Electromagnetic shielding flame-retardant material for carbon fiber base material as well as preparation method and application thereof
A carbon fiber base material and electromagnetic shielding technology, applied in conductive coatings, fireproof coatings, coatings, etc., can solve problems such as transmission loss, shield surface reflection loss, absorption loss, etc., to avoid metal carbonization, improve application performance, and improve Effect of Environmental Resistance
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Embodiment 1
[0089] Add toluene, melamine-coated modified ammonium polyphosphate (APP) (Sichuan Shifang Changfeng Chemical Co., Ltd.), neopentyl glycol phosphorus oxychloride (DPPC) into the reaction kettle at 10°C (refer to literature for synthesis, for example, Zhao Xiaotao , Zhao Wuli, Li Zuguang, microwave synthesis of neopentyl glycol phosphorus oxychloride, "Guangdong Chemical Industry", 2012), mechanically stirred and mixed uniformly, acid-binding agent triethylamine was added dropwise within 2h, and the reaction was continued for 4h after dropping; the temperature was raised to 60°C, add melamine aqueous solution within 3 hours, and react for 6 hours after dripping; then raise the temperature to 110°C, add melamine aqueous solution again within 3 hours, and react for 8 hours after dripping; after the reaction is completed, the mixture is concentrated, filtered, washed, and dried , A phosphorus-nitrogen one-component intumescent flame retardant with a three-dimensional macromolecular...
Embodiment 2
[0091] In the reaction vessel, add 200 grams of ethanol, 50 grams of silver-coated copper powder, and then dropwise add 0.4 grams of γ-glycidyl etheroxypropyltrimethoxysilane and 0.2 vinyltriethoxysilane, and stir and reflux at 78°C 3 hours, then filtered, washed the solid 3 times with absolute ethanol, and dried in vacuo to obtain silver-coated copper powder after the surface treatment of the coupling agent.
Embodiment 3
[0093] In the reaction vessel, add 200 grams of ethanol, 60 grams of nickel-coated copper powder, and then dropwise add 0.5 grams of isopropyl tris(dioctyl pyrophosphate acyloxy) titanate, 0.5 grams of γ-glycidyl ether oxypropyl base triethoxysilane, stirred and refluxed at 78°C for 3 hours, then filtered, washed the solid three times with absolute ethanol, and dried in vacuo to obtain nickel-coated copper powder after the surface treatment of the coupling agent.
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