Method for reducing and removing organic pollutant deposition and ink in pulp and paper production
A technology of organic pollutants, pulping and papermaking, applied in pulp fat/resin/pitch/wax removal, papermaking, textiles and papermaking, etc., can solve the problems of narrow application range, poor effect and poor effect, and achieve elimination Interaction, reduction of organic pollutant deposition and deinking effect
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preparation example Construction
[0076] 1. The preparation methods of polymers A, B, D, E, G and H are: The synthesis method of polyoxystyrene includes:
[0077] (1) Add tri-styrene phenol and ethylene oxide into the reactor according to the required mole ratio of the target product, and mix them evenly; then add the catalyst zincdiethyl and Water, the weight of which is based on the ratio of water: zinc diethyle: ethylene oxide to 1:1.10:13; then a large amount of dioxan is added as the reaction solvent, The reaction kettle was evacuated, and after reaching a high vacuum, the above reactants were heated to 80° C. and allowed to stir and mix continuously for 240 hours of reaction.
[0078] (2) Dissolve the product obtained from the above reaction in a benzene solution, then add methanol to precipitate the catalyst Zinc Diethyl, and terminate the polymerization reaction; then, the solid matter is separated and removed by centrifugal separation.
[0079] (3) Polymers D and H need to evolve the sulfonation reaction ac...
Embodiment 1
[0093] A method for reducing the deposition of organic pollutants in the production of pulping and papermaking. The method is mainly used for the control of organic pollutants (stickies) in the process of recycling waste newspapers to produce newsprint.
[0094] 1. Material
[0095] The dry cellulose pulp of deinked waste newspaper pulp (ONP) was obtained from a paper mill in the south.
[0096] Conventional stickies control agent adopts the registered trademark of Ashland Company Make reference comparison.
[0097] See Table 1 for other polymer products.
[0098] Two, method
[0099] Use a food mixer ( ) Simulate the pulp mixing and drying process in the process of pulp and paper production, measure the amount of stickies deposited on the surface of the mixing tank and stirring blade under different conditions, and then compare the effects of various components on the deposition of organic matter.
[0100] The conditions of the deposition test are: dry cellulose pulp 100 grams (dry pul...
Embodiment 2
[0109] A method for reducing the deposition of organic pollutants in the production of pulp and paper. The method is mainly used to control organic pollutants (stickies) in the process of producing corrugated paper with recycled boxboard (OCC).
[0110] 1. Material
[0111] The dry cellulose pulp of recycled boxboard pulp (OCC) was obtained from a paper mill in the south.
[0112] Biological enzyme composition (cellulase, hemicellulase and esterase), wherein: cellulase is a commercial product FiberZyme G200 of Dyadic Company, hemicellulase is a commercial product, and esterase is Guangzhou Ruichen Shengda Bio Clean Enzyme from Technology Co., Ltd. TM The product, model SC-3000, is derived from Aspergillus (Aspergillus) and expressed in E. coli after recombination. The relative activity ratio to the reaction substrate triglyceride and ethyl acetate is between 10 and 3.
[0113] See Table 1 for other polymer products used.
[0114] Two, method
[0115] according to figure 1 The producti...
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