Low-temperature worm and gear lubricating grease composition and preparation method thereof
A lubricating grease composition and worm gear technology, applied in the field of lubricating grease, can solve problems such as difficult start-up, frequent maintenance and oil changes, etc., and achieve the effects of high output efficiency, excellent low-temperature start-up performance, and low friction coefficient
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Embodiment 1
[0045] Embodiment one (normal pressure method)
[0046] 1) 180 kg of polyethylene glycol ether (V40=69.22mm 2 / s, the same below), 50 kg of 12-hydroxystearic acid were added to the reaction kettle in sequence, stirring and heating was started to raise the temperature to 90±10°C, all the mixture in the kettle became liquid, and 7.5 kg of LiOH·H 2 O and 37.5 kg of distilled water mixed solution, saponification reaction at constant temperature between 100-110°C for 30-90 minutes (12-hydroxystearic acid, LiOH·H 2 O reacts with distilled water mixture to generate lithium soap as a thickening agent).
[0047] 2) Continue to heat up to 160±10°C, add 167kg of polyethylene glycol ether, further stir and heat up to 210±15°C, and add metal deactivator: 2kg of benzene Triazole (T706) and antioxidant: 20 kg of phenyl-α-naphthylamine (T531), stirred for 10±5 minutes.
[0048] 3) 300 kilograms of polyethylene glycol ether and 150 kilograms of trimethylolpropane saturated fatty acid ester ...
Embodiment 2
[0049] Embodiment two (prefabricated soap method)
[0050] 1) Base oil: 380 kg polyalphaolefin oil (V40=146.98mm 2 / s, the same below) and thickener: 92 kg of 12-hydroxy lithium stearate were added to the reaction kettle in turn, and the temperature was raised to 210±15°C with heating and stirring. Agent: 3 kilograms of benzotriazole (T706), antioxidant: 5 kilograms of phenyl-α-naphthylamine (T531) and 5 kilograms of 2,6-di-tert-butyl-p-cresol (T501), stirred for 10 ± 5 minutes.
[0051] 2) The material is discharged into a blending kettle in which 190 kg of polyalphaolefin oil and 192 kg of bis-(2-ethylhexyl) sebacate have been added, stirred and cooled to 70±15°C, and extreme pressure anti-wear Agent: 3 kg amine phosphate, 30 kg oily potassium borate (T361), friction modifier: 15 kg isomeric monoglyceride stearate, rust inhibitor: 5 kg barium dinonyl naphthalene sulfonate (T705), solid Lubricant: 30 kg polytetrafluoroethylene ultrafine powder (PTFE) and 50 kg boron nitrid...
Embodiment 3
[0052] Embodiment three (prefabricated soap method)
[0053] 1) 393 kilograms of polyalphaolefin oil (V40=19.14mm 2 / s, the same below) and thickener: 45 kg of lithium stearate were added to the reaction kettle in turn, and the temperature was raised to 210±15°C with stirring and heating. Diphenylamine and 2.5 kg of diisooctyldiphenylamine were stirred for 10 ± 5 minutes.
[0054] 2) The material is discharged into the blending kettle that has added base oil: 200 kg of polyalphaolefin oil and 180 kg of di-(2-ethylhexyl) adipate, stirred and cooled to 70±15°C, and then added polar Pressure antiwear agent: 15 kg tricresyl phosphate (T306), 45 kg oily potassium borate (T361), friction modifier: 15 kg isomeric monoglyceride stearate, rust inhibitor: 5 kg dimer oleic acid, 3 kilograms of dodecenylsuccinic acid (T746), metal deactivator: 1.5 kilograms of benzotriazole derivatives (T551), solid lubricant: 30 kilograms of polytetrafluoroethylene ultrafine powder (PTFE) and 70 kilogr...
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