Rolling-resistant semi-rigid base internal curing water retention material and preparation method thereof
A technology of semi-rigid base layer and water-retaining material, which is applied in the field of road materials, can solve the problems of weakening the performance of semi-rigid base layer, internal curing material maintenance efficiency, premature release of internal moisture, low strength, etc., so as to enhance rigidity, ensure water demand, Chemically stable effect
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[0047] A method for preparing an internal health-preserving and water-retaining material for a rolling-resistant semi-rigid base, comprising the following steps:
[0048] Step 1: Weigh silica airgel powder, glass powder, and nano-silicon nitride by mass, and mix them uniformly for later use;
[0049] Step 2: hydrolyze the silane coupling agent Si-602 under the action of acetic acid, add a certain amount of mixed solution of absolute ethanol and deionized water, wherein, m 无水乙醇和去离子水 :m 硅烷偶联剂Si-602 = 16:1, v 去离子水 : v 无水乙醇 =7:3, forming silane coupling agent Si-602 hydrolyzate;
[0050] Step 3: Evenly disperse the evenly mixed silica airgel powder, glass powder, and nano-silicon nitride in the hydrolyzate of the silane coupling agent Si-602 in step 2, stir with argon gas, and then let stand Until the layers are separated, the supernatant liquid is poured off, and the remaining mixture is dried to obtain modified silica airgel powder, glass powder, and nano-silicon nitride, wh...
Embodiment 1
[0062] This example provides a preparation method for an internal health-preserving and water-retaining material of a rolling-resistant semi-rigid base, which consists of the following raw materials by weight:
[0063] 10% silica airgel powder, 3% glass powder, 5% nano silicon nitride, 2% silane coupling agent Si-602, 1% acetic acid, 27% methacrylic acid, 7% oil phase material, 3% Carrageenan, 16% polyaspartic acid, 20% succinimide, 0.1% 1,4 butanediol diacrylate, 0.2% azobisisobutyronitrile, 0.3% cerium ammonium nitrate, 5.6% sodium ethoxide .
[0064] Wherein, in the oil phase material, Span 80 is 4% of the mass fraction of diethyl phthalate.
[0065] In particular, absolute ethanol, deionized water, and isopropanol are used as solvents, used to prepare solutions or wash raw materials, and do not participate in chemical reactions.
[0066] The preparation method of the internal health and water retention material of the above-mentioned rolling-resistant semi-rigid base com...
Embodiment 2
[0078] This example provides a preparation method for an internal health-preserving and water-retaining material of a rolling-resistant semi-rigid base, which consists of the following raw materials by weight:
[0079] 10% silica airgel powder, 3% glass powder, 8% nano silicon nitride, 3% silane coupling agent Si-602, 1.5% acetic acid, 25% methacrylic acid, 8% oil phase material, 3% Carrageenan, 14% polyaspartic acid, 18.82% succinimide, 0.18% 1,4 butanediol diacrylate, 0.2% azobisisobutyronitrile, 0.3% cerium ammonium nitrate, 5% sodium ethoxide .
[0080]In particular, the oil phase material is Span 80 and diethyl phthalate, and Span 80 is 6% of the mass fraction of diethyl phthalate.
[0081] In particular, absolute ethanol, deionized water, and isopropanol are used as solvents, used to prepare solutions or wash raw materials, and do not participate in chemical reactions.
[0082] The preparation method of the internal health and water retention material of the above-ment...
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