Composite fiber material for wig and preparation method of composite fiber material

A composite fiber and wig technology, which is applied in the direction of wigs, fiber chemical characteristics, applications, etc., can solve the problems of unsatisfactory breaking strength and elongation of composite fibers, skin-friendly, poor air permeability and hygroscopicity, and air permeability and skin-friendly effects. problems such as poor, to achieve excellent high hygroscopicity, improve compatibility, improve spinnability and water absorption effect

Active Publication Date: 2021-05-28
SHAOYANG SUNSHINE HAIR PROD
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  • Description
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  • Application Information

AI Technical Summary

Problems solved by technology

However, the currently researched polymers are mainly synthetic fibers such as PVC and polyacrylonitrile. The breaking strength and elongation of the composite fibers spun by them are not ideal, and the skin-friendly, air permeability and hygroscopicity are poor.
[0004] Chinese invention patent CN104862818A discloses a method for preparing keratin composite fibers. It mixes dry keratin powder, fiber-forming polymers, ionic liquids, etc., and mechanically stirs and dissolves at a certain temperature to obtain a keratin composite solution. The keratin composite fiber is prepared by the silk process, and the strength and elongation at break of the composite fiber are greatly improved compared with the pure keratin fiber, but the fiber-forming high polymer is a chemical synthetic fiber, which pollutes the environment and has poor air permeability and skin-friendly effect. Poor, general elasticity
Chinese invention patent CN105002591B discloses a method for preparing composite fibers for hair with quail feathers. The method uses quail feather protein, sodium alginate and polyvinyl alcohol as raw materials to prepare artificial wigs by wet spinning. The artificial wig fibers have Excellent flame retardancy, heat resistance, high strength, soft hand feeling and good gloss, but the artificial wig has poor toughness, easy breakage and poor coloring effect

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Composite fiber material for wig and preparation method of composite fiber material

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preparation example Construction

[0032] The preparation method of the pig hair keratin solution in the present invention is as follows: the pig hair is cleaned, impurity-removed and dried, then pulverized, and then mixed evenly with 0.5 mol / L tributyl phosphine solution, and the temperature is raised to 60-70°C , stirred and reacted for 2-3h, then dropped into NaOH solution to adjust the pH value to 7.5-8.5, and then centrifuged to remove solid impurities to obtain a pure pig hair protein solution. The protein with a molecular weight cut-off of dialysis bag of 5000-10000 was selected to make The protein content in the pig hair protein solution reaches 8-12%, and the required pig hair keratin solution is obtained. Wherein, the solute mass of the tributyl phosphine solution is 5-8% of the dry weight of pig hair after pulverization.

[0033] The preparation method of the wool keratin solution in the present invention is as follows: wash, remove impurities, and dry the wool, then pulverize it, add 0.5mol / L tribut...

Embodiment 1

[0035] Embodiment 1 A kind of composite fiber material for wig

[0036] A preparation method of a composite fiber material for a wig specifically comprises the following steps:

[0037] (1) Preparation of grafted PBAT: Put 30 parts of PBAT (polybutylene adipate / butylene terephthalate) into 90 parts of phenol / trichloromethane prepared by phenol and chloroform with a mass ratio of 3:1 In the methane solution, raise the temperature to 40°C, stir until dissolved, then add 0.3 parts of potassium persulfate and 6 parts of 1,2,4-1H-triazole, raise the temperature to 90°C, stir for 3 hours to prepare the grafted PBAT solution.

[0038] (2) Preparation of modified keratin: Put 80 parts of montmorillonite / sodium alginate modification solution, 25 parts of hair keratin solution and 3 parts of cross-linking agent sodium periodate into the reaction kettle, and heat up to 70°C , stirred for 3 hours to obtain modified keratin. The hair keratin solution is prepared by compounding pig hair k...

Embodiment 2

[0045] Embodiment 2 A kind of composite fiber material for wig

[0046] A preparation method of a composite fiber material for a wig specifically comprises the following steps:

[0047] (1) Preparation of grafted PBAT: Put 45 parts of PBAT into 225 parts of phenol / chloroform solution prepared by phenol and chloroform with a mass ratio of 3:1, heat up to 50 ° C, stir until dissolved, and then Add 1.35 parts of potassium persulfate and 22.5 parts of 1,2,4-1H-triazole, raise the temperature to 80°C, and stir for 5 hours to obtain a grafted PBAT solution.

[0048] (2) Preparation of modified keratin: put 60 parts of montmorillonite / sodium alginate modification solution, 10 parts of hair keratin solution and 2 parts of crosslinking agent dicyclohexylcarbodiimide (DCC) into the reactor , heated to 50°C and stirred for 3 hours to obtain modified keratin. The hair keratin solution is prepared by compounding pig hair keratin solution and wool keratin solution with a mass ratio of 1.5...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention discloses a composite fiber material for a wig and a preparation method of the composite fiber material, and relates to the field of wig manufacturing raw materials. The invention discloses the composite fiber material for a wig. The composite fiber material is prepared from the following raw materials in parts by weight of 30-45 parts of poly (adipic acid)/butylene terephthalate, 60-80 parts of montmorillonite/sodium alginate modified liquid, 10-25 parts of a hair keratin solution, 2-3 parts of a cross-linking agent, 5-8 parts of a nonionic surfactant and a proper amount of coagulating bath. A preparation method of the composite fiber material comprises the following steps of preparing grafted PBAT; preparing modified keratin; mixing the grafted PBAT solution, the modified keratin, the nonionic surfactant and water, and spinning; and post-processing the composite fiber to obtain the composite fiber material for the wig. The composite fiber material for the wig is wide in raw material source, environmentally friendly, relatively low in cost, excellent in strength, toughness, air permeability and skin friendliness, soft and smooth in hand feeling, good in coloring effect and good in flame retardance.

Description

technical field [0001] The invention belongs to the field of raw materials for making wigs, and in particular relates to a composite fiber material for wigs and a preparation method thereof. Background technique [0002] With the improvement of people's living standards, wig products are becoming more and more popular. At present, the raw materials for making wigs on the market are mostly chemical synthetic fibers. Because they are not restricted by resources, they have been industrialized and have low cost and cheap price. The mainstream of the hair products market. Synthetic fibers commonly used in wigs include PVC fibers, polyacrylonitrile fibers, polyester fibers, polypropylene-based fibers, and protein fibers. Although these synthetic fibers have good elasticity, smoothness, and bright color, their skin-friendly properties , Air permeability and moisture absorption are poor, and there is still a big gap with natural human hair. In addition, most of the synthetic fiber...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10D01F1/09D01F1/07A41G3/00
CPCD01F6/92D01F1/10D01F1/07D01F1/09A41G3/0083
Inventor 黄永祥王士喜黄小云唐泳
Owner SHAOYANG SUNSHINE HAIR PROD
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