Nanocapsule containing a bioactive compound, and a method of reducing toxicity resulting from cancer therapy
a bioactive compound and nanocapsule technology, applied in the field of nanocapsules, can solve the problems of high mortality outcome, insoluble or unstable, and poor survival of glioblastoma
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example 1
Cancer Cell Lines and Reagents
[0175]Human pancreatic cancer cell lines, SUIT2 expressing firefly luciferase, were provided by MD Anderson Cancer Center, Houston, Tex. Glioblastoma (U87), colon carcinoma cells (HT-29 and HCT-116), breast cancer cells (triple negative MDA-MB-231, MCF7, and MCF7 chemo-resistant), ovarian cancer cells (OVAR-3), and bladder cancer cells (253J-BV) were tested as well. Cell culture reagents and hemoglobin standard, Drabkin's reagent, ellagic acid, diindolylmethane, and other common reagents were purchased from Sigma (St. Louis, Mo.). D-Luciferin potassium salt was purchased from Caliper Life Sciences (Hopkinton, Mass.). Matrigel was purchased from BD Bioscience (San Jose, Calif.).
example 2
Cells and Cell Culture Procedure
[0176]SUIT2-luc cells were grown in DMEM supplemented with 5% fetal bovine serum, 1% penicillin, and 1% streptomycin. Cells were cultured at 37° C. to sub-confluence and treated with 0.25% w / v trypsin / EDTA to affect cell release from culture flask. After washing cells with culture medium, cells were suspended in DMEM (free of phenol red and fetal bovine serum) and counted.
example 3
Synthesis of Nanocapsules
[0177]PLGA-PEG nanocapsules encapsulating ellagic acid (EA) and / or diindolylmethane (DIM) were prepared by double emulsion / solvent evaporation methods previously described (Bharali D J, Sahoo S K, Mozumdar S, Maitra A. Cross-linked polyvinylpyrrolidone nanocapsules: a potential carrier for hydrophilic drugs. J Colloid Interface Sci. 2003 Feb. 15; 258(2):415-23; and Khalil N M, do Nascimento T C, Casa D M, Dalmolin L F, de Mattos A C, Hoss I, Romano M A, Mainardes R M. Pharmacokinetics of curcumin-loaded PLGA and PLGA-PEG blend nanocapsules after oral administration in rats. Colloids Surf B Biointerfaces. 2013 Jan. 1; 101:353-60, each incorporated herein by reference in their entirety). The molecular weight of PLGA (70% poly L-lactic: 30% polyglycolic acid) ranged from 4,000-12,000 Dalton and the PEG molecular weight ranged from 400-4,000 Dalton. PLGA was preferred because it is bio-degradable, safe and FDA approved. Briefly, a stock solution of PLGA-PEG poly...
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