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Microbial filtering membrane for treating high-ammonia-nitrogen sewage and preparation method of microbial filtering membrane

A microbial filtration and high ammonia nitrogen technology, applied in the field of filtration membranes, can solve the problems of poor reusability of microbial filtration membranes, poor water quality filtration effect, poor microbial immobilization effect, etc., to improve antifouling and mechanical properties, and increase repeated use Sexual, well-tolerated effect

Inactive Publication Date: 2021-06-18
广州市点滴生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the commonly used microbial filtration membranes generally have no filtering effect on water quality; on the one hand, the way of enrichment of the membrane layer has poor immobilization effect on microorganisms, which tends to make the microorganisms appear free in the sewage, while the high concentration of ammonia nitrogen can inhibit the activity of microorganisms effect, thereby reducing the removal rate of ammonia nitrogen; on the other hand, the treatment process is likely to cause microbial contamination, making the microbial filtration membrane reusable.
[0003] In addition, the common microorganisms that deal with ammonia nitrogen include nitrifying bacteria, which need oxygen in the process of nitrifying ammonia nitrogen, and generally oxygenate through aeration, which consumes a lot of oxygen mechanically.
The photosynthesis of cyanobacteria can produce oxygen, supply nitrifying cells, reduce oxygen consumption, and reduce costs, but light has an inhibitory effect on the activity of nitrifying bacteria

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Step 1: Wash and crush the celery, put it in a nitrogen atmosphere, set the gas flow rate to 230mL / min, the pyrolysis temperature to 450°C, and the pyrolysis time to 2.5 hours; grind and sieve, wash with deionized water, and dry. Autoclave to obtain biochar; at room temperature, mix biochar with 10g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 7.8, and transfer to a constant temperature shaking incubator , set the temperature at 28°C, the shaking speed at 135 rpm, and the shaking time at 5.5 hours; wash with sterile saline to obtain nitrifying bacteria / biomass charcoal.

[0029] Step 2: Add 32 parts of polysulfone and 6 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in sequence, set the temperature at 60°C, stir for 7 hours, and cool to obtain a polysulfone with a concentration of 15wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix the cultured 4g / L cyanobacteria stock...

Embodiment 2

[0033] Step 1: Wash and crush the celery, place it in a nitrogen atmosphere, set the gas flow rate to 200 mL / min, the pyrolysis temperature to 400°C, and the pyrolysis time to 2 hours; grind and sieve, wash with deionized water, and dry , high-pressure sterilization to obtain biochar; at room temperature, mix biochar with 8g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 7.6, and transfer to constant temperature shaking culture In the box, set the temperature to 25° C., the shaking speed to 120 rpm, and the shaking time to 5 hours; wash with sterile physiological saline to obtain nitrifying bacteria / biomass charcoal.

[0034] Step 2: Add 30 parts of polysulfone and 4 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in turn, set the temperature at 60°C, stir for 6 hours, and cool to obtain a polysulfone with a concentration of 10wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix th...

Embodiment 3

[0038] Step 1: Wash and crush the celery, place it in a nitrogen atmosphere, set the gas flow rate to 250 mL / min, the pyrolysis temperature to 500°C, and the pyrolysis time to 3 hours; grind and sieve, wash with deionized water, and dry , high-pressure sterilization to obtain biochar; at room temperature, mix biochar with 12g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 8.0, and transfer to constant temperature shaking culture In the box, set the temperature to 30° C., the shaking speed to 150 rpm, and the shaking time to 6 hours; wash with sterile physiological saline to obtain nitrifying bacteria / biomass charcoal.

[0039] Step 2: Add 35 parts of polysulfone and 9 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in turn, set the temperature at 60°C, stir for 8 hours, and cool to obtain a polysulfone with a concentration of 20wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix t...

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Abstract

The invention discloses a microbial filtering membrane for treating high-ammonia-nitrogen sewage and a preparation method of the microbial filtering membrane. The microorganism filtering membrane is prepared from the following raw materials in parts by weight: 18-22 parts of multi-layer bacterium fixing capsules, 25-30 parts of sodium alginate and 50-60 parts of acrylamide. The invention has the beneficial effects that (1) cyanobacteria and nitrifying bacteria are combined as microorganisms, so recyclable oxygen supply is formed, and high-ammonia-nitrogen sewage is synergistically removed; (2) microorganisms are packaged to prepare the multi-layer bacterium fixing capsule, so biological pollution is effectively inhibited, the activity of the microorganisms in high-concentration sewage is ensured, and the recycling rate is increased; (3) by utilizing the shell of the multi-layer bacterium immobilizing capsule, the microorganism filtering membrane forms a calcium ion crosslinking and polyacrylamide interpenetrating network taking the microorganism filtering membrane as a winding point, so that the mechanical strength and the water flux are effectively enhanced.

Description

technical field [0001] The invention relates to the technical field of filter membranes, in particular to a microbial filter membrane for treating high-ammonia-nitrogen sewage and a preparation method thereof. Background technique [0002] The microbial filtration membrane used for sewage treatment can utilize the microorganisms enriched on the membrane layer to absorb and metabolize the chemical components in sewage, and has a good purification effect on sewage treatment. However, the commonly used microbial filtration membranes generally have no filtering effect on water quality; on the one hand, the way of enrichment of the membrane layer has poor immobilization effect on microorganisms, which tends to make the microorganisms appear free in the sewage, while the high concentration of ammonia nitrogen can inhibit the activity of microorganisms effect, thereby reducing the removal rate of ammonia nitrogen; on the other hand, the treatment process is likely to cause microbia...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F3/10C02F3/34C02F101/16
CPCC02F3/102C02F3/105C02F3/34C02F2101/16Y02W10/10
Inventor 杨宏明
Owner 广州市点滴生物科技有限公司
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