Adhesive and preparation method thereof
A technology of adhesives and additives, used in adhesives, inorganic adhesives, polymer adhesive additives, etc., can solve the problems of difficult to control the thickness of copper cladding, high sintering temperature, easy to shrink, etc. Strong force, high bending strength and repeatability
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Embodiment 1
[0039] An adhesive consisting of the following materials:
[0040] 90 parts by weight of alumina ceramic powder, 50 parts by weight of bisphenol A epoxy resin E-54, 2 parts by weight of polyethylene glycol 600, 2 parts by weight of polyoxypropylene oxide glyceryl ether, 1 part by weight of 2 -Methylimidazole, 5 parts by weight 1 μm CaCO 3 Powder, the acetone of 50 parts by weight.
[0041] To prepare the adhesive:
[0042] S1: Resin dissolution: Weigh 50 parts by weight of bisphenol A epoxy resin E-54, 5 parts by weight of 1 μm CaCO 3 The powder, 50 parts by weight of acetone, 2 parts by weight of polyethylene glycol 600 and 2 parts by weight of polyoxyethylene polyoxypropylene glyceryl ether are placed in a container, and the resin is stirred and dissolved to obtain a resin solution;
[0043] S2: Mixing: Weigh 90 parts by weight of alumina ceramic powder with an average particle size of 1 μm, and slowly add it to the resin solution described in step S1 under stirring condi...
Embodiment 2
[0049] An adhesive consisting of the following materials:
[0050] 70 parts by weight of alumina ceramic powder and 20 parts by weight of magnesium oxide ceramic powder, 50 parts by weight of glycidyl methacrylate, 2 parts by weight of polyethylene glycol 600, 2 parts by weight of glycerol polyether, 0.5 parts by weight Parts of cumene hydroperoxide, 5 parts by weight of CaO powder, 50 parts by weight of xylene.
[0051] To prepare the adhesive:
[0052]S1: Resin dissolution: Weigh 50 parts by weight of glycidyl methacrylate, 5 parts by weight of CaO powder, 50 parts by weight of xylene, 2 parts by weight of polyethylene glycol 600 and 2 parts by weight of glycerol polyether in a container In, stir and dissolve resin, obtain resin solution;
[0053] S2: Mixing: Weigh 70 parts by weight of alumina ceramic powder with an average particle size of 1 μm and 20 parts by weight of magnesium oxide ceramic powder with an average particle size of 1 μm, and slowly add them to the In t...
Embodiment 3
[0059] An adhesive consisting of the following materials:
[0060] 20 parts by weight of alumina ceramic powder and 10 parts by weight of magnesium oxide ceramic powder, 10 parts by weight of organosilicon-modified methyl methacrylate, 2 parts by weight of polyethylene glycol 600, 0.5 part by weight of polydimethyl base siloxane, 0.5 parts by weight of cumene hydroperoxide, 5 parts by weight of 1 μm SiO 2 Powder, the dehydrated alcohol of 10 weight parts.
[0061] To prepare the adhesive:
[0062] S1: Resin dissolution: Weigh 10 parts by weight of silicone-modified methyl methacrylate, 5 parts by weight of 1 μm SiO 2 The powder, 10 parts by weight of absolute ethanol, 2 parts by weight of polyethylene glycol 600 and 0.5 parts by weight of polydimethylsiloxane are placed in a container, and stirred to dissolve the resin to obtain a resin solution;
[0063] S2: Mixing: Weigh 20 parts by weight of alumina ceramic powder with an average particle size of 1 μm and 10 parts by wei...
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Abstract
Description
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Application Information

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