product yield and process reaction The effect of mild conditions and enhanced production flexibility
CN107641084AActive Publication Date: 2018-01-30BEIJING RISUN TECH CO LTD
8 Cites 5 Cited by

Patent Information

Authority / Receiving Office
CN · China
Current Assignee / Owner
BEIJING RISUN TECH CO LTD
Publication Date
2018-01-30

Smart Images

  • Figure 1
    Figure 1
  • Figure 2
    Figure 2
  • Figure 3
    Figure 3
Patent Text Reader

Abstract

The invention relates to a method for producing nitroalkane and co-producing ketoxime. The method comprises the following steps: in the presence of a molecular sieve catalyst of ketone ammoxidation, taking ketone, ammonia and hydrogen peroxide as reaction raw materials to generate nitroalkane and co-generate ketoxime. The method disclosed by the invention is mild in reaction conditions, safe and environment-friendly, simple in separation and high in the purity of the product, and the yield of the nitroalkane in the product can be adjusted, so as to obtain the ratio of the required nitroalkaneto ketoxime, so that the method for producing nitroalkane and co-producing ketoxime enhances the production elasticity of the nitroalkane, and the economic benefits of the whole process are improved.
Need to check novelty before this filing date? Find Prior Art

Description

technical field

[0001] This application relates to a method for producing nitroalkanes and co-producing ketoxime, in particular to a method for producing nitroalkanes and co-producing ketoxime by using a specific catalyst and using ketone, ammonia and hydrogen peroxide as raw materials . Background technique

[0002] Nitroalkane is an important fine chemical raw material, such as 2-nitropropane can be used to produce 2-amino-2-methylisopropanol and so on. At present, the production method of this nitroalkane all adopts the nitration method of alkane (as disclosed in the Chinese patent application CN201080047327.4), and the Chinese patent application CN201010592408.4 has also carried out certain improvements in the reactor and other aspects. However, in these methods, there are still problems of dangerous operation, serious pollution and low selectivity of target products.

[0003] Ketoxime, such as acetone oxime, as a low toxicity, efficient reducing agent, has not only be...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More