Method for improving garlic oil yield
A technology for garlic essential oil and yield, which is applied in the directions of essential oils/spice, fat production, etc., can solve the problems of improving distillation efficiency, increasing the yield of garlic essential oil, etc., and achieves the effects of increasing yield and improving quality
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[0041] Example 1, according to the following steps:
[0042] The first step is pretreatment: Place the fresh garlic cloves in 5 times the drinking water, soak for 2 hours, and rinse with running water to remove impurities such as dirt and garlic skin. Control dry water, put it on a crusher and crush it into garlic pulp with a particle size of about 200 mesh.
[0043] The second step is to carry out enzymatic hydrolysis of alliin: add alliinase activity regulator (30 g blue vitriol, 1 kg 20 Baume lime milk, 20 g bittern 20 Baume, at room temperature) per ton of garlic pulp Enzymatic hydrolysis is performed for 1 hour to completely convert alliin into allicin. The enzymatic hydrolysis process ends when the presence of alliin cannot be detected. The specific detection method is: the standard alliin standard solution and the enzymatically hydrolyzed garlic juice On the same piece of silica gel, use a mixture of n-butanol: glacial acetic acid: water (4:1:1) as the mobile phase for chro...
Example Embodiment
[0050] Example 2, the same as Example 1, the first, second, fourth, fifth, and sixth steps are omitted, and the third step different from Example 1 is:
[0051] In the second step, add alliinase activity regulator, add 50 grams of blue alum, 3 kilograms of lime milk, and 100 grams of bittern per ton of garlic pulp.
[0052] The third step is to add transforming agent: add 0.01% hydrochloric acid, disodium hydrogen phosphate 2.4%, sodium bisulfite 0.5% (all calculated based on the amount of enzymatic hydrolysis solution). The transformation agent is first dissolved in a small amount of water, and then added to the enzymatic hydrolysis solution. Enter the loading step.
[0053] If the enzymatic hydrolysis and distillation are carried out in the same container, it can be added before the distillation, and the yield is 0.65% (W / W).
Example Embodiment
[0054] Example 3, the same as Example 1, the first, second, fourth, fifth, and sixth steps are omitted. The third step different from that of Example 1 is:
[0055] In the second step, add alliinase activity regulator, add 30 grams of blue alum, 2 kilograms of lime milk, and 60 grams of bittern per ton of garlic pulp.
[0056] The third step is to add transforming agent: add 0.2% lactic acid, 0.5% sodium bicarbonate, and 0.1% sodium metabisulfite (all calculated based on the amount of enzymatic hydrolysis solution). The transformation agent is first dissolved in a small amount of water, and then added to the enzymatic hydrolysis solution. Enter the loading step.
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