Preparation method of composite phase change coating beneficial to heat dissipation of lithium ion battery
A lithium-ion battery, composite phase change technology, applied in secondary batteries, battery pack components, circuits, etc., can solve the problems of shortened service life, low thermal conductivity, poor thermal conductivity of paraffin, and improve thermal conductivity and heat dissipation. The effect of large internal surface area and excellent thermal conductivity
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[0029] The invention provides a method for preparing a composite phase-change coating that is beneficial to heat dissipation of lithium-ion batteries. The phase-change precursor is made by encapsulating the phase-change agent in attapulgite with a channel structure, and then the phase-change precursor is Mix with alumina sol to make a slurry, then coat lithium batteries, and form a composite phase change coating after drying; the phase change agent is paraffin; the attapulgite has a purity ≥ 85%, and the attapulgite used in the present invention Attapulgite is a kind of phase change agent adsorption carrier. Attapulgite is a hydrous aluminum-magnesium silicate mineral with two-dimensional nanoscale crystals (about 20nm in diameter and about 100-200μm in length). The series of crystal channels have small volume and mass, but large internal surface area, and have good adsorption performance, which can increase the adsorption amount of paraffin phase change agent while reducing th...
Embodiment 1
[0039] Under the condition of 80°C water bath, melt the paraffin wax, add an appropriate amount of attapulgite (Jiangsu Xuyi, purity ≥ 85%), the mass ratio of attapulgite to paraffin wax is 1.5:1, and stir evenly to obtain a phase change precursor; Aluminum alkoxide was configured into a 1mol / L aqueous solution at 90°C, and the pH of the solution was adjusted to 3 with nitric acid, and the stirring was continued until the solution was clear, and the alumina sol was obtained after standing for 24 hours; Mix at 1:15 and disperse by ball milling to obtain a uniform slurry, then coat to form a coating with a thickness of less than 20 μm, and vacuum dry at room temperature for more than 24 hours to obtain a composite phase change coating.
Embodiment 2
[0041] Under the condition of 80°C water bath, melt the paraffin wax, add an appropriate amount of attapulgite (Jiangsu Xuyi, purity ≥ 85%), the mass ratio of attapulgite to paraffin wax is 2:1, and stir evenly to obtain a phase change precursor; Aluminum alkoxide was configured into a 0.8mol / L aqueous solution at 90°C, and the pH of the solution was adjusted to 4 with nitric acid, and the stirring was continued until the solution was clear, and left to stand for 24 hours to obtain alumina sol; the phase change precursor and alumina sol were mixed by mass Mix at a ratio of 1:20, and disperse by ball milling to obtain a uniform slurry, and then coat to form a coating with a thickness of less than 20 μm, and dry it in vacuum at room temperature for more than 24 hours to obtain a composite phase change coating.
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