Method for detecting radix astragali

A detection method and technology for medicinal materials, which are applied in the field of quality detection of astragalus medicinal materials, can solve the problems of difficult quality control, complicated detection methods for astragalus medicinal materials, etc., and achieve the effects of high accuracy, good accuracy and practical effect, and simple method.

Inactive Publication Date: 2014-12-10
LONGXI ZHONGTIAN PHARM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] For this reason, the technical problem to be solved by the present invention is that the detection method of Radix Astragali medicinal material is complicated in the p

Method used

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  • Method for detecting radix astragali
  • Method for detecting radix astragali
  • Method for detecting radix astragali

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Example 1 Determination of Astragaloside IV Content

[0039] 1. Instruments and reagents

[0040] 1.1 Instrument Shimadzu LC-20AT high performance liquid chromatograph, Shimadzu SPD-M10A VP diode array detector, Mettler AL-204 electronic balance, D101 macroporous adsorption resin column, Soxhlet extractor.

[0041] 1.2 Reagents Standard products of astragaloside IV and calycocetin glucoside were purchased from China Food and Drug Administration, acetonitrile, methanol (chromatographic grade); formic acid, ammonia test solution, n-butanol, purified water, were analytical reagents.

[0042] 1.3 Samples of medicinal materials Astragalus samples from various places in Gansu were collected. The batches of the tested medicinal materials were selected from: 2 batches in Longxi County, Gansu, marked as 1-2, Dongjiabao in Shouyang, Longxi, Gansu, Caiziping, Shouyang, Longxi, Gansu, and Caiziping, Shouyang, Gansu. Weiyuan Huichuan, Gansu Lintao, Gansu Weiyuan 2 batches, respecti...

Embodiment 2

[0053] Example 2 Calycosin glucoside content:

[0054] 1. Instruments and reagents

[0055] 1.1 Instrument Shimadzu LC-20AT high performance liquid chromatograph, Shimadzu SPD-M10A VP diode array detector, Mettler AL-204 electronic balance, D101 macroporous adsorption resin column, Soxhlet extractor.

[0056] 1.2 Reagents Standard products of astragaloside IV and calycocetin glucoside were purchased from China Food and Drug Administration, acetonitrile, methanol (chromatographic grade); formic acid, ammonia test solution, n-butanol, and purified water were analytical reagents.

[0057] 1.3 Samples of medicinal materials Astragalus samples from various places in Gansu were collected. The batches of the tested medicinal materials were selected from: 2 batches in Longxi County, Gansu, marked as 1-2, Dongjiabao in Shouyang, Longxi, Gansu, Caiziping, Shouyang, Longxi, Gansu, and Caiziping, Shouyang, Gansu. Weiyuan Huichuan, Gansu Lintao, Gansu Weiyuan 2 batches, respectively marke...

Embodiment 3

[0069] Example 3 Determination of Pesticide Residues in Radix Astragali

[0070] 1 Instruments and reagents

[0071] 1.1 Instrument

[0072] Clarus600 gas chromatography-mass spectrometry (US PE company), HS10260D ultrasonic extractor (Kunshan Ultrasonic Instrument Co., Ltd.), RE-52A rotary evaporator (Shanghai Yarong Biochemical Instrument Factory).

[0073] 1.2 Reagent

[0074] Dichlorvos, methamidophos, acephate, tetrachloronitrobenzene, hexachlorobenzene, α-666, β-666, γ-666, δ-666, omethoate, dimethoate Azinon, pentachloronitrobenzene, monocrotophos, difenthion, phosphamide I, dimethoate, heptachlor, pentachloroaniline, chlorothalonil, chlorpyrifos-methyl, aldrin, captan, phosphamide II. Methyl parathion, pirimiphos-methyl, methyl pentachlorophenyl sulfide, metalaxyl, triadimefon, chlorpyrifos, malathion, fenitrothion, parathion, pendimethalin , cis epoxy heptachlor, trans epoxy heptachlor, triadimenol A, triadimenol B, trans chlordane, cis endosulfan, cis chlordane, ...

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Abstract

The invention belongs to the field of detection of the quality of traditional Chinese medicinal materials and in particular relates to a method for detecting the quality of radix astragali. The method comprises the steps of determining the content of astragaloside and calycosin contained in radix astragali and determining the pesticide residues of radix astragali. The method conduces to solving the technical problems that identification methods of traditional physicochemical properties are complex to operate and have limitation and the quality is difficult to regulate and control, has high degree of accuracy, is simple, convenient and fast to operate, is low in cost and has good application prospect and economic benefits.

Description

technical field [0001] The invention belongs to the field of quality detection of traditional Chinese medicinal materials, and in particular relates to a quality detection method of medicinal materials of Radix Astragali. Background technique [0002] Astragalus, containing several chemical components, including sucrose, glucuronic acid, astragaloside IV, calycosin, formononetin, astragaloside Ⅱ, astragaloside Ⅲ, astragalus polysaccharides A, B, C, D, mucilage, and various amino acids , Bitterin, astragaloside, choline, folic acid, flavan compounds and various trace elements such as selenium, silicon, zinc, cobalt, copper and molybdenum. For invigorating qi and solidifying the surface, diuretic and toxin support, evacuation of pus, astringing sores and promoting granulation. Astragalus has been on the market in my country for many years, and its clinical effects have been widely affirmed. The main components of astragaloside IV, calycosin, formononetin, astragaloside Ⅱ, an...

Claims

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Application Information

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IPC IPC(8): G01N30/02
Inventor 杨锡陈杰李波韩斌李登鹏赵建邦何禄仁宋平顺张平
Owner LONGXI ZHONGTIAN PHARM CO LTD
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