Filtrate loss reducer for drilling fluid and preparation method thereof
A technology of fluid loss reducer and drilling fluid, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of high drilling fluid treatment costs, unstable performance of gel blocks, and heavy workload of mud workers. Achieve the effects of reduced treatment costs, excellent fluid loss reduction performance, and short production cycles
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Embodiment 1
[0031] The fluid loss control agent for drilling fluid in Example 1 of the present invention is an inverse emulsion polymer formed by emulsifying the water phase and the oil phase.
[0032] The preparation method of fluid loss reducer for drilling fluid in Example 1 of the present invention comprises the following steps:
[0033] Add 120kg of deionized water into the reaction kettle 1, add 51Kg of high-purity 2-acryloyloxy-2-methylpropanesulfonic acid powder (sulfonic acid group monomer), 34kg of acrylamide (amide group monomer), Styrene (rigid structure monomer) 6kg, N,N-methylenebisacrylamide (crosslinking agent) 9.1g and 1kg mass fraction are 10% azobisisoidine imidazoline hydrochloride (initiator) stirring Until it is completely dissolved, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust the pH to 8.0 to obtain a clear solution without solid phase particles; add 100 kg of white oil to the reaction kettle 2, start stirring, and slowly add fatty alco...
Embodiment 2
[0035] The preparation method of fluid loss reducer for drilling fluid in Example 2 of the present invention comprises the following steps:
[0036] Add 120kg of deionized water in the reaction kettle 1, add high-purity sodium styrene sulfonate powder (sulfonic acid group monomer) 47Kg, acrylamide (amide group monomer) 38kg, acrylonitrile (rigid structure monomer) 6kg , N, N-methylenebisacrylamide (crosslinking agent) 9.1g, 1.365kg mass fraction is 10% azobisisoidine imidazoline hydrochloride, 0.2kg ammonium bisulfite (initiator) is stirred to Dissolve completely, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust pH to 8.0, obtain clear solution without solid phase particles; add white oil 90kg in reaction kettle 2, start stirring, slowly add polyoxyethylene lose Sorbitan fatty acid ester (emulsifier) 0.5kg, sorbitan fatty acid ester (emulsifier) 6.8kg, stir evenly; Turn on the electric pump, slowly pump the solution in the reactor 1 to the reactor ...
Embodiment 3
[0038] The preparation method of fluid loss reducer for drilling fluid in Example 3 of the present invention comprises the following steps:
[0039]Add 120kg of deionized water in reactor 1, add high-purity 2-acrylamido-2-methylpropanesulfonic acid powder (sulfonic acid monomer) 56Kg, N,N-dimethylacrylamide (amide group monomer) 25kg, styrene (rigid structure monomer) 6kg, N,N-methylenebisacrylamide (crosslinking agent) 8.7g, control the temperature in the reactor 1 below 25°C, add 0.1kg persulfuric acid Ammonium (initiator), 0.03kg sodium bisulfite (initiator) are stirred to all dissolvings, add sodium carbonate and sodium hydroxide (acid-base regulator) to adjust pH to 8.0, make clear solution without solid phase particles; Add white oil 110kg in reactor 2, start stirring, slowly add 0.5kg alkylphenol polyoxyethylene ether (emulsifier), 6.8kg sorbitan fatty acid ester (emulsifier), stir; Slowly pump the solution in reactor 1 to reactor 2, open the nitrogen bottle, pass nitr...
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