Method of preparing nano-silicon fungi type magnetic aerobic granular sludge and application
A technology of aerobic granular sludge and nano-silicon, which is applied in chemical instruments and methods, water/sludge/sewage treatment, water pollutants, etc. Inhomogeneity, long-term use performance of aerobic granular sludge needs to be discussed and other issues, to achieve the effect of avoiding core disintegration, small particle size and high utilization rate
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Embodiment 1
[0026] (1) Dissolve 0.02mol of ferric chloride and 0.01mol of ferric chloride as raw materials in 100ml of distilled water, stir for 1 hour under a nitrogen atmosphere, slowly add 10ml of concentrated ammonia water to adjust the pH value to 8.5-10, and cool to room temperature , after magnetic separation, repeated washing with distilled water to obtain ferric oxide nanospheres.
[0027] (2) Dilute 1g of iron ferric oxide nanospheres in a mixture of 20ml of distilled water, 60ml of absolute ethanol and 1.5ml of concentrated ammonia water, stir evenly, vibrate ultrasonically for 3 hours in a constant temperature water tank, and add 4.5-5ml dropwise Tetraethyl orthosilicate, continue magnetic stirring for 12 hours, use magnet to separate to obtain magnetic particles, wash the magnetic particles with absolute ethanol 3 times, dry and dry to obtain magnetic nanosphere ferric oxide / silicon dioxide.
[0028] (3) In the sequencing batch activated sludge reactor, the volume index SVI o...
Embodiment 2
[0032] (1) Dissolve 0.02mol of ferric chloride and 0.01mol of ferric chloride as raw materials in 100ml of distilled water, stir for 1 hour under a nitrogen atmosphere, slowly add 10ml of concentrated ammonia water to adjust the pH value to 8.5-10, and cool to room temperature , after magnetic separation, repeated washing with distilled water to obtain ferric oxide nanospheres.
[0033] (2) Dilute 1g of iron ferric oxide nanospheres in a mixture of 20ml of distilled water, 60ml of absolute ethanol and 1.5ml of concentrated ammonia water, stir evenly, vibrate ultrasonically for 3 hours in a constant temperature water tank, and add 4.5-5ml dropwise Tetraethyl orthosilicate, continue magnetic stirring for 12 hours, use magnet to separate to obtain magnetic particles, wash the magnetic particles with absolute ethanol 3 times, dry and dry to obtain magnetic nanosphere ferric oxide / silicon dioxide.
[0034] (3) In the sequencing batch activated sludge reactor, the volume index SVI of ...
Embodiment 3
[0038] (1) Dissolve 0.02mol of ferric chloride and 0.01mol of ferric chloride as raw materials in 100ml of distilled water, stir for 1 hour under a nitrogen atmosphere, slowly add 10ml of concentrated ammonia water to adjust the pH value to 8.5-10, and cool to room temperature , after magnetic separation, repeated washing with distilled water to obtain ferric oxide nanospheres.
[0039] (2) Dilute 1g of iron ferric oxide nanospheres in a mixture of 20ml of distilled water, 60ml of absolute ethanol and 1.5ml of concentrated ammonia water, stir evenly, vibrate ultrasonically for 3 hours in a constant temperature water tank, and add 4.5-5ml dropwise Tetraethyl orthosilicate, continue magnetic stirring for 12 hours, use magnet to separate to obtain magnetic particles, wash the magnetic particles with absolute ethanol 3 times, dry and dry to obtain magnetic nanosphere ferric oxide / silicon dioxide.
[0040] (3) In the sequencing batch activated sludge reactor, the volume index SVI o...
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