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Combination processing method of coal tar

A processing method and combined processing technology, applied in the field of coal chemical industry, can solve problems such as utilization rate of heavy distillate oil not involved in coking, short operation period, etc., and achieve the effects of avoiding catalyst carbon deposition, avoiding cracking reaction, and reducing energy consumption

Active Publication Date: 2014-02-12
上海竣铭化工工程设计有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method also does not involve the improvement of the utilization rate of coking heavy distillate oil, and the short operation period of the hydrocracking catalyst due to coking

Method used

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  • Combination processing method of coal tar

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Experimental program
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Effect test

Embodiment 1

[0073] The low-temperature dry distillation coal tar of Yilan lignite, whose properties are shown in Table 1, is sent to the pretreatment unit to remove mechanical impurities and water, and then enters the fractionation tower with the liquid phase of the delayed coking oil gas and hydrocracking heat high-pressure separator to fractionate light fractions Oil (top oil), bottom oil and wax oil, the initial boiling point of wax oil is 320°C, and the final boiling point is 670°C. The bottom oil enters the delayed coking unit. The light distillate oil and wax oil enter the hydrotreating unit for hydrotreating reaction, the gasoline fraction and diesel fraction obtained from the hydrotreating reaction can exit the unit, and the heavy distillate oil obtained from the hydrotreating reaction (the difference between 325°C cutting) into the hydrocracking unit for hydrocracking reaction, the hydrocracking reaction product is separated into gas phase and liquid phase in the hot high-pressur...

Embodiment 2

[0075] The hydrotreating catalyst (by weight of oxides) was prepared with the following composition: Mo, 30.0%; W, 8.0%; Ni, 2.5%; Co, 2.0%.

[0076] The solution containing the active components is a solution containing ammonium metatungstate, ammonium molybdate, nickel nitrate, and cobalt nitrate; the peptizer is nitric acid, the extrusion aid is azurite powder, and the pore expander is carbon black.

[0077] (1) Preparation of silicon-containing aluminum hydroxide. Prepare solid sodium aluminate to a concentration of 200gAl 2 o 3 / L concentrated sodium aluminate solution, then diluted to a concentration of 25gAl 2 o 3 / L sodium aluminate working solution, first add 10L containing 25gAl to the gel forming tank 2 o 3 / L sodium aluminate working solution, while passing air and passing CO with a concentration of 45v% 2 Gas, the reaction temperature is 25°C, the reaction time is 1 hour, and when the pH value reaches 12.0, add alkaline silicon-containing materials according ...

Embodiment 3

[0082] The raw material is a mixed coal tar, the main properties are shown in Table 2. The reaction temperature of the hydrotreating section is 350°C. Before the hydrotreating section, a hydrogenation protecting agent is used for pretreatment. The hydrogenation protecting agent is a conventional hydrogenation protecting agent, with alumina as the carrier, containing 6% molybdenum oxide and 1% cobalt oxide. %, the pore volume is 0.82mL / g, and the specific surface area is 128M 2 / g. The treatment conditions of the hydrogenation protective agent are reaction temperature 310°C, pressure 15.1MPa, hydrogen oil volume ratio 1200:1 and liquid hourly volume space velocity 1.2h -1 . Others are identical with embodiment 2.

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Abstract

The invention comprises a combination processing method of coal tar. The method comprises the steps of: the coal tar raw material: (a) introducing a coal tar raw material, delayed coking gas oil and at least part of a liquid phase from a step (d) into a distillation tower, so as to distillate out a light distillate, wax oil and bottom oil; and subjecting the light distillate and the wax oil to a hydrotreating reaction; (b) carrying out gas-liquid separation on an effluent from the hydrotreating reaction, and sending a liquid phase into a fractionation device, so as to distillate out a light fraction and a heavy fraction; (c) carrying out a hydrocracking reaction on at least part of the heavy fraction obtained in the step (b); (d) sending an effluent from the hydrocracking reaction into a hot high pressure separator, so as to separate out a gas phase and a liquid phase; and sending at least part of the liquid phase to the distillation tower in the step (a); and (e) subjecting the bottom oil obtained from distillation in the step (a) to delayed coking, and sending the delayed coking oil gas to the distillation tower in the step (a). Compared with the prior art, the invention method improves the yield of light fuel production from coal tar, prolongs the service life of a catalyst, and increases operation cycle of the device.

Description

technical field [0001] The invention relates to a combined processing method of coal tar, which belongs to the technical field of coal chemical industry. Background technique [0002] The shortage of crude oil resources in the world is imminent, and the distribution is extremely uneven, while the coal reserves are very abundant, so using coal to produce vehicle fuel oil is a necessary way. The main technologies of coal-to-oil include direct liquefaction of coal and indirect liquefaction of coal, etc., but these technologies are costly and complicated. Another coke production technology can produce coal tar by-product while producing coke, which is a widely used method at present. However, the further processing of coal tar is relatively difficult, the utilization method is relatively single, and the price is relatively low, and the product outlet is not smooth, which is a waste of existing resources, especially in the process of use, which has a very large impact on the env...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G69/00
Inventor 王小英
Owner 上海竣铭化工工程设计有限公司
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