Kit for accurately and quantitatively detecting vibrio vulnificus in food and detection method
A technology of vibrio vulnificus and kit, which is applied in the kit and detection field of quantitative detection of vibrio vulnificus, which can solve the problems of quantitative detection of vibrio vulnificus that have not been seen yet, and achieve shortened detection time, high tolerance and high accuracy degree and repeatability of the effect
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Embodiment 1
[0050] Embodiment 1 ddPCR primer, probe design
[0051] In order to achieve the specific detection and absolute quantitative analysis of Vibrio vulnificus in food, we selected the species-specific and highly conserved single-copy lipoprotein D gene (nplD, GenBank no.AY187681.1), RNA Polymerase subunit sigma factor S gene (rpoS, GenBank no.AY187681.1), virulence-related gene E (vcgE, GenBank no.AY626581.1) and metalloproteinase gene (met, GenBank no.U50548.1) as targets Sequences were analyzed and compared using NCBI online tools, and 4 pairs of primers and probe combinations were designed using Prime Express software V3.0 (ABI, Foster City, CA, USA). There are 4 sets of primer / probe combinations for ddPCR amplification conditions, and the sequences are shown in Table 1. Primers and probes were synthesized by Beijing Liuhetong Economic and Trade Co., Ltd. The primer / probe positions refer to GenBank no. AY187681.1 (nplD, rpoS gene), AY626581.1 (vcgE gene) and U50548.1 (met gen...
Embodiment 2
[0052] Example 2 Screening and specificity verification of primers and probes
[0053] Firstly, the designed and synthesized primers and probes were screened by qPCR method. Through the detection of the genomic DNA of Vibrio vulnificus (ATCC27562), it was found that all the primer probes could effectively amplify the target gene, but the fluorescent signal of the primer probe group met-F / R / P appeared earliest, which was compared with the negative control ratio, the fluorescence signal intensity is the largest, so the amplification effect is the best ( figure 1 A).
[0054] Next, in order to verify the specificity of the amplification reaction, the met-F / R / P primer probe was selected by qPCR method to detect the DNA of common Vibrio and food-borne pathogenic bacteria listed in Table 4. A total of 107 strains were used in this experiment (Table 4), including 1 standard strain of Vibrio vulnificus, 20 self-isolated strains, 66 other Vibrio standard / reference / self-isolated strai...
Embodiment 3
[0062] Embodiment 3 kit composition
[0063] The kit includes primers and probes for detecting Vibrio vulnificus designed in Example 1, a positive control (Vibrio vulnificus ATCC 27562 genomic DNA, 1000 copies / μL), a negative control (Escherichia coli ATCC 25922 genomic DNA, 1000 copies / μL), ddPCR master mix (purchased from BioRad, USA), microdroplet generation oil (purchased from BioRad, USA), microdroplet generation card (purchased from BioRad, USA), Twin Tec Semi-Skirted 96-well plate ( purchased from Eppendorf, Germany), and aluminum foil heat-sealing film (purchased from BioRad, USA).
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