Microbial filtering membrane for treating high-ammonia-nitrogen sewage and preparation method of microbial filtering membrane
A microbial filtration and high ammonia nitrogen technology, applied in the field of filtration membranes, can solve the problems of poor reusability of microbial filtration membranes, poor water quality filtration effect, poor microbial immobilization effect, etc., to improve antifouling and mechanical properties, and increase repeated use Sexual, well-tolerated effect
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Embodiment 1
[0028] Step 1: Wash and crush the celery, put it in a nitrogen atmosphere, set the gas flow rate to 230mL / min, the pyrolysis temperature to 450°C, and the pyrolysis time to 2.5 hours; grind and sieve, wash with deionized water, and dry. Autoclave to obtain biochar; at room temperature, mix biochar with 10g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 7.8, and transfer to a constant temperature shaking incubator , set the temperature at 28°C, the shaking speed at 135 rpm, and the shaking time at 5.5 hours; wash with sterile saline to obtain nitrifying bacteria / biomass charcoal.
[0029] Step 2: Add 32 parts of polysulfone and 6 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in sequence, set the temperature at 60°C, stir for 7 hours, and cool to obtain a polysulfone with a concentration of 15wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix the cultured 4g / L cyanobacteria stock...
Embodiment 2
[0033] Step 1: Wash and crush the celery, place it in a nitrogen atmosphere, set the gas flow rate to 200 mL / min, the pyrolysis temperature to 400°C, and the pyrolysis time to 2 hours; grind and sieve, wash with deionized water, and dry , high-pressure sterilization to obtain biochar; at room temperature, mix biochar with 8g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 7.6, and transfer to constant temperature shaking culture In the box, set the temperature to 25° C., the shaking speed to 120 rpm, and the shaking time to 5 hours; wash with sterile physiological saline to obtain nitrifying bacteria / biomass charcoal.
[0034] Step 2: Add 30 parts of polysulfone and 4 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in turn, set the temperature at 60°C, stir for 6 hours, and cool to obtain a polysulfone with a concentration of 10wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix th...
Embodiment 3
[0038] Step 1: Wash and crush the celery, place it in a nitrogen atmosphere, set the gas flow rate to 250 mL / min, the pyrolysis temperature to 500°C, and the pyrolysis time to 3 hours; grind and sieve, wash with deionized water, and dry , high-pressure sterilization to obtain biochar; at room temperature, mix biochar with 12g / L nitrifying bacteria liquid evenly, use 0.2mol / L sodium hydroxide to adjust the pH of the solution to 8.0, and transfer to constant temperature shaking culture In the box, set the temperature to 30° C., the shaking speed to 150 rpm, and the shaking time to 6 hours; wash with sterile physiological saline to obtain nitrifying bacteria / biomass charcoal.
[0039] Step 2: Add 35 parts of polysulfone and 9 parts of polyethylene glycol 10000 into N-methyl-2-pyrrolidone in turn, set the temperature at 60°C, stir for 8 hours, and cool to obtain a polysulfone with a concentration of 20wt%. Sulfone-polyethylene glycol solution, set aside; at room temperature, mix t...
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