Light heat insulating castable for lower part of CFB circulating fluidized bed separator and preparation method thereof
A technology of circulating fluidized bed and separator, which is applied in the field of lightweight thermal insulation castables, can solve the problems of complex manufacturing process, high power consumption of induced draft fan, and large resistance, so as to improve wear resistance and alkali corrosion resistance, and realize Reasonable utilization and the effect of saving manufacturing costs
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Embodiment 1
[0035] Example 1: Lightweight thermal insulation castable for the lower part of CFB circulating fluidized bed separator, including the following raw materials in parts by weight: 20 parts of lightweight skeleton material, 5 parts of wear-resistant thermal insulation material, 5 parts of bonding rubber, and composite admixture 3 parts, 10 parts of deionized water;
[0036]The lightweight skeleton materials include: 4 parts of vitrified microbeads, 3 parts of silicon carbide micropowder, 3 parts of nano-silicon dioxide, 2 parts of titanium dioxide, 3 parts of light calcium carbonate, 2 parts of closed-cell perlite, 2 parts of floating beads, heavy 1 part spar;
[0037] Wear-resistant insulation materials include: 2 parts of nano-ceramic powder, 1 part of alumina micropowder, 1 part of yttrium oxide, and 1 part of aerated aluminum powder;
[0038] The bonding compound includes: 2 parts of aluminate cement, 1 part of silicone resin, 1 part of nano-cerium oxide, and 1 part of mine...
Embodiment 2
[0040] Embodiment 2: What this embodiment records is the preparation method of the lightweight thermal insulation castable of embodiment 1, comprising the following steps:
[0041] S1. Preparation of lightweight skeleton materials;
[0042] S1-1. Weigh the raw materials of lightweight skeleton materials in proportion, mix them at a speed of 300rad / min for 15min, and then coarsely crush them until the particle size is 0.5-0.7mm; finally, put the coarsely crushed materials at 900°C Calcining for 1 hour, after the material is cooled, crush it again into a powder with a particle size of 0.06-0.09mm;
[0043] S1-2. Add 45wt% deionized water to the powder obtained in step S1-1, stir and mix evenly, and then place it in a vacuum extruder with a pressure of 2MPa, a vacuum degree of -0.09a and an extrusion temperature of 20°C Extruded in a medium to obtain a lightweight skeleton material precursor with a diameter of 0.3mm and a length of 0.4mm;
[0044] S1-3. Dry the lightweight skel...
Embodiment 3
[0052] Embodiment 3: What this embodiment records is the construction method of the castable finished product prepared by the method of Example 2, comprising the following steps: 1) supporting the mold according to the lower structure of the CFB circulating fluidized bed separator; 2) placing the castable The finished product is mixed with water to form a slurry, and the slurry is placed in a vacuum box with a vacuum degree of 5Mpa for vacuum degassing treatment for 35 minutes; through the vacuum degassing treatment of the slurry, the concentrated suspension inside the slurry forms a gel and is in situ Solidify and form to improve the wear resistance of the castable; wherein the amount of water added is 5% of the volume of the finished castable; 3) inject the slurry obtained in step 2) into the mold, and remove the mold after natural curing for 12 hours to obtain the embryo body, and then the embryo body Placed in a medium frequency induction sintering furnace, fired for 3 hour...
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