Preparation method and application of porous carbon reinforced microbial biofilm culturing carrier material
A film-hanging carrier and porous carbon technology, which is applied in chemical instruments and methods, sustainable biological treatment, biological water/sewage treatment, etc., can solve the problems of poor mechanical strength of immobilized particles, long time for microbial film hanging, and difficult recovery operations. and other problems, to achieve the effect of enriching charged atoms, promoting homogeneous nucleation and granulation, improving adsorption and mechanical strength
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Embodiment 1
[0042] The preparation of embodiment 1 porous carbon
[0043] 1) Put 1 kg of rice straw biochar (10-20 mesh) into 0.1 mol / L 10L hydrochloric acid solution, treat it at 75°C for 60 minutes, wash until the eluate is neutral, and dry (drying temperature 103 ±2°C, time 4h) to obtain acidified rice straw biochar;
[0044] 2) Mix 1 kg of acidified rice straw biochar, 100 g of nano-montmorillonite, 100 g of hydrated silicate, 50 g of polyacrylamide and 300 g of amino starch binder to obtain a premix;
[0045] 3) Add 0.3mol of FeCl 3 ·6H 2 O, 0.1mol of CaCl 2 , 0.2mol of LaCl 3 ·7H 2 O is diluted with 110g of solvent water and sprayed onto the surface of 100g of the premixed material, then the moisture content of the material system is adjusted to 45±2%, and then the material is transferred to the HTLAB high-temperature and high-pressure reactor (150°C, 6MPa, stirring speed 100r / min), carry out surface functional modification for 3 hours, and obtain surface-modified biochar;
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Embodiment 2
[0049] The preparation of embodiment 2 porous charcoal microorganism hanging film carrier material
[0050] Add film-hanging carrier materials (the test group FPB obtained in Example 1, the control group PB) in the reactors whose tops are not closed, and the input amount accounts for 4 / 5 of the total volume of the reactor, and the activated sludge (this example The medium activated sludge comes from the aerobic pool of Zhenjiang Jingkou District Sewage Treatment Plant, and the MLSS of activated sludge is 5500mg / L. In specific implementation, aerobic activated sludge from other sources can also be used).
[0051] The dosage is 15g of dry weight sludge per liter of porous carbon material. The porous carbon material is immersed in the activated sludge, injected into the reactor from the top through the nozzle, and the remaining activated sludge flowing out from the bottom is collected, introduced into the recovery tank, and passed through the pressure The water pump is circulated...
Embodiment 3
[0059] Example 3 Porous carbon membrane-hanging carrier material phosphorus accumulating bacteria domestication and nitrogen and phosphorus removal test in water
[0060]Take aquaculture wastewater as test sewage, take 100 mL of aquaculture wastewater solution (ammonia nitrogen content is 20 mg / L, TP content is 10 mg / L), put it in a 150 mL Erlenmeyer flask, add 0.2 g of M -FPB (membrane-hanging 36h), acclimatization at room temperature for 14 days, adding 100mL solution of the same solute concentration to the system on the 2nd, 4th, 8th, and 14th day respectively, and measuring the changes of ammonia nitrogen and TP content in the system solution at different days. The test results are as follows: Figure 4 shown.
[0061] The domestication refers to: the enrichment and domestication of phosphorus-accumulating bacteria by using the conventional construction of anaerobic-aerobic alternating environment (see the literature "Li Wei, Sun Huizhi, Wei Wei, etc. 2019, the domesticati...
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