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Radiation cured adhesive for indium tin oxide (ITO) circuit and module protection

A technology of radiation curing and adhesives, which is applied in the direction of adhesives, adhesive types, polyurea/polyurethane adhesives, etc., which can solve the problems of long time, at least 48 hours, poor fluidity of RTV-1, hidden dangers of LCM reliability, etc. problems, to achieve the effects of high environmental test reliability, good product application reliability, and improved production efficiency and yield

Active Publication Date: 2013-04-24
DONGGUAN POWERBOND NEW MATERIALS TECH DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the curing time of RTV-1 is long, and it takes at least 48 hours to completely cure, which seriously affects the production efficiency; moreover, corrosive gases, such as acetic acid, etc. will be generated during room temperature vulcanization, which will cause damage to ITO circuits and IC chip modules. Corrosion; In addition, RTV-1 has poor fluidity, and it is prone to corner shrinkage during construction, thereby reducing the one-time yield rate, high rework rate, and wasting manpower and material resources; RTV-1 colloid has poor strength and weak adhesion. Reliability will cause hidden dangers; RTV-1 cannot pass the environmental test of high and low temperature impact for 1000 hours, high temperature and high humidity lighting test for 1000 hours, and cannot be applied to occasions that have higher requirements for LCD displays; RTV-1 is moisture curing type, it is required to be used up once after opening the package, otherwise it is easy to absorb moisture and thicken or even be scrapped, which brings great inconvenience to the on-site production organization

Method used

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  • Radiation cured adhesive for indium tin oxide (ITO) circuit and module protection
  • Radiation cured adhesive for indium tin oxide (ITO) circuit and module protection
  • Radiation cured adhesive for indium tin oxide (ITO) circuit and module protection

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A radiation curing adhesive used for ITO circuit and module protection, by weight, contains components and the percentage content of each component is as follows

[0034]

[0035] Described polyester acrylate is polyester acrylate CN922; Described reactive diluent is isobornyl acrylate (IBOA), 1,6 hexanediol diacrylate (HDDA) and trimethylolpropane triacrylate (TMPTA ), wherein the mass content of IBOA in the radiation-curable sealant is 9%, the mass content of HDDA in the radiation-curable sealant is 18.7%, and the mass content of TMPTA in the radiation-curable sealant is 9%; photoinitiator is cracking photoinitiator 184; coupling agent is silane coupling agent, choose γ-methacryloxypropyl trimethoxysilane (KH570); anti-aging agent is antioxidant 1010 ; The defoamer is silicone defoamer BYK-088.

[0036] The polysiloxane acrylate is self-made, and by weight, the contained components and the mass percentages of each component are:

[0037] Isocyanates: 50%

[...

Embodiment 2

[0049] A radiation curing adhesive used for ITO circuit and module protection, by weight, contains components and the percentage content of each component is as follows

[0050]

[0051] The polyester acrylate is polyester acrylate CN736; the reactive diluent is a mixture of isobornyl methacrylate (MIBOA), tripropylene glycol diacrylate (TPGDA) and dipentaerythritol hexaacrylate (DPHA) , wherein the mass content of MIBOA in the radiation-cured sealant is 10.8%, the mass content of TPGDA in the radiation-cured sealant is 3.6%, and the mass content of TMPTA in the radiation-cured sealant is 7.1%; The photoinitiator is a mixture of cleavage-type photoinitiator 184 and photoinitiator TPO; the coupling agent is a silane coupling agent, and γ-methacryloxypropyl trimethoxysilane (KH570) is selected; the anti The aging agent is antioxidant 2246; the defoamer is non-organic silicon defoamer Airex920.

[0052] The polysiloxane acrylate is self-made, and by weight, the contained comp...

Embodiment 3

[0064] A radiation curing adhesive used for ITO circuit and module protection, by weight, contains components and the percentage of each component is as follows,

[0065]

[0066]

[0067] Described polysiloxane acrylate is polysiloxane acrylate prepared in embodiment 1; Described polyester acrylate is polyester acrylate CN736; Described reactive diluent is isobornyl methacrylate (MIBOA ); the photoinitiator is a cleavage-type photoinitiator TPO; the silane coupling agent is a mixture of vinyltrimethylsilane and 3-methacryloxypropyltrimethoxysilane.

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PUM

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Abstract

The invention provides a radiation cured adhesive for indium tin oxide (ITO) circuit and module protection, which comprises the following components in percentage by mass: 30 to 70 percent of polysiloxane-acrylic ester, 10 to 50 percent of polyester acrylate, 0 to 40 percent of reactive diluent, 0.2 to 8 percent of photoinitiator, 0.1 to 5 percent of coupling agent, 0 to 2 percent of antiaging agent and 0 to 2 percent of defoamer, wherein the reactive diluents is an acrylate with a single(double or multiple) functional group; the photoinitiator is a cracking initiator, a hydrogen abstracting type initiator or a combination of the two; the coupling agent is a silane coupling agent; and the antiaging agent is one or several of a phenol antioxygen, an amine antioxygen, a sulfur compound antioxygen, a phosphorus compound antioxygen and an organic metal salt antioxygen. In the curing process of the adhesive, moisture is not required to participate in reaction, the adhesive can be cured quickly in the irradiation of ultraviolet, and then package can be accomplished; and thus, the production efficiency is improved greatly, energy is saved and raw material cost is reduced.

Description

technical field [0001] The invention belongs to the technical field of adhesives, and in particular relates to an adhesive for protecting COG, COF, and TAB modules of LCD liquid crystal screens, in particular to a radiation-cured adhesive for protecting ITO circuits and modules. Background technique [0002] In the LCD panel manufacturing process, it can be roughly divided into three stages, which are Array process, Cell process and Module process. The Array process refers to the fabrication of thin-film transistors (TFT) and color filters (CF) on a glass substrate; the Cell process uses the glass substrate of the TFT as the substrate, and combines it with the glass substrate of the CF. Liquid crystal (ODF process) is dripped between the substrates and the backlight plate is bonded to form an LCD panel (LCD panel); while the Module process is to assemble the driver IC, flexible circuit and some mechanical parts after inspecting the appearance of the LCD panel, and finally A...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J175/16C09J167/06C08G18/67C08G18/61G02F1/13
Inventor 黄战光杜学锋陈三多张小中吴国飞黄育环
Owner DONGGUAN POWERBOND NEW MATERIALS TECH DEV
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