Filtrate loss reducer for drilling fluid and preparation method thereof

A technology of fluid loss reducer and drilling fluid, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of high drilling fluid treatment costs, unstable performance of gel blocks, and heavy workload of mud workers. Achieve the effects of reduced treatment costs, excellent fluid loss reduction performance, and short production cycles

Inactive Publication Date: 2016-12-28
TIANJIN BO XING ENG SCI & TECH LIMITED COMPANY OF CNPC +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Currently widely used fluid loss control agents are supplied and used in powdered polymer products. Practice has shown that powdered polymers have many disadvantages when used, such as: slow dissolution rate, slow dissolution rate in the process of compounding the glue solution in field application, resulting in Increased working hours and even some polymers form gel blocks, resulting in unstable performance and easy to be screened out by vibrating sieves, resulting in waste; in addition, powdery polymers generally have a drying and crushing process, and the production cycle is long, and due to degradation, crosslinking, etc. The reaction will cause adverse effects and affect its performance, and it cannot be directly added to the drilling fluid during use, the dispersion speed is slow, the workload of the mud workers on site is heavy, and the cost of drilling fluid treatment is high

Method used

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  • Filtrate loss reducer for drilling fluid and preparation method thereof
  • Filtrate loss reducer for drilling fluid and preparation method thereof

Examples

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Effect test

Embodiment 1

[0031] The fluid loss control agent for drilling fluid in Example 1 of the present invention is an inverse emulsion polymer formed by emulsifying the water phase and the oil phase.

[0032] The preparation method of fluid loss reducer for drilling fluid in Example 1 of the present invention comprises the following steps:

[0033] Add 120kg of deionized water into the reaction kettle 1, add 51Kg of high-purity 2-acryloyloxy-2-methylpropanesulfonic acid powder (sulfonic acid group monomer), 34kg of acrylamide (amide group monomer), Styrene (rigid structure monomer) 6kg, N,N-methylenebisacrylamide (crosslinking agent) 9.1g and 1kg mass fraction are 10% azobisisoidine imidazoline hydrochloride (initiator) stirring Until it is completely dissolved, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust the pH to 8.0 to obtain a clear solution without solid phase particles; add 100 kg of white oil to the reaction kettle 2, start stirring, and slowly add fatty alco...

Embodiment 2

[0035] The preparation method of fluid loss reducer for drilling fluid in Example 2 of the present invention comprises the following steps:

[0036] Add 120kg of deionized water in the reaction kettle 1, add high-purity sodium styrene sulfonate powder (sulfonic acid group monomer) 47Kg, acrylamide (amide group monomer) 38kg, acrylonitrile (rigid structure monomer) 6kg , N, N-methylenebisacrylamide (crosslinking agent) 9.1g, 1.365kg mass fraction is 10% azobisisoidine imidazoline hydrochloride, 0.2kg ammonium bisulfite (initiator) is stirred to Dissolve completely, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust pH to 8.0, obtain clear solution without solid phase particles; add white oil 90kg in reaction kettle 2, start stirring, slowly add polyoxyethylene lose Sorbitan fatty acid ester (emulsifier) ​​0.5kg, sorbitan fatty acid ester (emulsifier) ​​6.8kg, stir evenly; Turn on the electric pump, slowly pump the solution in the reactor 1 to the reactor ...

Embodiment 3

[0038] The preparation method of fluid loss reducer for drilling fluid in Example 3 of the present invention comprises the following steps:

[0039]Add 120kg of deionized water in reactor 1, add high-purity 2-acrylamido-2-methylpropanesulfonic acid powder (sulfonic acid monomer) 56Kg, N,N-dimethylacrylamide (amide group monomer) 25kg, styrene (rigid structure monomer) 6kg, N,N-methylenebisacrylamide (crosslinking agent) 8.7g, control the temperature in the reactor 1 below 25°C, add 0.1kg persulfuric acid Ammonium (initiator), 0.03kg sodium bisulfite (initiator) are stirred to all dissolvings, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust pH to 8.0, make clear solution without solid phase particles; Add white oil 110kg in reactor 2, start stirring, slowly add 0.5kg alkylphenol polyoxyethylene ether (emulsifier), 6.8kg sorbitan fatty acid ester (emulsifier), stir; Slowly pump the solution in reactor 1 to reactor 2, open the nitrogen bottle, pass nitr...

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Abstract

The invention provides a filtrate loss reducer for a drilling fluid and a preparation method thereof. The filtrate loss reducer is an inverse emulsion polymer prepared from a water phase and an oil phase through emulsification. The water phase comprises, by weight, 45-56 parts of a sulfonic monomer, 25-38 parts of an amide group monomer, 5-10 parts of a rigid structure monomer and 100-120 parts of water. The water phase also comprises a cross-linking agent and an initiator, a mass ratio of the cross-linking agent to the sulfonic monomer, the amide group monomer and the rigid structure monomer is 0.008-0.015%, and a mass ratio of the initiator to the sulfonic monomer, the amide group monomer and the rigid structure monomer is 0.05-0.15%. The oil phase comprises 80-110 parts by weight of base oil and 4-10% by mass of an emulsifier. The preparation method has simple processes, a fast dissolution rate and excellent filtrate loss reduction performances.

Description

technical field [0001] The invention belongs to the technical field of drilling fluid treatment agents, in particular to a fluid loss control agent for drilling fluid and a preparation method thereof. Background technique [0002] In oil exploration or drilling operations, the drill bit is easily damaged under the action of huge pressure and friction, so drilling fluid is used to protect the drill bit during drilling operations, but the drilling fluid will seep into the formation soil under pressure and cause loss , this process is commonly referred to as "dehydration". A large amount of water loss entering the soil will not only induce wellbore instability, but also cause damage to oil and gas layers. The current solution to this problem is to add fluid loss control agents to the drilling fluid, which can block all directions The capillary channels in the mud cake formed by the drilling fluid and the soil make it smooth and dense; increase the negative charge density of th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/035C08F220/38C08F220/56C08F212/08C08F222/38C08F212/14C08F220/44C08F220/58C08F220/54C08F226/10
CPCC08F212/14C08F220/38C08F220/382C08F220/58C08F220/585C09K8/035C08F220/56C08F220/44C08F222/385C08F212/08C08F220/54C08F226/10
Inventor 朱红卫杨金龙刘建军谭文礼侯薇
Owner TIANJIN BO XING ENG SCI & TECH LIMITED COMPANY OF CNPC
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