A kind of production process of glycerol fructose sodium chloride injection
A technology of sodium chloride injection and production process, which is applied in the direction of blood diseases, extracellular fluid diseases, active ingredients of hydroxyl compounds, etc. Problems such as slow heat conduction can reduce the probability of bursting bottles (bags), improve production safety, and speed up preheating
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specific Embodiment approach
[0036] As a specific embodiment of the present invention, the prescription feeding of glycerin fructose injection comprises by weight:
[0037] Glycerin 9-11 parts
[0038] 4-6 servings of fructose
[0039] Sodium chloride 1-3 parts
[0040] 1-3 parts of pH regulator
[0041] 78-82 parts of water for injection.
[0042] As a specific embodiment of the present invention, the preparation temperature in S2 is 10-30°C, the pH regulator in S3 is hydrochloric acid or sodium hydroxide, and micropores below 0.22um are used for filtration in S4, and fructose is filtered at high temperature. Or generate this impurity of 5-hydroxymethylfurfural under weak acid condition, the present invention adopts preparation temperature control, pH adjuster selection and microporous filtration, controls fructose to the intermediate product of 5-hydroxymethylfurfural conversion process, thereby effectively reduces 5-hydroxymethylfurfural HMF content.
[0043] As a specific embodiment of the presen...
Embodiment 1
[0049] A kind of glycerin fructose sodium chloride injection production technology, comprises the following steps:
[0050] S1: Add 70% water for injection into the preparation container, control the temperature at 60°C, add the prescribed amount of sodium chloride and glycerin, stir for 12 minutes to dissolve the sodium chloride and glycerin, and obtain the medicinal solution 1;
[0051] S2: Lower the preparation temperature of S1 Chinese medicinal solution 1 to 15°C, add the prescribed amount of fructose, stir for 8 minutes to dissolve the fructose, and set the volume to the prepared amount to obtain medicinal solution 2. Prepare medicinal liquid 1 and medicinal liquid 2 Inert gas protection is used in the process;
[0052] S3: After circulating the second medicinal solution in S2 for 15 minutes, use a pH regulator to adjust the second medicinal solution so that the pH value of the second medicinal solution is 4.0, and obtain the finished injection. Sampling and characterizi...
Embodiment 2
[0055] A kind of glycerin fructose sodium chloride injection production technology, comprises the following steps:
[0056]S1: Add 70% water for injection into the preparation container, control the temperature at 60°C, add the prescribed amount of sodium chloride and glycerin, stir for 12 minutes to dissolve the sodium chloride and glycerin, and obtain the medicinal solution 1;
[0057] S2: Lower the preparation temperature of S1 Chinese medicinal solution 1 to 40°C, add the prescribed amount of fructose, stir for 8 minutes to dissolve the fructose, and set the volume to the prepared amount to obtain medicinal solution 2. Prepare medicinal liquid 1 and medicinal liquid 2 Inert gas protection is used in the process;
[0058] S3: After circulating the second medicinal solution in S2 for 15 minutes, use a pH regulator to adjust the second medicinal solution so that the pH value of the second medicinal solution is 4.0, and obtain the finished injection. Sampling and characterizin...
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