Bacillus subtillis and hymexazol compounded soil treating agent
A solvent and emulsifier technology, applied in the direction of fungicides, biocides, disinfectants, etc., can solve the problems of poor chemical pesticide effect, soil ecosystem damage, and excessive pesticide residues, so as to improve the effect, eradicate soil-borne diseases, The effect of reducing dosage
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Embodiment 1
[0020] Embodiment 1: 10% hymexazol·50 billion spores / gram Bacillus subtilis wettable powder
[0021]Get 50 kilograms of Bacillus subtilis former powder (100 billion spores / gram), 10.2 kilograms of 98% hymexazol former medicine, 3 kilograms of alkylnaphthalene sulfonate condensation polymer sodium salt, 2 kilograms of sodium isopropyl naphthalene sulfonate, 5 kg of magnesium aluminum silicate, 29.8 kg of diatomaceous earth, all the raw materials are mixed evenly, pulverized by a pulverizer and sieved. Promptly make 100 kilograms of 10% hymexazol·50 billion spores / gram Bacillus subtilis wettable powder like this, and this product is sepia powder.
[0022] Detection method of hymexazol content: high performance liquid chromatography. The sample was dissolved and diluted with methanol, methanol: 0.1% acetic acid aqueous solution (80:20) was used as the mobile phase, and the TC-C18 (2) stainless steel column was used as the packing stainless steel column and a variable wavelength ...
Embodiment 2
[0044] Example 2: 5% Hymexazol · 20 billion spores / gram Bacillus subtilis SC
[0045] Get 20 kg of Bacillus subtilis powder (100 billion spores / gram), 1 kg of alkyl naphthalene sulfonate, 2 kg of phenylethylphenol polyoxyethylene polyoxypropylene ether, 0.1 kg of xanthan gum, magnesium aluminum silicate 1 kg, 60 kg of water, after stirring evenly, enter the colloid mill and sand mill for grinding. When the fineness of the material reaches 1-5 microns, the material is transferred to the reaction kettle. Add 5 kg of hymexazol to the reaction kettle and stir for 30 minutes until the hymexazol is completely dissolved, then add 0.5 kg of 37% hydrochloric acid solution and stir for 10 minutes, and finally add water to make up to 100 kg. Promptly obtain 5% hymexazol · 20 billion spores / gram Bacillus subtilis aqueous suspension.
[0046] The assay method of active ingredient content in this water suspension concentrate is identical with the assay method among the embodiment 1. Afte...
Embodiment 3
[0047] Example 3: 10% Hymexazol · 60 billion spores / gram Bacillus subtilis WDG
[0048] Get 60 kilograms of the former powder of Bacillus subtilis (100 billion spores / gram), 10.2 kilograms of the former medicine of 98% hymexazol, 4 kilograms of alkylphenol polyoxyethylene ether formaldehyde condensate sulfate, 2 kilograms of alkylnaphthalene sulfonate kg, 2 kg of fatty alcohol polyoxyethylene ether, 3 kg of white carbon black, and 18 kg of kaolin were put into a mixer and fully mixed, and pulverized by a jet mill. In the kneader, 13 kg of water was uniformly added to the pulverized material for kneading, and then put into the granulator for extrusion granulation. Transfer the extruded wet granules to a fluidized bed for drying until the residual moisture content in the product is about 1%. Promptly make about 100 kilograms of 10% hymexazol·60 billion spores / gram Bacillus subtilis water-dispersible granule like this.
[0049] The assay method of the active ingredient content ...
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