Preparation method of dielectric material for high energy storage capacitor
A technology of dielectric materials and capacitors, applied in the direction of fixed capacitor dielectrics and components of fixed capacitors, to achieve the effects of simple equipment, uniform particles, and high breakdown field strength
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Embodiment 1
[0024] The preparation method of the dielectric material for high energy storage capacitors in this embodiment, the specific steps are as follows:
[0025] 1) Nano-ZnO particles are placed in a high-speed ball mill, and then sodium dodecylbenzenesulfonate in an amount of 1.25% of the mass of the nano-ZnO particles is dissolved in 2 times the volume of deionized water and stirred until completely dissolved, then loaded In the atomizer, first adjust the high-speed ball mill to a low speed of 100r / min, and spray the sodium dodecylbenzenesulfonate solution on the surface of the nano-ZnO particles while the ball mill is rotating. After spraying, increase the speed of the high-speed ball mill to 100r / min. 4500r / min for ball milling pretreatment for 20min, after natural ventilation and drying, then add the modified nano-ZnO particles, aniline, ammonium persulfate initiator into the autoclave, first pass a small amount of CO 2 Exhaust the internal air, and then inject CO with a high-p...
Embodiment 2
[0029] This embodiment is the same as embodiment 1, and the difference is that in the present embodiment, the nano-inorganic particles are Al 2 o 3 , the surfactant is sodium dodecylsulfonate, the addition amount is 0.8% of the mass of nano-ceramic particles, and the condition of magnetron sputtering is that the vacuum degree is 5×10 - 4 Pa, the gas flow rate is 8mL / min, the working pressure is 0.6Pa, the sputtering power is 50w, and the sputtering time is 80s.
Embodiment 3
[0031] The present embodiment is the same as Example 1, and the difference is that in the present embodiment, the nano-inorganic particle graphene, the surfactant addition is 1.5% of the nano-ceramic particle quality, and the nano-inorganic particle, aniline and initiator mass ratio are 0.35:1: 0.015, the condition of magnetron sputtering is that the vacuum degree is 8×10 -4 Pa, the gas flow rate is 17mL / min, the working pressure is 0.9Pa, the sputtering power is 75w, and the sputtering time is 100s.
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