Aluminum or aluminum alloy antibacterial material
An antibacterial material and aluminum alloy technology, which is applied in metal material coating process, ion implantation plating, coating, etc., can solve the problems of high difficulty in sterilizing particles, incomplete filling, unsatisfactory actual control speed, etc.
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Embodiment 1
[0047] An aluminum or aluminum alloy antibacterial material, the preparation process is as follows:
[0048] (1) Pretreatment: rough polishing - degreasing - washing - heat treatment - electropolishing:
[0049] The rough polishing is to use 600-mesh and 800-mesh water-grinding sandpaper to polish the surface of the aluminum material in sequence.
[0050] The degreasing is to use acetone solution to wash and soak.
[0051] Described thermal treatment is under inert condition, at 450 o C under high temperature treatment for 20min.
[0052] The electrolytic polishing is 50g / L phosphoric acid, 20g / L sulfuric acid, 3g / L glycerol, voltage 15V, time 2-5min, temperature 45 o c.
[0053] (2) Self-assemble monolayer PS pellets on the pretreated aluminum surface: Weigh 0.1g sodium dodecylsulfonate and 0.1g potassium persulfate and dissolve them in 70ml methanol and water solution, wherein the ratio of methanol is 10:2, keep the nitrogen atmosphere, magnetically stir for 30min, rais...
Embodiment 2
[0062] An aluminum or aluminum alloy antibacterial material, the preparation process is as follows:
[0063] (1) Pretreatment: rough polishing - degreasing - washing - heat treatment - electropolishing:
[0064] The rough polishing is to use 600-mesh and 800-mesh water-grinding sandpaper to polish the surface of the aluminum material in sequence.
[0065] The degreasing is to use acetone solution to wash and soak.
[0066] Described heat treatment is under inert condition, at 475 o C under high temperature treatment for 25min.
[0067] The electrolytic polishing is 50g / L phosphoric acid, 20g / L sulfuric acid, 3g / L glycerol, voltage 15V, time 3.5min, temperature 45 o c.
[0068] (2) Self-assemble monolayer PS pellets on the pretreated aluminum surface: Weigh 0.2g sodium dodecylsulfonate and 0.1g potassium persulfate and dissolve in 70ml methanol and water solution, wherein the ratio of methanol is 10:3.5, keep the nitrogen atmosphere, magnetically stir for 30min, raise the ...
Embodiment 3
[0077] An aluminum or aluminum alloy antibacterial material, the preparation process is as follows:
[0078] (1) Pretreatment: rough polishing - degreasing - washing - heat treatment - electropolishing:
[0079] The rough polishing is to use 600-mesh and 800-mesh water-grinding sandpaper to polish the surface of the aluminum material in sequence.
[0080] The degreasing is to use acetone solution to wash and soak.
[0081] Described heat treatment is under inert condition, at 500 o C under high temperature treatment for 30min.
[0082] The electrolytic polishing is 50g / L phosphoric acid, 20g / L sulfuric acid, 3g / L glycerin, voltage 15V, time 5min, temperature 45 o c.
[0083] (2) Self-assemble monolayer PS pellets on the pretreated aluminum surface: Weigh 0.3g of sodium dodecylsulfonate and 0.1g of potassium persulfate and dissolve them in 70ml of methanol and water solution, wherein the ratio of methanol is 10:5, keep the nitrogen atmosphere, magnetically stir for 30min, ...
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