Preparation method of phase-change solar heat-absorption coating with high heat absorption rate
A technology of solar heat absorption and absorption rate, applied in the direction of radiation-absorbing coatings, heat exchange materials, chemical instruments and methods, etc., can solve the problems of low light absorption capacity, low energy storage efficiency, low heat absorption efficiency, etc., to achieve Improved thermal conductivity, reduced heat loss, and increased specific surface area
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[0024]Put 12-15g of p-nitroaniline into a beaker, add 35-40mL of hydrochloric acid with a mass fraction of 20%, heat up to 70-80°C, keep stirring until the solids are completely dissolved, and then place the beaker in an ice bath Rapidly cool to 0-5°C, stir at a speed of 300-400r / min and add 40-50mL sodium nitrite aqueous solution with a mass fraction of 5%, react for 30-35min, then add 4-5g sulfamic acid into the beaker , suction filtration, and separation to obtain the filtrate, which is p-nitroaniline diazonium salt solution; take 10-12g of single-walled carbon nanotubes and place them in a three-necked flask, add 200-300mL of deionized water, and place the three-necked flask in an ultrasonic disperser At a temperature of 50-55°C, ultrasonically disperse at a frequency of 25-30kHz for 30-35min, and drop 40-50mL of p-nitroaniline diazo Saline solution, react while adding dropwise, until the dropwise addition is complete, filter the reaction solution in the three-necked flask...
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