A kind of anti-radiation sandwich pipe and its preparation method
A radiation protection and pipeline technology, applied in pipeline protection, chemical instruments and methods, pipeline damage/wear prevention, etc., can solve the problems of poor impact resistance, cumbersome operation, length limitation, etc., to improve mechanical strength, improve preparation quality, The effect of increasing safety
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preparation example Construction
[0057] A preparation method for a radiation-proof sandwich pipe, comprising the steps of:
[0058] 1) Add polymer monomers into the reactor, and according to the bonding strength to the intermediate layer, shielding performance (such as lead equivalent), impact resistance, elastic modulus, dimensional stability and apparent viscosity and flow of the slurry According to the requirements of material performance and process performance, such as diluent, initiator, coupling agent, etc.; initiate polymerization and control the conversion rate of monomer; add radioactive shielding function treated with or without coupling agent under high-speed stirring Powder and / or inorganic modified powder treated with or without coupling agent, the mass ratio of prepolymer: (radioactive functional powder + inorganic modified powder) is 1.0:0.5~4.0, wherein, shielding The mass ratio of the radioactive functional powder to the inorganic modified powder is 5.0:0-4.0. Carry out vacuum degassing the...
example 1
[0072] A preparation method for a radiation-proof sandwich pipe, comprising the steps of:
[0073] Step 1) Add a certain amount of additives such as polyvinyl alcohol (PVA), n-butyraldehyde, diluent, initiator, coupling agent, curing agent, etc. to the reactor, condense under the action of acid catalysis and control the conversion rate of monomer Add nano-lead powder and boric acid powder through or without coupling agent under high-speed stirring, prepolymer: (nano-lead powder+boric acid) mass ratio is 1.0:4.0, wherein, the mass ratio of nano-lead powder and boric acid The ratio is 5.0:0.5; then carry out vacuum degassing to obtain slurry;
[0074] Step 2) washing and drying the first-diameter pipe 7 made of borosilicate glass with different diameters and the second-diameter pipe 8 made of borosilicate glass with cleaning agent solution and water;
[0075] Step 3) nesting the first diameter pipe 7 and the second diameter pipe 8 together to form a set of nested pipes;
[007...
example 2
[0082] A preparation method for a radiation-proof sandwich pipe, comprising the steps of:
[0083] Step 1) First add methyl acrylate, dibutyl ester, benzoic acid, silane, benzoyl peroxide, azobisisobutyronitrile, dibutyl phthalate and methacrylic acid in the reaction kettle according to the weight ratio and other additives to initiate polymerization and control the conversion rate of the monomer; add barium sulfate + titanium oxide treated with or without coupling agent under high-speed stirring, and select the prepolymer: (barium sulfate + titanium oxide) with a mass ratio of 1.0 : 0.5, wherein, the mass ratio of nano-lead powder and boric acid is 5.0: 0.5; then carry out vacuum degassing to obtain slurry;
[0084] Step 2) Rinse and dry lithium-aluminosilicate glass-ceramic pipes of different diameters, and / or borosilicate glass or silicate glass pipes with cleaning agent solution and water;
[0085] Step 3) nesting the first diameter pipe 7 and the second diameter pipe 8 to...
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