The invention discloses an optimization method of a synchronous ultrasonic field
low oxygen evolution
overpotential zinc electrodeposition process. The method comprises the steps that a Pb-
Ag alloy serves as an
electrode, and a
zinc electrodeposition electrolytic bath and an LSV testing electrolytic bath are built respectively; respectively electrifying the
zinc electrodeposition electrolytic bath and the LSV test electrolytic bath for
electrolysis, and applying a synchronous ultrasonic field to obtain an
anode LSV curve; after
electrolysis is finished, the
anode is recycled, an electrodeposition oxidation layer film of the recycled
anode is reserved, and an LSV curve of the electrodeposition oxidation layer film is obtained again; and repeating the steps to perform single-factor variable optimization on the zinc electrodeposition process parameters to obtain the optimal
process conditions. According to the method, through a single-factor control experiment on variable factors in the zinc electrodeposition process, a correlation relation between each variable factor and an optimization effect is established by utilizing
oxygen evolution
overpotential and the
ion concentration of an electrodeposition
electrolyte, so that the optimal process condition is obtained in a targeted manner; the problems that in the prior art, in the zinc electrodeposition process of an anode, the
oxygen evolution
overpotential of the anode is high, the
corrosion rate of lead and silver is high, and the zinc electrodeposition cost is increased are effectively solved.