Method for preparing coal ash ceramic water washing ball

A technology of fly ash and ceramics, which is applied in the field of preparation of fly ash ceramic washing balls, which can solve the problems of poor color effect of clothing materials, troublesome use and environmental protection, high production cost, etc., achieve strong three-dimensional effect, low production cost, and improve efficacy Effect

Inactive Publication Date: 2011-05-04
SHANDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The plastic hollow rinse ball involved in the Chinese patent ZL89108618 is not easy to wear, but the preparation cost is high, the process is complicated, and the color effect of the cloth after grinding and washing is poor;
[0004] Chinese patent ZL92100090.1 relates to a synthetic zeolite rinse ball, which uses cement hydration to bond zeolite particles, zeolite powder and expanded perlite. It needs to be soaked with potassium permanganate or oxalic acid before use, which brings many troubles to use and environmental protection;
[0005] Chinese patent ZL92104698.7 relates to a synthetic washing ball, the preparation method is to mix zeolite slag or zeolite powder with quicklime, cement, gypsum and aluminum powder The air agent and the acacia powder degreasing agent are placed together in a high-speed mixer, stirred and mixed to generate gas, and then sent to the autoclave for constant temperature maintenance. This method has complex processes and high costs;
The disadvantage is that the texture is soft and the cost is high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] (1) Ingredients: Mix 78wt% of glass powder with a particle size of 50 μm, 12wt% of fly ash, 5wt% of flux and 5wt% of foaming agent, and mix and grind in a ball mill with a material: ball ratio of 1:1 Form the fly ash porous ceramic powder in 3 hours, wherein the composition and proportioning of fluxing agent are: sodium fluorosilicate 30wt%, sodium silicate 20wt%, borax 50wt%, foaming agent adopts charcoal powder and light calcium carbonate Mixture, its weight ratio is 1:10;

[0024] (2) Molding: adopt water-added dry pressing molding, add the water of 10wt% of fly ash porous ceramic powder amount, after uniform mixing, molding is made into ceramic water-washing ball green body;

[0025] (3) Firing: The dried green body is fired at 950°C for 1 hour to obtain fly ash ceramic water-washed balls.

[0026] The purity of the batching raw materials used in the experiment is industrial pure.

[0027] After inspection, the technical indicators of the prepared product are: the...

Embodiment 2

[0029] (1) Ingredients: mix 45wt% of glass powder with a particle size of 100 μm, 25wt% of fly ash, 10wt% of flux and 20wt% of foaming agent, and mix and grind in a ball mill with a material: ball ratio of 1:1 Fly ash porous ceramic powder is formed in 1 hour, wherein the composition and proportioning of fluxing agent are: sodium fluorosilicate 10wt%, sodium silicate 30wt%, borax 60wt%, foaming agent adopts charcoal powder and light calcium carbonate Mixture, its weight ratio is 1:5;

[0030] (2) Forming: the fly ash porous ceramic powder plus 20wt% water of the fly ash porous ceramic powder is mixed in a mud mill to form plastic mud and extruded mud sticks, and then cut into columnar water-washed ball green bodies;

[0031] (3) Firing: put the dried body at 1050°C and fire for 0.5 hour to obtain the fly ash ceramic water-washed ball.

[0032] The purity of the batching raw materials used in the experiment is industrial pure.

[0033] After inspection, the technical indicato...

Embodiment 3

[0035] (1) Ingredients: mix 86wt% of glass powder with a particle size of 5 μm, 5wt% of fly ash, 5wt% of flux and 4wt% of foaming agent, and mix and grind in a ball mill with a material: ball ratio of 1:1 Fly ash porous ceramic powder is formed in 2 hours, wherein the composition and proportioning of the fluxing agent are: 20wt% sodium fluorosilicate, 50wt% sodium silicate, 30wt% borax, and the blowing agent is a mixture of charcoal powder and magnesium carbonate. Its weight ratio is 1:3;

[0036] (2) Forming: the fly ash porous ceramic powder plus 15wt% water of the fly ash porous ceramic powder is mixed in a mud mill to form plastic mud and extruded mud sticks, and hand-made fly ash of different diameters Ceramic water washing ball green body;

[0037] (3) Firing: The dried green body is fired at 780°C for 2 hours to obtain fly ash ceramic water-washed balls.

[0038] The purity of the batching raw materials used in the experiment is industrial pure.

[0039] After inspec...

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Abstract

The present invention provides a method which is used for preparing a flyash ceramic flush sphere and comprises the procedures of batching, molding and baking, and the method has the following characters: 25-97% powdered glass with granularity 1 mu m to 100 mu m, 1-30wt% flyash, 1-15wt% fluxing agent and 1-30wt% foaming agent is mixed according to the proportion and is grinded to prepare the homogeneous flyash porous ceramic powder, then the flyash porous ceramic powder is prepared to flush sphere base substrate, the base substrate is baked for 0.5-2 hours at the temperature 600-1100 DEG C after drying, and the flyash ceramic flush sphere is prepared. The technique of the invention is simple, as the powered glass adopted by the raw material can be domestic waste glass powder or glass fiber industrial waste, the flyash is also industrial waste, the cost is reduced by waste utilization, the natural zeolite waste is reduced by 20-30 times and the pollution is reduced, the inside and outside arrangement of the pore diameter of the produced flyash ceramic flush sphere is uniform and the wear-resisting property is 10-20 times of the common ceramic flush sphere, the cubic effect of the washed cloth decorative pattern is excellent, the appearance is beautiful and the property is excellent.

Description

Technical field [0001] The invention relates to a method for preparing fly ash ceramic water washing balls, belonging to the technical field of porous ceramic preparation technology. Background technique [0002] Washing balls are mainly used in the garment industry for grinding, washing and rinsing of materials and garments, such as denim fabrics, washed fabrics and their garments. At present, natural zeolite is mainly used, but because natural zeolite is soft and consumes a lot, it needs to be stopped at any time to replenish during use, which seriously affects the efficacy, and the zeolite waste residue is difficult to recycle, which is easy to cause environmental pollution. In response to the above problems, there have been technical reports on washing balls made of other materials, such as: [0003] The plastic hollow rinsing ball involved in the Chinese patent ZL89108618 patent is not easy to wear, but the preparation cost is high, the process is complicated, and the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B38/02C04B38/08C04B35/14
Inventor 唐竹兴
Owner SHANDONG UNIV OF TECH
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