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Metal fine polishing antigorite powder as well as preparation method and application thereof

A technology of serpentine powder and leaf serpentine, which is applied to chemical instruments and methods, polishing compositions containing abrasives, other chemical processes, etc., can solve the problem of many scratches on the polished surface, long polishing time and low polishing accuracy. and other problems, to achieve the effect of improving gloss, improving gloss, and polishing effect.

Inactive Publication Date: 2020-06-26
CHINA UNIV OF GEOSCIENCES (BEIJING)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For example, patent applications CN200710300043A and CN103952083A respectively disclose methods for producing polishing powder with hard kaolin, but all involve high-temperature calcination of kaolin, and such calcined products all contain mullite crystal phases, and the hardness is usually greater than 7, so that in fine polishing hard scratches
At the same time, although graphite, talc, pyrophyllite and other mineral powders with a Mohs hardness lower than 2 can be used for fine polishing of metal surfaces without calcination, but due to the low hardness, there are disadvantages such as long polishing time and low efficiency.
[0004] In addition, because the polishing powder in the existing micro-nano polishing materials is approximately spherical particles, there are also problems such as many scratches on the polished surface and low polishing accuracy.

Method used

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  • Metal fine polishing antigorite powder as well as preparation method and application thereof
  • Metal fine polishing antigorite powder as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] (1) Preparation

[0048] Select and use natural antigorite minerals (excluding olivine and chrysotile, and the composition of the atomic number ratio conforms to Si 5.8-6.2 [Mg 3.8-4.2 o 9.8-10.2 ](OH) 7.8-8.2 ) as a raw material, after it is roughly crushed by a jaw crusher, it is processed by a ball mill wet grinding method under stirring to obtain a fine powder.

[0049] Stir and mix 20kg of the obtained fine powder with 180kg of water and 10g of oleylamine in a vertical mixer for 120min to obtain an aqueous suspension. Then, utilize the GSDF50 cyclone (working pressure is 0.3MPa) to carry out cyclone classification treatment to this aqueous suspension and measure powder size on-line (BT-9300ST type laser particle size distribution analyzer), and collect the diameter in 3-18μm The overflow liquid of flake powder within the range of 20-24 and the flake diameter / thickness ratio in the range of 20-24. The obtained overflow liquid was dried (HB881-8 drying oven, 105...

Embodiment 2

[0057] (1) Preparation

[0058] Except that polyvinylpyrrolidone was used instead of oleylamine, metal fine polished antigorite powder was prepared by the same process as in Example 1, and the same detection and analysis as in Example 1 were carried out.

[0059] As a result, the resulting metal finely polished antigorite powder has the atomic ratio composition formula of Si 5.95 [Mg 4.05 o 10.05 ](OH) 7.95, the Mohs hardness is 4.0; and the morphology of the powder in the obtained metal finely polished antigorite powder is in the shape of a roughly cuboid sheet with a sheet diameter in the range of 3 to 15 μm and a sheet diameter / thickness ratio of 20 ~24 range.

[0060] (2) Application

[0061] Except using the 45# steel plate sample with the same size and its initial surface roughness is 90nm, the solid content of the metal fine polishing antigorite powder of the obtained metal fine polishing antigorite powder prepared by the same procedure as Example 1 is a polishing ...

Embodiment 3

[0063] (1) Preparation

[0064] Except that sodium dodecylbenzenesulfonate was used instead of oleylamine, metal fine polished antigorite powder was prepared by the same process as in Example 1, and the same detection and analysis as in Example 1 were carried out.

[0065] As a result, the resulting metal finely polished antigorite powder has the atomic ratio composition formula of Si 5.85 [Mg 4.15 o 10.15 ](OH) 7.92 , the Mohs hardness is 4.2; and the morphology of the powder in the obtained metal finely polished antigorite powder is in the shape of a roughly cuboid sheet with a sheet diameter in the range of 3 to 18 μm and a sheet diameter / thickness ratio of 22 -24 range.

[0066] (2) Application

[0067] Except using the GH1015 nickel alloy plate sample with the same size and its initial surface roughness as 42.3nm, the resulting metal finely polished antigorite powder had a solid content of 8.5% by mass prepared by the same procedure as in Example 1. liquid and perfo...

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Abstract

The invention relates to metal fine polishing antigorite powder as well as a preparation method and application thereof. More specifically, the present invention provides metal fine polishing antigorite powder which is composed of surface-modified sheet-shaped powder, the atomic number ratio structural formula of the sheet-shaped powder being Si<5.8-6.2>[Mg<3.8-4.2>O<9.8-10.2>](OH)<7.8-8.2>, the sheet diameter being in the range of 3-18 [mu]m, and the sheet diameter / thickness ratio being in the range of 20-24. The polishing material is moderate in hardness (the Moh's hardness is within the range of 3.5-4.5), good in metal fine polishing effect, high in efficiency, environmentally friendly and clean, the preparation process is simple, the raw material source is wide, and the cost is low.

Description

technical field [0001] The invention belongs to the field of metal surface treatment, and in particular relates to metal fine polishing antigorite powder and its preparation method and application. Background technique [0002] Polishing powder and polishing liquid are the key materials commonly used in fine metal surface treatment. Polishing powder is a commonly used material in the metal polishing process. Its function is to reduce the roughness of the processed surface, improve the gloss and eliminate stains through the adsorption and grinding between the polishing powder and the polished object. It is mainly used for metal workpieces. fine grinding and polishing. Polishing powder is usually composed of α-corundum, quartz, cerium oxide, lanthanum oxide, zirconia, silicon carbide, silicon nitride and other components. Most of their Mohs hardness (Moh'shardness) is above 7, which belongs to high hardness abrasives. Hard scratches are thus likely to occur in fine polishing...

Claims

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Application Information

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IPC IPC(8): C09K3/14C09G1/02
CPCC09G1/02C09K3/1454
Inventor 白志民余良李桂金李硕
Owner CHINA UNIV OF GEOSCIENCES (BEIJING)