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227results about How to "Reduce ion concentration" patented technology

Process and equipment for rejuvenation treatment of photoresist development waste

The disclosed process for rejuvenation treatment of a photoresist development waste mainly containing a photoresist and tetraalkylammonium (TAA) ions comprises at least a simple membrane separation step of treating the photoresist development waste or a treated solution derived from the photoresist development waste with a nanofiltration membrane (NF membrane) to obtain a concentrate (NF concentrate) mainly containing impurities such as the photoresist and a higher-purity permeate (NF permeate) mainly containing TAA ions. The NF concentrate and/or the NF permeate, preferably the NF permeate, is desirably subjected to a step of concentration and refining by electrodialysis or electrolysis and/or a step of refining by ion exchange treatment, for example, with an anion exchange resin and/or a cation exchange resin in one of the H form and the TAA form. The NF permeate may advantageously be passed through the concentrating cells of an electrodialysis unit while passing the NF concentrate through the desalting cells of the electrodialysis unit to further recover TAA ions remaining in the NF concentrate, whereby the amount of wastewater discharged as the desalted waste can be decreased. The NF membrane separation step is preferably effected in multiple stages.
Owner:ORGANO CORP

Hexagonal boron-nitride material, preparation method and application of hexagonal boron-nitride material

The invention provides a hexagonal boron-nitride material, a preparation method and application of hexagonal boron-nitride material. The hexagonal boron-nitride material is of an assembling structure consisting of porous boron-nitride whiskers and porous boron-nitride piece layers, or a porous boron-nitride whisker structure distributed with mesopores and macropores and with the specific surface area reaching 420m<2>/g. The preparation method comprises the following steps: (1) adding boric acid, melamine and optional surface active agent into water, mixing, heating, adjusting pH value of solution to be 3-11, crystallizing, and separating solid and liquid to obtain precursor; and (2) carrying out two-section type calcining reduction on the precursor in the step (1) under the atmosphere of ammonia gas or the mixed atmosphere containing the ammonia gas to obtain the hexagonal boron-nitride material. The hexagonal boron-nitride material can be used as an absorbing agent for absorbing metal ions and/or organic matters. The invention also provides a cyclic regeneration method of the hexagonal boron-nitride material. The hexagonal boron-nitride material is an excellent absorbing agent, is excellent in absorbing performance and cyclic regeneration performance, and has good application prospect in the field of water treatment.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Medical wastewater three-stage treatment technique

The invention relates to the field of medical wastewater treatment, particularly a medical wastewater three-stage treatment technique which comprises the following steps: a primary macroscopic impurity removal technique is performed, wherein the primary macroscopic impurity removal technique comprises sedimentation tank treatment, precipitation tank treatment and regulating tank treatment, and is used for macroscopic impurity removal; medical wastewater after the primary macroscopic impurity removal technique enters a secondary microscopic impurity removal technique, wherein the secondary microscopic impurity removal technique comprises water softener tank treatment, hydrolysis-acidification tank treatment, aeration biological tank treatment, electrolysis cell treatment and MBR (membrane bioreactor) tank treatment, and is used for microscopic impurity removal; and medical wastewater after the secondary microscopic impurity removal technique enters a tertiary disinfection discharge technique, wherein the tertiary disinfection discharge technique comprises secondary sedimentation tank treatment, disinfection tank treatment and discharge, and is mainly used for sterilizing and disinfecting the wastewater. The technique can remove different pollutants in the medical wastewater by using different treatment processes, and can implement efficient purification on the medical wastewater.
Owner:ZONBONG LANDSCAPE

Method for synthesizing super absorbent resin containing phosphorus and nitrogen by graft copolymerization reaction of potato starch organic phosphate

The invention discloses a method for synthesizing super absorbent resin containing phosphorus and nitrogen by the graft copolymerization reaction of potato starch organic phosphate, which comprises the following main processes: carrying out neutralization reaction between a sodium hydroxide solution and acrylic acid from which polymerization inhibitor is removed under the cooling of ice-water bath; respectively mixing potato starch organic phosphate and acrylamide with de-ionized water to obtain a potato starch organic phosphate solution and an acrylamide solution; mixing the prepared acrylicacid and the sodium salt solution with the potato starch organic phosphate solution and the acrylamide solution; adding an evocating agent persulfate; stirring the mixture for 0.5-1.0 hour to ensure that the mixture is uniformly mixed; heating the mixture by water bath and stirring under the protection of nitrogen; stopping stirring when reaching certain temperature; keeping the temperature for 1-2 hours in boiling water bath; stopping supplying nitrogen, taking the product out, and cutting the product into small pieces; drying the small pieces in a baking oven to keep constant weight, and crashing to obtain the super absorbent resin containing phosphorus and nitrogen. Compared with the similar products, the water absorption of the super absorbent resin is greatly enhanced; the super absorbent resin contains the nutrition elements of nitrogen and phosphorus, does not need pasting in comparison with the process of directly using starch and greatly improves the preparation process. The super absorbent resin has favorable development prospect in agriculture management, such as desert greening, water conservation, soil improvement, seedling transplantation and the like.
Owner:INNER MONGOLIA UNIVERSITY

Method and device for treating phosphorus wastewater by adopting multi-electrode baffling electric flocculation process

The invention belongs to the technical field of sewage treatment in environmental engineering, and particularly relates to a method and a device for treating phosphorus wastewater by adopting a multi-electrode baffling electric flocculation process. The PH value of wastewater is regulated with alkaline liquor to 7.0-8.0; the regulated wastewater is pumped into an electric flocculation tank through a peristaltic pump, is subjected to electrolytic flocculation treatment through the baffling of a multi-electrode under the condition of aeration, and then is discharged through an overflow launder, the discharged water is collected and left to stand for 30 minutes, a liquid supernatant is discharged, a floc is recycled; a power supply of the electric flocculation tank is a direct current power supply, the current density is 1.27-5.08mA/cm<2>, and the electrolysis time is 2 minutes to 48 hours. The technical characteristics are as follows: the wastewater baffles along the multi-electrode, then the short stream of the wastewater is avoided, the chance of enabling a pollutant in the wastewater to be in contact with a high-concentration flocculating agent in an electrolysis plate is increased, the flocculent precipitation is promoted, so that the pollutant treatment effect is improved. The multi-electrode baffling electric flocculation process is suitable for treating inorganic phosphorus wastewater at medium and low concentrations, needed equipment is simple, easy in operation and low in cost, and runs stably, so that the process is an electrochemistry phosphorous removal process having a high potential.
Owner:中国中化股份有限公司 +2

Method for recycling acid and valuable metal from oxalic acid wastewater

The invention discloses a method for comprehensively recovering acid and valuable metals from waste water of oxalic acid, comprising the steps: neutral phosphorus type extracting agent is used for extracting the oxalic acid, and then de-ionized water is used for back extracting the oxalic acid from the washed organic phase; the obtained diluted oxalic acid solution is concentrated and crystallized to obtain oxalic acid crystal; after the oxalic acid is extracted, acid solution is adjusted by chloride or chlorine hydride solution to ensure the concentration of chloridion to be not less than 3.0mol/L; valuable metallic ions are extracted out of the acid solution with the adjusted concentration of chloridion by polymer amine extracting agent, and the valuable metals is back extracted out from the washed organic phase by using dilute hydrochloric acid or dilute sulphuric acid solution. The method leads the recovery rate of the oxalic acid in the waste water of oxalic acid to be more than 95%, the recovery rate of valuable metals be more than 95%, the oxalic acid content of the recovered oxalic acid crystal to be more than 99.5%, the oxalic acid content of the inorganic acid to be less than 0.2g/L and the concentration of the valuable metallic ion to be less than 0.05g/L. The method can realize the comprehensive recycling of various valuable materials in the waste water and zero emission of waste water.
Owner:CENT SOUTH UNIV

Treatment process and device of industrial wastewater containing heavy metal ions

The invention belongs to the technical field of water treatment, and in particular relates to a treatment process and device of industrial wastewater containing heavy metal ions. The treatment process and device comprise two parts namely an enhanced pre-treatment process and device and an adsorption treatment process and device, wherein the enhanced pre-treatment device comprises a raw water bucket, a reaction sedimentation tank and a filter tower which are connected with one another in sequence; the adsorption treatment device comprises a middle water tank, an adsorption tower and a clean water tank which are connected with one another in sequence. A filter material in the filter tower consists of quartz sand, anthracite, cobblestone, activated carbon, or zeolite; and a filling material in the adsorption tower is a hydrogel adsorption material. The treatment process and device disclosed by the invention have the advantages that a polymer hydrogel adsorbent and a fixed bed technology are adopted for effectively reducing the concentration of the heavy metal ions in a water body; and the adsorbed hydrogel is desorbed by using acid liquor to recycle the adsorption materials and reduce the wastewater treatment cost. The device disclosed by the invention is simple in structure and occupies a small space; the equipment is compact and simple and easy to operate so as to ensure high water quality and stability of effluent.
Owner:NANJING UNIV

Method for recycling nickel, buffer salt and water from chemical nickel-plating ageing solution

The invention discloses a method for recycling nickel, buffer salt and water from chemical nickel-plating ageing solution. The method comprises the following steps: 1) filtering the ageing solution by virtue of a filter; 2) carrying out electrolysis treatment on the chemical nickel-plating ageing solution; 3) heating the ageing solution by utilizing a heat exchanger, enabling the ageing solution to enter a low temperature vacuum evaporation concentrator to be evaporated and concentrated, so that phosphate and sulfate are crystallized; 4) enabling condensation water to sequentially pass through a reverse osmosis membrane, an ion exchange filter and a porous medium adsorption filter to be filtered and recycled as production water supply; and 5) enabling mixed liquor after crystallization to enter a crystallization fluidized bed to be separated, so that mixed crystals of sulfate and phosphate are obtained, removing crystal salt particles in effluent by virtue of a security filter, then recycling to an electrolytic tank, and carrying out secondary recycling on residual nickel. The method disclosed by the invention can realize complete recycling of metal nickel, dissolved salt and water in the chemical nickel-plating ageing solution, and pollution of electroplating ageing solution to the environment is reduced to the greatest extent.
Owner:生态环境部华南环境科学研究所(生态环境部生态环境应急研究所)

Liquid crystal composition with high reliability and application thereof

The invention provides a liquid crystal composition with the high reliability and application thereof. The liquid crystal composition is prepared from, by weight, 5-40 parts of a compound represented by the general formula I (the formula is shown in the description), 20-70 parts of a compound represented by the general formula II (the formula is shown in the description), 1-40 parts of a compound represented by the general formula III (the formula is shown in the description) and 0-30 parts of a compound represented by the general formula IV (the formula is shown in the description). The liquid crystal composition has the high voltage holding ratio, the low ion concentration, the excellent light stability, the appropriate optical anisotropy, the good low-temperature intersolubility, the high elastic constant and the good thermal stability and can effectively solve the reliability problem of a liquid crystal display, effectively solve the residual image problem of the liquid crystal display, improve the display quality of the liquid crystal display and prolong the service life of the liquid crystal display. Therefore, the liquid crystal composition is suitable for high-reliability TN, IPS and FFS type TFT liquid crystal display devices and especially suitable for IPS and FFS type liquid crystal display devices.
Owner:BEIJING BAYI SPACE LCD MATERIALS TECH

Preparation method of ultra-pure and ultrafine silver nanowire

The invention provides a preparation method of an ultra-pure and ultrafine silver nanowire. The preparation method comprises the following steps: step 1, an ethylene glycol solution with sodium bromide, an ethylene glycol solution with sodium chloride, an ethylene glycol solution with PVP and an ethylene glycol solution with silver nitrate are prepared, and in the preparation process, moisture inethylene glycol is removed through heating; and step 2, the ethylene glycol is taken, heating is conducted to remove the moisture, the ethylene glycol solution with sodium bromide, the ethylene glycolsolution with sodium chloride, the ethylene glycol solution with PVP and the ethylene glycol solution with silver nitrate which are prepared in the step 1 are added, the temperature is increased to form a nucleus, temperature increasing is reduced, and the ultra-pure and ultrafine silver nanowire is prepared. According to the preparation method, the adsorbed moisture in the ethylene glycol is removed through heating, thus the concentration of hydroxyl plasma in a reaction solution is effectively decreased, seed crystal damage caused by ion etching is reduced, the dynamic process of nucleus forming is adjusted and controlled, the probability that the crystal nucleus grows into the nanowire is increased significantly, and the ultra-pure and ultrafine silver nanowire can be obtained withoutthe need of the subsequent purification process.
Owner:SHAANXI COAL & CHEM TECH INST +1

Preparation method of A-site magnesium-calcium double-doped lanthanum ferrite composite oxide material

InactiveCN107857302ABest preparation conditionsPrecise and controllableNanotechnologyIron compoundsWater bathsComposite oxide
The invention belongs to the technical field of preparation of lanthanum ferrite composite oxide materials, and particularly discloses a preparation method of an A-site magnesium-calcium double-dopedlanthanum ferrite composite oxide material. The preparation method comprises the following steps of adding La(NO3)3.6H2O (lanthanum nitrate), Fe(NO3)3.9H2O (ferric nitrate), Mg(NO3)2.6H2O (magnesium nitrate) and Ca(NO3)2.4H2O (calcium nitrate) into a prepared citric acid solution; then, adding ammonium hydroxide, treating in a water bath, drying, and calcining, so as to obtain the composite oxidematerial. The preparation method has the advantages that the Mg<2+> ion and Ca<2+> ion double-doped La0.85Mg0.15-xCaxFeO3 nanoparticle is synthesized by an accurate, controllable and easy nitrate saltsol-gel method at low temperature; the obtained samples has a single phase, and is of an orthorhombic crystal system structure, the space group is Pnma, Mg<2+> and Ca<2+> are used for replacing La<3+>, and the growth of particles is inhibited; the A-site magnesium-calcium double-doped lanthanum ferrite composite oxide material has wide application prospect in fields of electricity, magnetic sensors, industrial catalyzing, gas-sensitive material, information storage, spin-electron devices, and the like.
Owner:HAINAN MEDICAL COLLEGE
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