Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

105results about How to "Limit diffusion" patented technology

Nitrogen doped porous carbon/sulfur composite positive material as well as preparation method and application thereof

The invention belongs to the field of electrochemical energy and discloses a nitrogen doped porous carbon/sulfur composite positive material as well as a preparation method and an application thereof in preparation of a lithium-sulfur battery positive plate. The nitrogen doped porous carbon/sulfur composite positive material disclosed by the invention is prepared by adopting a sulfur-ammonium chemical precipitation method; three-dimensional wedged nitrogen-containing porous carbon and sulfur particles form a core-shell structure, so that the electronic and ionic conductivity of the composite positive material are improved; meanwhile, the sulfur bearing capacity is also improved, dissolution and diffusion of polysulfides are limited, and thus the circulation stability and the capacity retention rate of a composite electrode prepared from the nitrogen doped porous carbon/sulfur composite positive material disclosed by the invention can be effectively increased. The preparation method can be used for accurately controlling the content of loaded sulfur without complex pretreatment and post-treatment procedures, so that the process cost is greatly lowered, the process operation is simplified, and the consistency and the stability of the composite material are improved as well.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Laser-enhanced three-dimensional micro-region electro-deposition method and corresponding device thereof

The invention provides a laser-enhanced three-dimensional micro-region electro-deposition method. the method integrates laser irradiation into a microtubule-based micro-region electro-deposition device to obtain an improved deposition rate. Electrolyte is poured into an electrolyte chamber and a microtubule, a tip of the microtubule is close to a sample surface by the regulation of a translation stage, a droplet at the tip of the microtubule forms a meniscus on the sample surface so that the diffusion of the droplet on the sample surface is limited, and machining accuracy of electro-depositionis beneficially controlled. As the electrolyte in the microtubule is connected with the positive potential and the surface of a conductive sample is the negative potential, the electro-deposition process can occur. The laser is irradiated on the contact surface between the droplet and the sample, and a laser thermal effect improves the electron transfer efficiency in the electrolyte, acceleratesthe positive shift of the electrochemical balance potential and causes local eddy current stirring in the droplet, and therefore accelerates the electro-deposition process. According to the preset pattern, the electronic control transition stage movement is regulated, so the three-dimensional relative movement of the microtubule and the sample surface is realized.
Owner:橙河微系统科技(上海)有限公司

Multi-layer electrode structure for lithium sulfur battery and preparation method thereof

The invention discloses a multi-layer electrode structure for a lithium sulfur battery and a preparation method thereof. The multi-layer electrode structure comprises a current collector (1) and a multi-layer covering layer attached to the current collector (1), wherein the multi-layer covering layer has a loose porous layer (2), a conductive skeleton layer (3) and a confinement layer (4) which covers an electrode surface, close to the current collector (1) along a direction perpendicular to the current collector (1). The loose porous layer in the multi-layer electrode structure has a large pore structure and a high porosity, and can fully contain a sulfur active material, electrolyte and a multi-sulfide-ion charge-discharge product; the conductive skeleton layer in the middle provides a high-activity reaction interface for a charge-discharge reaction of the lithium sulfur battery by using a large specific surface area; the confinement layer on the electrode surface limits the diffusion of multiple sulfide ions; and the multi-layer electrode structure provided by the invention solves the problems of low sulfur utilization rate and poor cycle stability under high sulfur content andhigh sulfur loading of the lithium sulfur battery.
Owner:四川华昆能源有限责任公司

Sodium iron chlorophyllin-chitosan/sodium alginate microcapsules and preparation method thereof

The invention discloses sodium iron chlorophyllin-chitosan/sodium alginate microcapsules and a preparation method thereof. In the method, chitosan/sodium alginate is used as a capsule material, sodium iron chlorophyllin is used as capsule content, and the sodium iron (II) chlorophyllin is microencapsulated by an emulsification-gel method. The preparation method comprises: dissolving sodium iron chlorophyllin in sodium alginate solution at a certain concentration, adding the prepared solution in vegetable oil containing Span-60, and stirring at high steep and emulsifying for 20 minutes; dripping acetic acid aqueous solution containing 2.0-percent chitosan and calcium chloride, continuously stirring for 30 minutes, standing for 2 hours and removing an oil phase; and washing the microcapsules with petroleum ether and isopropanol for three times respectively, performing suction-filtration, and drying at room temperature to obtain the sodium iron chlorophyllin-chitosan/sodium alginate microcapsules. The chitosan which is a natural polysaccharide with high biocompatibility and biodegradability and the sodium alginate serve as sustained and controlled release agent and targeting preparation, the sodium iron chlorophyllin is encapsulated in the center of the microcapsules to be protected from instability caused by change in a light or placing condition, a new formulation is provided in pharmacy, and the microcapsules are suitable to be further developed and used as iron-supplying health-care food and new medicinal preparation for treating iron-deficiency anemia, and have a bright application prospect.
Owner:NORTH CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY

CoSe2/hollow carbon nanosphere/S composite lithium-sulfur battery positive electrode material and preparation method thereof

The invention relates to a CoSe2 / hollow carbon nanosphere / S composite lithium-sulfur battery positive electrode material and a preparation method thereof. The preparation method comprises the following steps: (1) adding hollow carbon nanospheres into a methanol solution dissolved with cobalt nitrate hexahydrate, and carrying out stirring; (2) carrying out washing and drying to obtain a solid product; (3) carrying out heat preservation on the obtained solid product to obtain Co / hollow carbon nanospheres; (4) uniformly mixing the obtained Co / hollow carbon nanospheres with selenium powder, and carrying out heat preservation again to obtain CoSe2 / hollow carbon nanospheres; and (5) uniformly mixing the obtained CoSe2 / hollow carbon nanospheres with sulfur powder, and carrying out heat preservation to obtain the CoSe2 / hollow carbon nanosphere / S composite material. The composite positive electrode material prepared by the invention has high cycling stability when being used as a lithium-sulfurbattery positive electrode material, and can be widely applied to the field of preparation of the lithium-sulfur battery positive electrode material; and the preparation process of the cathode material is controllable, raw materials are easy to obtain, and the cost is low.
Owner:QILU UNIV OF TECH

Ge-Sb-Te Ge-enriched N-doped phase-change material for phase-change memory and preparation method thereof

ActiveCN102347446AIncreased crystalline resistivityLarge change in resistanceElectrical apparatusPhase-change memoryExternal energy
The invention relates to a Ge-Sb-Te Ge-enriched N-doped phase-change material for a phase-change memory. The Ge-Sb-Te Ge-enriched N-doped phase-change material for the phase-change memory, provided by the invention, comprises chemical components which accord with a chemical formula as follows: Nx[(Ge1+yTe)a(Sb2Te3)b]100-x, wherein y is more than 0 but not more than 3, x is more than 0 but not more than 35, a is equal to 1 or 2 and b is equal to 1 or 2. The phase-change material is a storage material which has a reversible phase change under the effects of external energy. When a magnetic control sputtering is adopted, atom percentage contents of all the components are adjusted through controlling a power supply power of each target material and each target position and the N2/Ar2 flow ratio so that phase-change storage materials with different crystallization temperatures, smelting points and crystallization activation energies are obtained. Compared with the traditional Ge2Sb2Te5 thin-film material, the Ge-enriched N-doped phase-change material provided by the invention has the advantages of higher crystallization temperature, better data keeping capability, better heat stability, lower power consumption and the like.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Gravity type foundation pit supporting system under vacuum effect and construction method

The invention discloses a gravity type foundation pit supporting system under a vacuum effect and a construction method. The system comprises a peripheral vertical sealed curtain, a pit top horizontal sealing layer, a transverse drainage body, a slope surface sealing layer, a slope bottom vertical sealed curtain, a pit top vertical drainage body and a slope surface vertical drainage body. The peripheral vertical sealed curtain is downward vertically installed from an outside boundary of a setting range of the pit top horizontal sealing layer; the pit top vertical drainage body is arranged in foundation soil of the setting range of the pit top horizontal sealing layer; the transverse drainage body is arranged on the surface of the foundation soil at a top end of the pit top vertical drainage body; the pit top horizontal sealing layer is formed on the surface of the transverse drainage body; the slope surface vertical drainage body is arranged in the foundation soil inside the pit top vertical drainage body; the slope surface sealing layer is formed on the slope surface vertical drainage body; the slope bottom vertical sealed curtain is formed in a slope foot of a pit bottom. In the gravity type foundation pit supporting system under the vacuum effect and the construction method provided by the invention, a side wall is not arranged to solidify a wall body and a curtain shielding body, a greater cutting depth requirement can be met, construction cost is low and construction period is shorter.
Owner:CHINA CIVIL ENG CONSTR CORP

Ge-Sb-Te Ge-enriched N-doped phase-change material for phase-change memory and preparation method thereof

The invention relates to a Ge-Sb-Te Ge-enriched N-doped phase-change material for a phase-change memory. The Ge-Sb-Te Ge-enriched N-doped phase-change material for the phase-change memory, provided by the invention, comprises chemical components which accord with a chemical formula as follows: Nx[(Ge1+yTe)a(Sb2Te3)b]100-x, wherein y is more than 0 but not more than 3, x is more than 0 but not more than 35, a is equal to 1 or 2 and b is equal to 1 or 2. The phase-change material is a storage material which has a reversible phase change under the effects of external energy. When a magnetic control sputtering is adopted, atom percentage contents of all the components are adjusted through controlling a power supply power of each target material and each target position and the N2 / Ar2 flow ratio so that phase-change storage materials with different crystallization temperatures, smelting points and crystallization activation energies are obtained. Compared with the traditional Ge2Sb2Te5 thin-film material, the Ge-enriched N-doped phase-change material provided by the invention has the advantages of higher crystallization temperature, better data keeping capability, better heat stability, lower power consumption and the like.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Multistage resistive random access memory and manufacturing method thereof

The invention aims to provide a multistage resistive random access memory and a manufacturing method of the multistage resistive random access memory. The multistage resistive random access memory comprises a substrate, a bottom electrode, a resistive layer and a top electrode, wherein the substrate, the bottom electrode, the resistive layer and the top electrode are arranged from bottom to top in sequence. The multistage resistive random access memory is characterized in that an isolation layer is further arranged between the bottom electrode and the resistive layer. According to the multistage resistive random access memory and the manufacturing method of the multistage resistive random access memory, the nanoscale isolation layer is additionally arranged, so that the magnitude of a storage window of the resistive random access memory is increased to over 105, and the primary condition needed by multistage storage is met; electrochemical active materials are used as the top electrode, different resistance states are achieved under the condition of different voltage drives through the drifting character of the electrochemical active materials, and the purpose of multistage storage is achieved; in addition, due to the additional arrangement of the isolation layer, dissipation of oxygen ions in the movement process is reduced, the bottom electrode is effectively protected, and the stability of a device is improved. In addition, the manufacturing method of the multistage resistive random access memory is simple and easy to control.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Training method and device of longitudinal federal learning model and computer equipment

The invention discloses a training method and device for a longitudinal federated learning model, and relates to the field of big data and the technical field of computers such as deep learning. According to the specific implementation scheme, the training method is applied to first participant equipment, and the first participant equipment has label data. The longitudinal federated learning model comprises a first bottom layer sub-model in the first participant device, an interaction layer sub-model, a top layer sub-model based on a Lipschitz neural network and a second bottom layer sub-model in the second participant device. And obtaining first bottom layer output data of the first participant device and second bottom layer output data sent by the second participant device, inputting the first bottom layer output data and the second bottom layer output data to the interaction layer sub-model to obtain interaction layer output data, obtaining top layer output data according to the interaction layer output data and the top layer sub-model, and sending the top layer output data to the interaction layer sub-model. And training a longitudinal federal learning model according to the top output data and the label data. According to the invention, the anti-attack capability of the federal learning system can be improved.
Owner:BEIJING BAIDU NETCOM SCI & TECH CO LTD

Alloy plate for automobile body and preparation method thereof

The invention provides an alloy plate for an automobile body and a preparation method of the alloy plate. An alloy comprises, by mass percentage, not larger than 0.4% of Si, not larger than 0.4% of Fe, 0.2-0.5% of Mn, 3.0-6.0% of Mg, not larger than 0.03% of Cr, not larger than 0.15% of Cu and the balance Al and impurities. According to the alloy plate and the preparation method, by controlling the content of the trace element Cr and the final annealing process and the straightening amount, on one hand, the YPE of the plate is reduced, and on the other hand, the plate still has excellent mechanical and forming properties of the material. The preparation method comprises the following steps that final annealing is carried out on a continuous annealing line, wherein the temperature rise speed is larger than 20 DEG C / s, and after heat preservation at 480-520 DEG C is carried out for 15 s and 5 min, water quenching is carried out, and the cooling speed is larger than 10 DEG C / s; the finalgrain size should be controlled at 20-40 micrometers, and the YPE is smaller than or equal to 0.2%; and the final annealing plate is subjected to straightening treatment, and the straightening amountis 0.5-1%. The plate prepared by the method is suitable for an automobile body structural member and an automobile body covering panel inner plate.
Owner:CHINALCO MATERIALS APPL RES INST CO LTD

Silicon-based molecular sieve/carbon tube sulfur-loaded composite positive electrode material, preparation method and application thereof

The invention provides a silicon-based molecular sieve/carbon tube sulfur-loaded composite positive electrode material, a preparation method and an application thereof. The technical scheme is that the preparation method comprises the following steps: mixing and grinding a carbon tube and elemental sulfur, adding CS2 and fully stirring, after that, drying to obtain a carbon tube sulfur-loaded composite material; and mixing the carbon tube sulfur-loaded composite material with carbon black and polyvinylidene fluoride according to a certain mass ratio, then adding N-methylpyrrolidone and the silicon-based molecular sieve, stirring and performing ultrasonic dispersion to be uniform, controlling the viscosity to be 1,000 to 10,000cps to obtain slurry, uniformly coating the obtained slurry on acurrent collector aluminum foil with a thickness of 150 to 400mm, then transferring the aluminum foil to a drying oven at 40 to 60 DEG C to obtain the silicon-based molecular sieve/carbon tube sulfur-loaded composite positive electrode material. The preparation method disclosed by the invention is simple to operate and easy for large-scale production; the prepared silicon-based molecular sieve/carbon tube sulfur-loaded composite positive electrode material is used for a lithium-sulfur battery, so that the dissolution of polysulfide ions in liquid electrolyte in the charging and discharging process of the lithium-sulfur battery can be solved, a shuttle effect is effectively inhibited, and the coulombic efficiency and the cycling stability of the lithium-sulfur battery are improved.
Owner:WENZHOU UNIVERSITY

Method for treating hexavalent chromium ions in soil by combining grouting with electroosmosis

The invention discloses a method for treating hexavalent chromium ions in soil by combining grouting with electro-osmosis. The method includes the steps: S1 drilling holes in the soil to be treated, setting grouting holes, and arranging negative electrodes and positive electrodes of electro-osmosis devices on the peripheries of the grouting holes; S2 injecting grouting materials with reduction, adsorption and gelatinizing performances into the grouting holes through an injection pump, and starting the electro-osmosis devices after grouting is completed to perform electro-osmosis treatment; S3collecting water solution at negative electrodes of the electro-osmosis devices, detecting the concentration of the hexavalent chromium ions in the water solution, stopping construction if the concentration of the hexavalent chromium ions meets design requirements, and repeating the step S2 and the step S3 if the concentration of the hexavalent chromium ions cannot meet design requirements. A grouting treatment method and an electro-osmosis treatment method are combined, so that the method is simple and convenient to operate, short in treatment period, large in treatment area, high in efficiency and applicable to soil layers with all natures.
Owner:湖南宏禹工程集团有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products