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Composite material plugging agent for water plugging and leaking plugging of horizontal well and preparation method of composite material plugging agent

A composite material and horizontal well technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of high price, failure to meet wide range of applications, easy failure of plugging, interface adhesion and tensile shear strength low level problem

Pending Publication Date: 2021-10-08
陕西弘大众为石油科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The plugging agent has stable performance, good retention, strong adhesion, high elastic modulus, and high compressive strength. However, since the plugging agent is mainly composed of a large number of polymer materials, it cannot meet wide-scale applications due to its high price.
[0005] Chinese patent literature (CN 108504340 A) discloses a channeling and plugging agent for oilfields, which is measured by weight percentage and consists of 50% to 60% of inorganic salt microcrystalline material, 5% to 10% of honeycomb structure forming agent, microsphere Active filler 10%~20%, chelating performance modifier 2%~8%, colloidal structure toughening agent 3%~10%, colloidal structure strengthening agent 3%~10%, gel accelerator curing agent 2%~ 7%, mix and grind raw materials according to the above ratio to make powder with a particle size of 8-2500 mesh, and mix with water to make a slurry when used. Density: 1.45-1.8g / cm3, apparent viscosity: 20-85mpa.s. Because the plugging agent slurry prepared by this patented technology has a high water loss rate after hardening, it will cause volume shrinkage and cannot be applied to water plugging or channeling in the horizontal section of horizontal wells
Since the patented technology is mainly based on inorganic materials, the interface adhesion and tensile shear strength are low, and the plugging is easy to fail under the back pressure

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A composite material plugging agent for water plugging and leak plugging in horizontal wells, comprising the following components in parts by weight:

[0033] Inorganic cementitious material: 80 parts of 600-mesh G grade high sulfur-resistant oil well cement; inorganic auxiliary cementing material: 5.0 parts of 600-mesh sodium bentonite, 4.0 parts of 600-mesh quicklime; organic polymer reinforcement material: 120-mesh water-based polyester resin powder 4.0 parts; functional additives: 4.0 parts of asbestos wool below 100 mesh, 0.3 parts of hydroxypropyl methylcellulose, 2.4 parts of 80 mesh alcoholyzable silicone resin powder, retarder: 0.3 parts of trimethylene phosphonic acid;

[0034] A method for preparing a composite material plugging agent for water plugging and leak plugging in horizontal wells, comprising the following steps:

[0035] Step 1: 80 parts of 325-mesh G grade high sulfur-resistant oil well cement and 4.0 parts of 300-mesh quicklime are respectively p...

Embodiment 2

[0040] A composite material plugging agent for water and leakage plugging in horizontal wells, comprising the following components and steps:

[0041] Inorganic cementing material: 50 parts of 800 mesh 625 Portland cement; inorganic auxiliary cementing material: 15 parts of 800 mesh S95 mineral powder, 12 parts of 800 mesh national standard first-class fly ash; organic polymer reinforcement material: 100 mesh melamine 4.0 parts of resin powder; functional additives: 4.0 parts of short glass fibers below 200 mesh, 12 parts of 300 mesh UEA composite concrete expansion agent, 2.0 parts of octadecyltrimethoxysilane, 0.7 parts of carboxymethyl cellulose, retarder : 0.3 parts of sodium hexametaphosphate;

[0042] A method for preparing a composite material plugging agent for water plugging and leak plugging in horizontal wells, comprising the following steps:

[0043] Step 1: 50 parts of 325-mesh 625 Portland cement and 12 parts of 300-mesh national standard first-grade fly ash are...

Embodiment 3

[0048] A composite material plugging agent for water and leakage plugging in horizontal wells, comprising the following components:

[0049] Inorganic cementitious material: 65 parts of 600-mesh G-grade oil well cement; inorganic auxiliary cementing material: 6.0 parts of 600-mesh sodium bentonite, 6.0 parts of 600-mesh S95 mineral powder; organic polymer reinforcement material: modified ethylene-vinyl acetate copolymer 5.0 parts of functional additives: 8.0 parts of 600 mesh composite expansion agent, 5.0 parts of basalt short fiber below 200 mesh, 1.0 parts of AMPS-TPEG-AA terpolymer, 3.0 parts of water-based acrylic resin powder, retarder: retarder 1.0 parts of polycarboxylate superplasticizer;

[0050] A method for preparing a composite material plugging agent for water plugging and leak plugging in horizontal wells, comprising the following steps:

[0051] Step 1. Grinding 65 parts of 325-mesh G-grade oil well cement and 6.0 parts of 300-mesh sodium-based bentonite in a ...

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Abstract

The invention provides a composite plugging agent for water plugging and leakage plugging of a horizontal well. Thecomposite plugging agent comprises the following components in parts by weight: an inorganic cementing material, an inorganic auxiliary cementing material, an organic polymer reinforcing material, and a functional aid. The preparation method comprises the following steps: respectively processing an inorganic cementing material and an inorganic auxiliary cementing material into powder through a mechanical pulverizer or an airflow type ultrafine pulverizer; uniformly mixing an organic polymer reinforcing material and a part of inorganic material, heating by a double-screw extruder to prepare solid particles, and crushing the solid particles into powder; and uniformly stirring and mixing the prepared powder and a functional additive in a multifunctional stirrer to obtain composite material plugging agent powder for water plugging and leaking stoppage of the horizontal well. The use method comprises the following steps: preparing slurry-shaped plastic slurry in a dispersion machine, squeezing and injecting the prepared plastic slurry plugging agent to a layer needing to be plugged by using a cement pump truck and a squeezing and plugging pipe tool, lifting the squeezing and sealing tubular column, and waiting for solidification under pressure. According to the invention, the initial viscosity before thickening is low, the fluidity is good, the construction method is simple and feasible, and the storage is safe and stable.

Description

technical field [0001] The invention belongs to the field of oilfield chemistry, and in particular relates to a composite material plugging agent for water plugging and leakage plugging of horizontal wells and a preparation method thereof. Background technique [0002] Horizontal well water control and leak plugging technologies are still in the exploratory stage in oil and gas reservoir stimulation at home and abroad, and there is no effective method for reference at this stage. How to choose a high-performance plugging agent is particularly important in the research of water plugging and leak plugging technology for horizontal wells. For a long time, the development of oil and gas field plugging technology has been severely restricted by the two major defects of inorganic plugging agents, which cannot be injected and retained. Therefore, it is very urgent to develop a plugging agent for horizontal well water plugging and leakage plugging with micro-expansion and no fluid ...

Claims

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Application Information

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IPC IPC(8): C04B28/02C04B28/04C09K8/42C09K8/467C04B111/20C04B111/27C04B111/28
CPCC04B28/02C04B28/04C09K8/426C09K8/467C04B2201/50C04B2111/00724C04B2111/00663C04B2111/27C04B2111/28C04B2111/20C04B14/104C04B22/064C04B24/283C04B14/40C04B24/383C04B24/42C04B24/003C04B18/141C04B18/08C04B24/305C04B14/42C04B22/16C04B2103/0068C04B24/26C04B14/46C04B24/2688C04B2103/22C04B2103/302
Inventor 朱永刚徐贵东管盼盼吕鹏唐凡张涛
Owner 陕西弘大众为石油科技有限公司
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