Method for improving garlic oil yield
A technology for garlic essential oil and yield, which is applied in the directions of essential oils/spice, fat production, etc., can solve the problems of improving distillation efficiency, increasing the yield of garlic essential oil, etc., and achieves the effects of increasing yield and improving quality
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Embodiment 1
[0041] Embodiment 1, carry out according to the following steps:
[0042] The first step is pretreatment: put fresh garlic cloves in 5 times drinking water, soak for 2 hours, rinse with running water to remove impurities such as soil and garlic skin. Control the dry clear water, place it on a crusher and crush it into garlic pulp with a particle size of about 200 mesh.
[0043] The second step makes alliin enzymatic hydrolysis: add alliinase activity regulator (30 grams of blue alum, 1 kilogram of milk of lime at 20 degrees Baume, 20 grams of bittern at 20 degrees Baume, by every ton of garlic pulp, at room temperature Enzymolysis for 1 hour, so that alliin is completely converted into allicin. The enzymolysis process ends when no alliin is detected. The specific detection method is: standard solution of alliin, and the enzymolysis garlic juice point On the same silica gel sheet, use n-butanol: glacial acetic acid: water (4:1:1) mixture as mobile phase chromatography, and use...
Embodiment 2
[0050] Embodiment 2, identical with embodiment 1 the first, two, four, five, six steps are omitted, and the 3rd step operation that is different from embodiment 1 is:
[0051] The second step is to add alliinase activity regulator, add 50 grams of blue alum, 3 kg of lime milk, and 100 grams of bittern per ton of garlic pulp.
[0052] The third step is to add conversion agent: add hydrochloric acid 0.01%, disodium hydrogen phosphate 2.4%, sodium bisulfite 0.5% (both are calculated based on the amount of enzymatic hydrolysis solution), the conversion agent is first dissolved with a small amount of water, and then after adding the enzymatic hydrolysis solution Enter the loading step.
[0053] If enzymolysis and distillation are carried out in the same container, it can be added before distillation, and the yield is 0.65% (W / W).
Embodiment 3
[0054] Embodiment 3, identical with embodiment 1 the first, two, four, five, six steps are omitted, and the third step operation different from embodiment 1 is:
[0055] The second step is to add alliinase activity regulator, add 30 grams of blue alum, 2 kg of lime milk, and 60 grams of bittern per ton of garlic pulp.
[0056] The third step is to add conversion agent: add 0.2% lactic acid, 0.5% sodium bicarbonate, and 0.1% sodium metabisulfite (calculated based on the amount of enzymatic hydrolysis solution). Enter the loading step.
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