Preparation method of composite base material for facial masks
A technology of composite substrate and facial mask, applied in cosmetic preparations, chemical instruments and methods, pharmaceutical formulations, etc., can solve the problems of unaffordable, high cost of biological fibers, etc. The effect of high liquid rate
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[0015] The preparation method of composite base material for facial mask that the present invention proposes comprises the following steps:
[0016] (1) Lay the non-woven fabric support layer on the internally grounded metal plate. The non-woven fabric support layer is polyester (PET), polypropylene (PP) modified hydrophilic spun-bonded cloth, polyester / sticky Either glue or cotton fiber spunlace cloth;
[0017] (2) The polymer is dissolved in an organic solvent to obtain a polymer spinning solution. In the polymer spinning solution, the mass percent of the polymer is 5-20 wt%, and the polymer is polyacrylonitrile, polyvinyl alcohol Or polylactic acid, the organic solvent is: N, N-dimethylformamide (DMF), dimethylacetamide (DMAc), dichloromethane (DCM), acetone, tetrahydrofuran, formic acid, acetic acid, hexafluoroacetone , one or more of hexafluoroisopropanol, fluoroisopropanol, and trifluoroacetic acid.
[0018] (3) Add the biopolymer substance to the above-mentioned polym...
Embodiment 1
[0026] (1) Spread the spunlace PET non-woven fabric support layer with a grammage of 30g / m2 on the internally grounded metal plate;
[0027] (2) The polyvinyl alcohol with a weighed average degree of polymerization of 1750 and a degree of alcoholysis of 98% is dissolved in the mixed solution of acetone, hexafluoroacetone and DMF, wherein the volume ratio of acetone, hexafluoroacetone and DMF is 7:1:4, configured as a polyvinyl alcohol spinning solution with a mass fraction of 13%, and stirred to dissolve it;
[0028] (3) adding the weighed silk fibroin to the dissolved polymer spinning solution to prepare a mixed spinning solution, the mass percentage of silk fibroin being 10%;
[0029] (4) process the mixed spinning solution on an ultrasonic processor for 60 min;
[0030] (5) Use the above-mentioned mixed spinning solution for electrospinning, control the ambient humidity to 40%, and the temperature to be 25°C, place the spinning needle above the above-mentioned metal plate ...
Embodiment 2
[0032] (1) Spread the PP modified hydrophilic spunbond non-woven fabric support layer with a grammage of 20g / m2 on the inner grounded metal plate.
[0033] (2) be 1750 by the average degree of polymerization that weighed, alcoholysis degree is 98% polyvinyl alcohol, be dissolved in the mixed solution of acetone, hexafluoroisopropanol and DMF, wherein acetone, hexafluoroisopropanol and The volume ratio of DMF is 7:1:4, configured as a polyvinyl alcohol spinning solution with a mass fraction of 13%, and stirred to dissolve it;
[0034] (3) adding the weighed chitin into the dissolved polymer spinning solution to prepare a mixed spinning solution, the mass percentage of chitin is 4wt%;
[0035] (4) process the mixed spinning solution on the ultrasonic processor for 200min;
[0036] (5) Use the above-mentioned mixed spinning solution for electrospinning, control the ambient humidity to 40%, and the temperature to be 25°C, place the spinning needle above the above-mentioned metal ...
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