UV-curable environment-friendly nail polish and preparation method thereof
A nail polish and environmental protection technology, applied in the field of material chemistry, can solve the problems of nail polish cracking, poor adhesion, slow curing speed, etc., and achieve the effects of good adhesion, fast film formation, and good wear resistance and heat resistance.
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Embodiment 1
[0032] A kind of UV curing environment-friendly nail polish and preparation method thereof, concrete steps are as follows:
[0033] Take pentaerythritol tetrakis (2-mercaptoacetate) 48g in four-necked flask, add 1,4-butanediol diacrylate 56g, hydroquinone 0.1g, 2-methyl-1-(4 -Methylthiophenyl)-2-morpholino-1-acetone 3g, start stirring, at room temperature, 300-400r / min stirring for 0.5 hours, the output is UV curable nail polish resin prepolymer;
[0034] 64g of nail polish resin prepolymer obtained above, 6g of bentonite, 8g of talc, 4g of calcium carbonate, 4g of titanium dioxide, 3.2g of iron red, 0.3g of wetting and dispersing agent, 0.15g of leveling agent, and 0.12g of defoaming agent Add it to the mixing container and grind it to obtain material a, the grinding speed is 900r / min, and the grinding time is 1.5 hours; then add 0.15g of sweet-scented osmanthus essence and stir at a high speed for 0.5h, and the high speed stirring speed is 1500r / min; then add 1.5g of hydroxy...
Embodiment 2
[0036] A kind of UV curing environment-friendly nail polish and preparation method thereof, concrete steps are as follows:
[0037] Weigh 2,3-dimercapto-1-propanol (3-mercaptoacetate) 42g in a four-necked flask, add triethylene glycol dimethacrylate 58g, hydroquinone 0.1g, 2 -Methyl-1-(4-methylthiophenyl)-2-morpholino-1-propanone 3g, start stirring, at room temperature, 300-400r / min stirring for 1 hour, the output is UV cured nail Oleoresin prepolymers;
[0038]Add 66g of the nail polish resin prepolymer obtained above, 9g of bentonite, 9g of talc, 8g of titanium dioxide, 0.9g of ultramarine blue, 0.3g of wetting and dispersing agent, 0.15g of leveling agent, and 0.12g of defoaming agent into the container in sequence Grinding to obtain slurry a, grinding speed 900r / min, grinding time 1.5 hours to obtain material a, high-speed stirring speed 1500r / min After 0.5 hours, add rose essence 0.15g, continue stirring for 0.5 hours, add hydroxyethyl cellulose 3g and stir for 1 At the...
Embodiment 3
[0040] A kind of UV curing environment-friendly nail polish and preparation method thereof, concrete steps are as follows:
[0041] Take pentaerythritol tetrakis(2-mercaptoacetate) 42g in four-necked flask, add epoxy-modified acrylate 58g, hydroquinone 0.1g, 2-methyl-1-(4-methylthio) therein 3 g of phenyl)-2-morpholino-1-acetone, start stirring, and stir at 300-400 r / min for 1 hour at room temperature, and the output is UV-curable nail polish resin prepolymer;
[0042] 66g of nail polish resin prepolymer obtained above, 6g of bentonite, 5g of calcium carbonate, 8g of talcum powder, 8g of titanium dioxide, 0.9g of iron red, 0.4g of wetting and dispersing agent, 0.2g of leveling agent, and 0.15g of defoaming agent Add to the container and grind to obtain material a, the grinding speed is 900r / min, and the grinding time is 1.5 hours; the high-speed stirring speed is 1500r / min for 0.5 hours, then add 0.15g of rose essence, continue to stir for 0.5 hours, then add 3g of hydroxyethy...
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