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Iron-based oil-containing bearing material of controllable pore structure and preparation method of iron-based oil-containing bearing material

A bearing material and pore structure technology, which is applied in the field of bearing materials, can solve the problems of lack of communication with the outside world, the decline of the oil storage capacity of the material, the influence of the iron matrix, etc., so as to improve the mechanical properties, enhance the oil storage performance, and improve the connectivity.

Active Publication Date: 2019-05-07
HEFEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the preparation of iron-based oil-impregnated bearings, pore-forming agents such as ammonium bicarbonate, urea, and stearic acid are added to the raw material powder in advance in the industry, but these pore-forming agents are easy to decompose or gasify at relatively low temperatures. It is difficult to control the production management. The formed pores are easy to close during the long sintering process in the later stage, forming closed pores that are not connected to the outside world, resulting in the effective porosity not reaching the standard and the oil storage capacity of the material is reduced.
At the same time, when the urea decomposition product HCNO, which is corrosive to the iron base, is discharged through the iron base, it will affect the iron base, thereby affecting the performance and application of the material.

Method used

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  • Iron-based oil-containing bearing material of controllable pore structure and preparation method of iron-based oil-containing bearing material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] The operation steps of preparing the iron-based oil bearing material with controllable pore structure are as follows:

[0031] Step 1. According to the mass percentage, weigh 116.58g (97.15%) of iron powder, titanium hydride powder (TiH 2 ) 2.4g (2%), graphite powder 0.78g (0.65%), hair strands 0.24g (0.2%), a total of 120g; plus zinc stearate 0.6g (0.5% of the total mass).

[0032] Step 2. Add the above mixed powder into the grinding tank for ball milling. In the tank, there are 250g of large balls and 350g of small balls. Vacuumize, fill with high-purity argon, rotate at a speed of 300r / min, mill for 10 hours, and stop for 15 minutes every 60 minutes of ball milling to facilitate heat dissipation during ball milling. , after the ball milling, it was naturally cooled for 5 hours, and a uniformly mixed powder was obtained.

[0033] Step 3. Put the above-mentioned powder into a pressing mold, and make a green body under unidirectional pressure. The pressure for pressing...

Embodiment 2

[0038] The operation steps for preparing the iron-based oil-impregnated bearing material are as follows:

[0039] 1. According to the mass percentage, weigh 116.58g (97.15%) of iron powder, titanium hydride powder (TiH 2 ) 2.4g (2%), graphite powder 0.78g (0.65%), hair strands 0.24g (0.2%), a total of 120g; plus zinc stearate 0.6g (0.5% of the total mass);

[0040] 2. Same as Step 2 of Example 1;

[0041] 3. Same as Step 3 of Example 1;

[0042] 4. Same as Step 4 of Example 1;

[0043] 5. Put the sintered material into the ordinary oil and vacuum immerse it in oil. The amount of oil is more than the amount of immersion sample, the oil immersion time is 3 hours, the vacuum pressure value is not more than 7KPa, and the oil temperature is 70℃~100℃;

[0044] 6. The test samples were tested for mechanical properties and friction and wear performance under dry friction conditions. The prepared oil-containing iron base has a hardness of 59HRB, an oil content of 16.13%, and a den...

Embodiment 3

[0046] The operation steps for preparing the iron-based oil-impregnated bearing material are as follows:

[0047] 1. According to the mass percentage, weigh 116.58g (97.15%) of iron powder, titanium hydride powder (TiH 2 ) 2.4g (2%), graphite powder 0.78g (0.65%), hair strands 0.24g (0.2%), a total of 120g; plus zinc stearate 0.6g (0.5% of the total mass)

[0048] 2. Put the above powder into the pressing mold, and make a green body under unidirectional pressure. The pressure of pressing the green body is 650~750MPa.

[0049] 3. Put the pressed billet into the mesh belt sintering furnace, pass through the decomposed ammonia gas for protection, the sintering temperature is 1050~1200 ℃, and the holding time is 4 h.

[0050]4. Put the sintered material into the ordinary oil and vacuum immerse it in oil. The amount of oil is more than the amount of immersion sample, the oil immersion time is 3 hours, the vacuum pressure value is not more than 7KPa, and the oil temperature is 70℃...

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Abstract

The invention relates to an iron-based oil-containing bearing material of a controllable pore structure and a preparation method of the iron-based oil-containing bearing material. Hair and titanium hydride powder are mixed as a composite pore forming agent to be placed in an iron matrix blank. According to the bearing material, in the friction and wear process, oil in pores flows to the surface toform a lubricating oil film, friction is reduced, meanwhile, micro grooves in the surface of a friction pair can be filled with C60 nanoparticles in the oil so as to reduce roughness, and the effectof reducing friction is achieved. The ball grinding process is adopted, the composite pore forming agent and iron powder are mechanically alloyed, the shape of the pore forming agent is regular, the shape of the pore forming agent has geometric heritability to the pore forms, and therefore generated pores are regular in size and are evenly distributed in an iron matrix. The blank is placed in inert gas to be sintered, titanium hydride is subjected to dehydrogenation at high temperature in the sintering process, open pores are formed in the iron matrix, the hair is decomposed at high temperature, a large number of micron-order bridge pore channels are formed to penetrate through the open pores formed by titanium hydride, and connectivity of the pores is improved.

Description

technical field [0001] The invention belongs to the technical field of bearing materials, and in particular relates to an iron-based oil-containing bearing material with a controllable pore structure and a preparation method thereof. Background technique [0002] With the development of modern spaceflight and aviation industry, the tribology of space machinery has developed rapidly. The iron-based self-lubricating iron-based material with low friction coefficient has inherent advantages due to its simplified mechanical structure design, and has become a friction material. It is a hotspot in the field of scientific research and has been successfully applied to miniature iron-based bearings used in outer space. The pore volume in the bearing is about 10% -40%. This pore volume can be used to store fluid lubricant and supply oil under self-propelled state to improve the lubrication condition. [0003] In the preparation of iron-based oil-impregnated bearings, pore-forming agen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F5/10B22F3/11B22F3/26C22C38/14
Inventor 尹延国李蓉蓉张开源张国涛
Owner HEFEI UNIV OF TECH
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