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Burning-free and steaming-free brick microcrystalline assistant and preparation method thereof

A technology of microcrystals and additives, applied in the field of building materials, can solve the problems of difficult formation of building material gelling materials, poor activity excitation effect, poor freeze-thaw resistance, etc., and achieve good process performance, processing and molding performance, and water absorption. Low, early intensity high effect

Active Publication Date: 2019-10-18
山东辉石能源工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] With the expansion of urbanization, the demand for building materials is also increasing, and industrial waste and sand contain a large amount of SiO needed for building materials. 2 、Al 2 o 3 , Ca ions and other substances, but these substances in waste slag and sand are not active under normal conditions, and it is difficult to form the cementitious material required for manufacturing building materials. To prepare double-free bricks (steam-free and non-sintered bricks), they must be sintered and steam-cured. , Chemical activity can be excited to form, but the first two methods consume a lot of energy, but also cause different degrees of pollution to the environment
Chemical activity excitation, as a new technology, has been paid more and more attention by people, but the current domestic and foreign existing technologies have the problems of poor activity excitation effect, long molding time, slow strength growth, high water absorption rate, and poor freeze-thaw resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A double brick-free microcrystalline additive, comprising the following raw materials in percentage by weight: 18kg of saturated fatty acid, 12kg of organic tertiary amine, 0.25kg of chloride, 0.75kg of inorganic strong base, 69kg of inorganic acid salt, wherein the saturated fatty acid is palmitic acid, The organic tertiary amine is benzyl dimethylamine, the chloride is potassium chloride, the inorganic strong base is sodium hydroxide, and the inorganic acid salt is obtained by mixing sodium sulfate and potassium silicate at a weight ratio of 2:1.

[0021] A method for preparing a double brick-free microcrystalline additive, comprising the following steps:

[0022] (1) Add the weighed saturated fatty acid and organic tertiary amine into the reaction kettle, heat up and stir, react at 85°C for 6 hours, and then cool down to 65°C;

[0023] (2) Then add the weighed inorganic acid salt, chloride, and inorganic strong base into the reaction kettle of step (1), and continue ...

Embodiment 2

[0025] A double brick-free microcrystalline additive, comprising the following raw materials in weight percentage: 20kg of saturated fatty acid, 10.5kg of organic tertiary amine, 0.28kg of chloride, 0.6kg of inorganic strong base, 68.62kg of inorganic acid salt, wherein saturated fatty acid is octanoic acid and Lauric acid is obtained by mixing 1:1 by weight, the organic tertiary amine is obtained by mixing triethanolamine, piperidine, and pyridine by 1:1:1 by weight, the chloride is potassium chloride, and the strong inorganic base is sodium hydroxide and hydroxide Lithium is obtained by mixing at a weight ratio of 4:3, and the inorganic acid salt is obtained by mixing sodium sulfate and sodium silicate at a weight ratio of 5:2.

[0026] A method for preparing a double brick-free microcrystalline additive, comprising the following steps:

[0027] (1) Add the weighed saturated fatty acid and organic tertiary amine into the reaction kettle, heat up and stir, react at 87°C for 6...

Embodiment 3

[0030] A double brick-free microcrystalline additive, including the following raw materials in weight percentage: 23kg of saturated fatty acid, 8.5kg of organic tertiary amine, 0.3kg of chloride, 0.45kg of inorganic strong base, 67.75kg of inorganic acid salt, wherein the saturated fatty acid is capric acid , myristic acid, and arachidic acid are mixed in a weight ratio of 1:3:4, and the organic tertiary amine is triethanolamine, DMP-10, K-61B, piperidine, and picoline in a weight ratio of 1:1:1:1:1 It is obtained by mixing, the chloride is potassium chloride, the strong inorganic base is obtained by mixing sodium hydroxide, potassium hydroxide and lithium hydroxide in a weight ratio of 1:1:1, and the inorganic acid salt is sodium sulfate, potassium nitrite, potassium nitrate, Sodium silicate and sodium phosphate are mixed in a weight ratio of 1:1:1:1:1.

[0031] A method for preparing a double brick-free microcrystalline additive, comprising the following steps:

[0032] (1)...

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PUM

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Abstract

The invention discloses a burning-free and steaming-free brick microcrystalline assistant and a preparation method thereof, and belongs to the technical field of building materials. The burning-free and steaming-free brick microcrystalline assistant is prepared from the following raw materials in percentage by weight: 18-30% of saturated fatty acid, 5-12% of organic tertiary amine, 0.25-0.35% of chloride, 0.15-0.75% of inorganic alkali, and the balance of inorganic acid salt. According to the burning-free and steaming-free brick microcrystalline assistant and the preparation method thereof, the quality of burning-free and steaming-free bricks prepared by using the burning-free and steaming-free brick microcrystalline assistant can be significantly improved, and thus the burning-free and steaming-free bricks have the characteristics of the low admixture amount, high-efficiency activity excitation, the good process performance, the good machine shaping performance, the good plasticity, the high early strength, the low water absorption and excellent freeze-thaw resistance; and a more effective solidification technology for large-scale comprehensive utilization of industrial waste residue and sand is provided, broad market prospects are achieved in manufacturing of the building materials, and the very important significance for saving arable land, reducing environmental pollution,turning waste into treasure and recycling resources is achieved.

Description

technical field [0001] The invention relates to the technical field of building materials, in particular to a double brick-free microcrystalline additive and a preparation method thereof. Background technique [0002] With the progress of society and large-scale industrialization, natural resources are less and less, and industrial waste residues are increasing. It is urgent to save natural resources and develop high-tech comprehensive utilization of industrial waste residues. [0003] Fly ash, coal gangue, red mud, dredging sediment, industrial gypsum (such as desulfurization gypsum, phosphogypsum, titanium gypsum, fluorine gypsum, carbide slag, smelting waste residue, tailings slag, etc.) There are more and more industrial waste residues. Stockpiling not only takes up a lot of land, but also causes serious harm to the environment. The desert not only has a large stock, but also causes serious air pollution with the wind, and it is constantly encroaching on the surrounding...

Claims

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Application Information

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IPC IPC(8): C04B24/12
CPCC04B40/0039C04B2103/0068C04B24/085C04B24/121C04B22/124C04B22/062C04B22/147C04B12/04C04B24/122C04B24/128C04B24/12C04B22/085C04B22/16
Inventor 付宏正陈光平王锋陈泽健付华辉郭彩娥杨坤徐向开
Owner 山东辉石能源工程有限公司
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