Method for extracting lithium from bittern and preparing high-purity lithium concentrate
A high-purity lithium extraction technology, applied in the field of lithium extraction, can solve problems such as lithium ion sieves are easily broken, manganese cannot be recovered, and the operation efficiency of the adsorption bed is restricted, so as to reduce the dissolution loss of manganese, reduce the preparation cost, and accelerate crystallization Effects of speed and crystallographic integrity
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Embodiment 1
[0053] A certain brine contains lithium 0.3g / l, magnesium 100g / l, potassium 0.6g / l, sodium 1.3g / l, brine pH=5.0-5.3, add 10g / l magnetic manganese dioxide to the brine delivery pipeline Ion sieve, using sodium hydroxide to adjust the pH of the brine to ≥ 5.0, and then using a 1.25m diameter slurry electromagnetic machine for magnetic separation, the magnetic field strength is 1.3T, and the high gradient medium uses a diamond-shaped medium net. The above-mentioned magnetic separation equipment can realize the treatment capacity of 300 tons of brine per hour. The magnetic separation process integrates three process links: ion sieve capture, ion sieve cleaning in the magnetic field, and desorption solution elution outside the magnetic field. figure 1 , 2 shown.
[0054] The details are as follows: After magnetic separation, the non-magnetic liquid phase component is the brine after lithium extraction, which can be discharged directly; the magnetic part, that is, the magnetic ion...
Embodiment 2
[0055] Embodiment 2: Preparation of magnetic lithium ion sieve, as attached image 3 shown.
[0056] Prepare 1 ton of magnetic manganese dioxide ion sieve, add 0.5 g / l concentration of urea as a dispersion system, and add 0.17-0.18 t of ferrous chloride and 0.26-0.27 t of sulfurous acid at a molar ratio of 1:1.5 under the condition of 500 rpm stirring Iron solution, then slowly add 10% ammonia water 900-1000 L ammonia solution through a peristaltic pump until the solution pH=7.0, the black precipitate is ferroferric oxide magnetic core, and its average particle size is 20±3 nm. The above mixed solution is pumped into a φ300 mm slurry electromagnetic separator, which is filled with a stainless steel rhombic mesh as a high gradient medium. The magnetic component is ferroferric oxide magnetic core, which is washed by air-water mixed pulse, and the ferroferric oxide magnetic core is pumped into the silicon-coated mixing tank. The non-magnetic liquid phase component is unreacted a...
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