Method for preparing hydroxyapatite/nano silver antimicrobial composite coating by pulse electrochemical deposition
A hydroxyapatite and nano-silver antibacterial technology, which is applied in the field of surface modification of medical biomaterials, can solve problems such as uneven distribution of silver and large particle size of silver particles
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Embodiment 1
[0027] (1) Take the titanium plate as the working electrode, and then acid and alkali surface treatment after conventional acetone ultrasonication.
[0028] (2) Dissolve 0.5g of silver nitrate in an appropriate amount of distilled water, and then slowly add 0.2g of cysteine;
[0029] (3) Take 0.394g of calcium nitrate tetrahydrate and 0.115g of ammonium dihydrogen phosphate, dissolve and mix them with distilled water, then slowly add (2) into it to prepare an electrolyte solution with a total volume of 1000ml of pH=4.0, and place the beaker Stir on a magnetic stirrer to obtain a uniform electrolyte;
[0030] (4) With the uniform electrolyte in (3), the saturated calomel electrode is used as the reference electrode, the platinum sheet is used as the counter electrode, and the biomedical metal to be coated is used as the working electrode. deposition. The relevant parameters are: pulse high potential: 0V, pulse low potential: -2.0V, pulse width: 100s, deposition time: 2h.
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Embodiment 2
[0051] The ammonium dihydrogen phosphate of embodiment 1 is changed into the NaH of equimolar concentration 2 PO 4 , for electrochemical deposition, other conditions remain unchanged.
Embodiment 3
[0053] The ammonium dihydrogen phosphate of embodiment 1 is changed into the KH of equimolar concentration 2 PO 4 , for electrochemical deposition, other conditions remain unchanged.
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