Preparation method of composite silicate nitrogen fertilizer
A technology of compound silicate and nitrogen fertilizer, applied in fertilization methods, urea compound fertilizer, nitrogen fertilizer and other directions, can solve the problems of poor slow-release effect of urea-formaldehyde slow-release fertilizer, high energy consumption of silicate fertilizer, and poor particle strength, etc. , to achieve the effect of disease prevention and insect prevention plants absorbing heavy metals, reducing plants absorbing heavy metals, and increasing the effective silicon content
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Embodiment 1
[0028] A preparation method of composite silicate nitrogen fertilizer, comprising the following steps: 1. taking CaSiO 3 100kg of wollastonite raw material with a mass content of 95% was ground to a wollastonite micropowder with a particle size of 5um and a length-diameter ratio of 15:1 with a jet pulverization pressure of 0.6MPa, and the wollastonite micropowder was prepared in a chemical reaction kettle A slurry with a concentration of 55% was formed, and the stirring speed was 400 rpm. 2. In the slurry of step 1, dropwise add the sulfuric acid with a concentration of 0.5 mol / kg, and the sulfuric acid dripping rate is 0.03 mol / min, so that the pH value is under the condition of 5.5, and the reaction temperature is kept at 50 ° C, and the stirring speed is kept at 400 rpm. The reaction time 8min. 3. 500kg of urea with a particle diameter of 2.5mm is added to the drum granulator for preheating with hot air, and when the temperature reaches 35 ° C, the reaction mixture obtaine...
Embodiment 2
[0031] A preparation method of composite silicate nitrogen fertilizer, comprising the following steps: 1. taking CaSiO 3 100kg of wollastonite raw material with a mass content of 90% was ground to a wollastonite micropowder with a particle size of 10um and an aspect ratio of 8:1 at a jet pulverization pressure of 0.4MPa, and the wollastonite micropowder was prepared in a chemical reaction kettle A slurry with a concentration of 45% was formed, and the stirring speed was 200 rpm. 2. In the slurry of step 1, drip the sulfuric acid with a concentration of 0.35 mol / kg, and the sulfuric acid dripping rate is 0.03 mol / min, so that the pH value is under the condition of 6.5, and the reaction temperature is kept at 45 ° C, and the stirring speed is kept at 200 rpm, and the reaction time 8min. 3. 600kg of urea with a particle diameter of 1mm is added to the drum granulator for preheating with hot air, and when the temperature reaches 30 ° C, the reaction mixture obtained in step 2. A...
Embodiment 3
[0034] A preparation method of composite silicate nitrogen fertilizer, comprising the following steps: 1. taking CaSiO 3 105kg of wollastonite raw material with a mass content of 95% was ground to a wollastonite micropowder with a particle size of 6um and an aspect ratio of 13:1 at a jet pulverization pressure of 0.5MPa, and the wollastonite micropowder was prepared in a chemical reaction kettle A slurry with a concentration of 50% was formed, and the stirring speed was 300 rpm. 2. In the slurry of step 1, drip the sulfuric acid with a concentration of 0.4 mol / kg, and the sulfuric acid dripping rate is 0.03 mol / min, so that the pH value is under the condition of 5.8, and the reaction temperature is kept at 55 ℃, and the stirring speed is kept at 300 rpm, and the reaction time for 7min. 3. 600kg of urea with a particle diameter of 2mm is added to the drum granulator for preheating with hot air, and when the temperature reaches 32 ° C, the reaction mixture obtained in step 2. i...
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