Combined degumming and dewaxing process and refining process of wax-containing edible vegetable oil

An edible vegetable oil, degumming and dewaxing technology, applied in the field of combined degumming and dewaxing process and refining process, can solve the problems of high wax viscosity, high consumption, low hardness and the like

Pending Publication Date: 2021-12-17
SHANGHAI HAOYOU IND EQUIP
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) The existing simple freezing and crystallization requires a long freezing time for simple oil freezing (different types of oils have different freezing times, as short as ten hours and as long as 30 to 40 hours). This method has a slow winterization reaction and wax high oil content;
[0005] (2) The existing one is combined with the neutralization alkali refining section, and the free fatty acid in the oil is used to neutralize the alkali refining reaction, then cool down after the winterization dewaxing reaction, and then separate the soapstock and wax fat through a disc centrifuge; this method will There is a loss of oil saponification and a loss of beneficial ingredients oryzanol and phytosterol;
[0006] (3) In the prior art, there is also a method of adding diatomite crystallization nuclei in order to shorten the time (the dewaxing time can be within 20 hours). If diatomite is added, the disc type cannot be used due to the solid minerals therein. Centrifuge separation, the subsequent separation can only be filtered by a filter. If the amount of wax is small and the hardness of the wax is high, the filtration operation is not difficult, but once the amount of solid wax is large or the hardness is low, dewaxing filtration is very difficult. Operation, which seriously affects the processing capacity of the production line, especially rice oil, due to its high wax content, high wax viscosity, and low hardness, the traditional dewaxing process has the problems of difficult operation, high consumption, and low yield.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Combined degumming and dewaxing process and refining process of wax-containing edible vegetable oil
  • Combined degumming and dewaxing process and refining process of wax-containing edible vegetable oil
  • Combined degumming and dewaxing process and refining process of wax-containing edible vegetable oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0192] Raw materials: leached bran oil (hair rice oil), acid value 11.2mgKOH / g, impurity content 10.3%, wax content: 3.2%; phosphorus content 540ppm, water content 0.131%; oryzanol 1.49%; VE and sterols: 2.43%

[0193] The crude bran oil at room temperature is passed into the crude oil inlet pipe, heated to 58°C by the first heater, and a 50wt% citric acid aqueous solution is added through the acid solution inlet until the citric acid accounts for 0.25% of the crude oil weight, and mixed by the first mixer Enter the acid reaction tank, the stirring speed is 60 rpm, and the reaction time is 30 minutes. After the reaction, the reaction rate of non-hydratable phospholipids into hydratable phospholipids is >99.5%; add hot water (75°C) from the first water inlet, and the amount of water added Soft water with 2.5 times the weight content of phospholipids is mixed by the second mixer, cooled to 25°C by the first cooler, and the water-oil mixture is passed into the hydration reaction t...

Embodiment 2

[0198] Raw materials: leached corn germ oil, acid value 5.8mgKOH / g, wax content: 380ppm; moisture content 0.75%, phosphorus content 320ppm; oryzanol 780ppm and VE sterol content higher than 14700ppm.

[0199] The raw corn germ oil at normal temperature is passed into the crude oil inlet pipe, heated to 65°C by the first heater, and the concentration of 50wt% citric acid aqueous solution is added through the acid solution inlet until the citric acid accounts for 0.18% of the crude oil weight, and then passed through the first mixer After mixing, enter the acid reaction tank, the stirring speed is 60 rpm, and the reaction time is 30 minutes. After the reaction, the reaction rate of non-hydratable phospholipids into hydratable phospholipids is >99.5%; add hot water (75 ° C) from the first water inlet, The amount of soft water added is 2.5 times the weight content of phospholipids, mixed by the second mixer, cooled to 25°C by the first cooler, and the water-oil mixture is passed in...

Embodiment 3

[0209] Raw materials: leached sunflower oil, acid value 2.5mgKOH / g, wax content: 900ppm; moisture content 0.75%, phosphorus content 850ppm.

[0210] The normal temperature crude sunflower oil is passed into the crude oil inlet pipe, heated to 60°C by the first heater, and the concentration of 50wt% citric acid aqueous solution is added through the acid liquid inlet until the citric acid accounts for 0.15% of the crude oil weight, and then passed through the first mixer After mixing, enter the acid reaction tank, the stirring speed is 60 rpm, and the reaction time is 30 minutes. After the reaction, the reaction rate of non-hydratable phospholipids into hydratable phospholipids is >99.5%; add hot water (75 ° C) from the first water inlet, The amount of soft water added is 2.2 times the weight content of phospholipids, mixed by the second mixer, cooled to 25°C by the first cooler, and the water-oil mixture is passed into the hydration reaction tank. The hydration reaction tank ha...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
acid valueaaaaaaaaaa
smoke pointaaaaaaaaaa
Login to view more

Abstract

The invention relates to the field of edible oil processing, in particular to a combined degumming and dewaxing process and a refining process of wax-containing edible vegetable oil. On one hand, the invention provides a combined degumming and dewaxing process of wax-containing edible vegetable oil, which comprises the following steps of: reacting wax-containing crude oil with acid to convert non-hydrated phospholipid in the wax-containing crude oil into hydrated phospholipid, then carrying out hydration degumming and winterization dewaxing, and then carrying out centrifugal separation to obtain degummed and dewaxed oil. The method can simplify the processing flow, reduce the investment of a physical refining system and reduce the building area of a workshop. In addition, chemical refining is avoided, VE sterol and oryzanol are reserved to the maximum extent by adopting physical refining on the premise of high yield of finished product oil, and the contents of VE sterol and oryzanol both exceed 10000ppm.

Description

technical field [0001] The invention relates to the field of edible oil processing, in particular to a combined degumming and dewaxing process and a refining process for waxy edible vegetable oil. Background technique [0002] The production of all waxy edible vegetable oils is processed through refining processes such as crude oil removal, degumming, deacidification, desolventization, drying, decolorization, deodorization and winterization dewaxing. With the development of modern society, people pay more attention to healthy eating oil, and the market also prefers to use related rice oil, corn germ oil, sunflower oil and rapeseed oil with a small amount of wax. However, the processing and refining of these kinds of oils must be winterized. Wax (grease) process, winterization dewaxing process is to freeze the oil at low temperature, so that the wax with high freezing point or high melting point solid fat is crystallized, and then separated by solid-liquid separation, but the...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C11B3/04C11B3/12C11B3/00
CPCC11B3/04C11B3/12C11B3/001C11B3/008
Inventor 丁泓滨
Owner SHANGHAI HAOYOU IND EQUIP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products