Anti-cracking, anti-oxidation and anti-rust epoxy finish paint and preparation method thereof
An anti-oxidation and epoxy surface technology, applied in epoxy resin coatings, anti-corrosion coatings, coatings, etc., can solve problems such as performance degradation and cracking, and achieve improved crack resistance, enhanced service performance, and enhanced corrosion resistance. Effect
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[0038] The preparation method of the carbon nanotube slurry of the present embodiment is:
[0039] S111: Add 10-20 parts of carbon nanotubes to 35-45 parts of water to disperse to prepare a carbon nanotube suspension, and then add 1-5 parts by weight of 1-3% lanthanum nitrate aqueous solution, 1-2 parts by weight to the suspension parts of sodium dodecyl benzene sulfonate, ultrasonic dispersion treatment, the treatment is finished, washed with water, and dried to obtain pretreated carbon nanotubes;
[0040] S112: 25-35 parts of pretreated carbon nanotubes are added to 35-45 parts of ethanol solvent, 2-5 parts of chitosan, 1-3 parts of hydrochloric acid solution are added, and then 5-9 parts of N-2-aminoethyl acetate are added yl-3-aminopropyltrimethylsilane, 1-3 parts of triethanolamine borate, and stir well to obtain carbon nanotube slurry.
[0041] In S111 of this embodiment, the power of ultrasonic dispersion is 350-450W, and the ultrasonic time is 15-25min.
[0042] The ...
Embodiment 1
[0049] An anti-cracking, anti-oxidizing and anti-rust epoxy topcoat of the present embodiment includes the following raw materials in parts by weight:
[0050] 35 parts of epoxy resin, 10 parts of acrylic emulsion, 5 parts of modified potassium hexatitanate whiskers, 3 parts of magnesium-aluminum hydrotalcite improvement additives, 5 parts of anti-corrosion additives, 1 part of methyltrimethoxysilane, silicone defoamer 0.2 part of the solvent, 0.1 part of dimethylaminoethanol, and 30 parts of ethanol solvent.
[0051] The modification method of the modified potassium hexatitanate crystal whisker of the present embodiment is:
[0052] S101: The potassium hexatitanate whiskers are firstly sent into the carbon nanotube slurry with twice the amount of carbon nanotubes at a temperature of 75° C., stirred and dispersed for 35 minutes, and the stirring speed is 500 r / min, and the stirring is completed to obtain a modified whisker composite slurry ;
[0053] S102: The modified whisk...
Embodiment 2
[0065] An anti-cracking, anti-oxidizing and anti-rust epoxy topcoat of the present embodiment includes the following raw materials in parts by weight:
[0066] 45 parts of epoxy resin, 20 parts of acrylic emulsion, 9 parts of modified potassium hexatitanate whiskers, 6 parts of magnesium-aluminum hydrotalcite improvement additives, 9 parts of anti-corrosion additives, 5 parts of methyltrimethoxysilane, silicone defoaming 0.8 part of the solvent, 0.7 part of dimethylaminoethanol, and 40 parts of ethanol solvent.
[0067] The modification method of the modified potassium hexatitanate crystal whisker of the present embodiment is:
[0068] S101: The potassium hexatitanate whiskers are firstly sent into 4 times the carbon nanotube slurry at a temperature of 85°C, stirred and dispersed for 45 minutes, the stirring speed is 700 r / min, and the stirring is completed to obtain a modified whisker composite slurry ;
[0069] S102: The modified whisker composite slurry is washed with wat...
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