Composite material using nano inorganic powder as surface with autocatalytic activity and preparation method thereof
A nano-inorganic, active surface technology, used in catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc. Process flow, saving precious metals, reducing the effect of environmental pollution
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Embodiment 1
[0018] After the poly-p-phenylenebenzobisoxazole (PBO) fiber is repeatedly washed with ethanol and distilled water, it is immersed in a modified solution prepared by polyphosphoric acid and absolute ethanol at a volume ratio of 1:1 to 3 for 1 to 60 minutes, and then Wash repeatedly with distilled water.
[0019] Disperse 1-3g of nano-titanium dioxide powder in 50-500mL of distilled water, add 0.01-0.5g of sodium polyphosphate and 0.01-0.3g of sodium dodecylbenzenesulfonate as a dispersant, and adjust the pH to 7 with ammonia water ~12, ultrasonic vibration for 20~120min to prepare uniformly dispersed nano-titanium dioxide powder emulsion. The nano-titanium dioxide powder emulsion is placed in a constant temperature water bath, and the temperature is gradually raised to 50-100°C. Adjust the pH value to 2-6 with hydrochloric acid, then add 1-10 mL of silane coupling agent dropwise, and stir vigorously for 20-120 minutes.
[0020] Take 0.5-2.5g of the above-mentioned modified n...
Embodiment 2
[0024] Polyester fabric at 20~60g·L -1 After being treated in sodium hydroxide solution at 50-100°C for 10-60 minutes, wash repeatedly with distilled water.
[0025] Take 1-4g of nano-zinc oxide powder, dilute with 50-95% ethanol solution, and ultrasonically vibrate for 20-90 minutes to prepare uniformly dispersed nano-zinc oxide powder emulsion. The nano-zinc oxide powder emulsion is placed in a constant temperature water bath, and the temperature is gradually raised to 50-100° C., then 1-10 mL of titanate coupling agent is added dropwise, and vigorously stirred for 20-120 min.
[0026] Take 0.5-2.5g of the above-mentioned modified nano-zinc oxide powder and place it in 100-300mL of isopropanol solution, control the temperature at 50-100°C, and ultrasonically disperse for 20-90min to prepare a uniformly dispersed emulsion. Soak the modified polyester fabric in the emulsion, add 0.1-5mL titanate coupling agent dropwise into the emulsion, continue ultrasonic oscillation for 30...
Embodiment 3
[0030] Polypropylene plastic matrix at 20-50mL·L -1 Turpentine and 30~60mL·L -1 In a solution composed of non-ionic surfactants, treat at 50-90°C for 10-50 minutes, then in 250-400g·L -1 Chromic anhydride and 150~400g·L -1 Treat in a solution composed of sulfuric acid at 50-90°C for 10-50 minutes, and then wash repeatedly with distilled water.
[0031]Take 2-3g of nano tin oxide powder and disperse it in 50-400mL of deionized water, add 1-5g of sodium oleate as a dispersant at the same time, adjust the pH value to 7-12 with ammonia water, and oscillate ultrasonically for 20-100min to prepare evenly dispersed Nano tin oxide powder emulsion. The nano-tin oxide powder emulsion is placed in a constant temperature water bath, and the temperature is gradually raised to 50-100°C. Adjust the pH value to 2-6 with hydrochloric acid, then add 1-10 mL of silane coupling agent dropwise, and stir vigorously for 20-120 minutes.
[0032] Take 0.5-2.5g of the above-mentioned modified nano...
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