Light heat insulating castable for lower part of CFB circulating fluidized bed separator and preparation method thereof

A technology of circulating fluidized bed and separator, which is applied in the field of lightweight thermal insulation castables, can solve the problems of complex manufacturing process, high power consumption of induced draft fan, and large resistance, so as to improve wear resistance and alkali corrosion resistance, and realize Reasonable utilization and the effect of saving manufacturing costs

Inactive Publication Date: 2022-01-21
宜兴市兴贝耐火保温工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, the most popular circulating fluidized bed separator with the highest share in the international and domestic markets is a high-temperature cyclone separator made of refractory materials. Its main advantage is high separation efficiency, and its main disadvantages are bulky size and high wind speed at the tangential inlet of the separator. , high resistance, high power consumption of induced draft fan, high-speed flow of gas-solid two-phase toward the silo air flow reversely entrains a large amount of fly ash, and the original emission concentration of smoke and dust is high. The separator needs inner lining and outer heat insulation. The large amount of high-temperature grinding materials not only increases the cost of raw materials and manufacturing and installation of the separator, but also increases the thermal inertia, which is easy to coke at high temperature and slows down the boiler start-up and shutdown.
Some boilers use water-cooled or steam-cooled cyclone separators. Although the wear-resistant and high-temperature resistant materials are reduced, the problem of large thermal inertia is solved, the boiler does not coke, and the start and stop are fast, but there are also high wind speeds, large resistance, and induced draft fans. The power consumption is high, and the separation efficiency and stability are lower than those of cyclone separators made of wear-resistant high-temperature materials. In addition, the manufacturing process is complicated, resulting in high prices, which are not easy for customers to accept, and the market share is very low.

Method used

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  • Light heat insulating castable for lower part of CFB circulating fluidized bed separator and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Example 1: Lightweight thermal insulation castable for the lower part of CFB circulating fluidized bed separator, including the following raw materials in parts by weight: 20 parts of lightweight skeleton material, 5 parts of wear-resistant thermal insulation material, 5 parts of bonding rubber, and composite admixture 3 parts, 10 parts of deionized water;

[0036]The lightweight skeleton materials include: 4 parts of vitrified microbeads, 3 parts of silicon carbide micropowder, 3 parts of nano-silicon dioxide, 2 parts of titanium dioxide, 3 parts of light calcium carbonate, 2 parts of closed-cell perlite, 2 parts of floating beads, heavy 1 part spar;

[0037] Wear-resistant insulation materials include: 2 parts of nano-ceramic powder, 1 part of alumina micropowder, 1 part of yttrium oxide, and 1 part of aerated aluminum powder;

[0038] The bonding compound includes: 2 parts of aluminate cement, 1 part of silicone resin, 1 part of nano-cerium oxide, and 1 part of mine...

Embodiment 2

[0040] Embodiment 2: What this embodiment records is the preparation method of the lightweight thermal insulation castable of embodiment 1, comprising the following steps:

[0041] S1. Preparation of lightweight skeleton materials;

[0042] S1-1. Weigh the raw materials of lightweight skeleton materials in proportion, mix them at a speed of 300rad / min for 15min, and then coarsely crush them until the particle size is 0.5-0.7mm; finally, put the coarsely crushed materials at 900°C Calcining for 1 hour, after the material is cooled, crush it again into a powder with a particle size of 0.06-0.09mm;

[0043] S1-2. Add 45wt% deionized water to the powder obtained in step S1-1, stir and mix evenly, and then place it in a vacuum extruder with a pressure of 2MPa, a vacuum degree of -0.09a and an extrusion temperature of 20°C Extruded in a medium to obtain a lightweight skeleton material precursor with a diameter of 0.3mm and a length of 0.4mm;

[0044] S1-3. Dry the lightweight skel...

Embodiment 3

[0052] Embodiment 3: What this embodiment records is the construction method of the castable finished product prepared by the method of Example 2, comprising the following steps: 1) supporting the mold according to the lower structure of the CFB circulating fluidized bed separator; 2) placing the castable The finished product is mixed with water to form a slurry, and the slurry is placed in a vacuum box with a vacuum degree of 5Mpa for vacuum degassing treatment for 35 minutes; through the vacuum degassing treatment of the slurry, the concentrated suspension inside the slurry forms a gel and is in situ Solidify and form to improve the wear resistance of the castable; wherein the amount of water added is 5% of the volume of the finished castable; 3) inject the slurry obtained in step 2) into the mold, and remove the mold after natural curing for 12 hours to obtain the embryo body, and then the embryo body Placed in a medium frequency induction sintering furnace, fired for 3 hour...

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Abstract

The invention discloses a light heat insulating castable for the lower part of a CFB circulating fluidized bed separator and a preparation method thereof. The castable comprises a light framework material, a wear-resistant heat-insulating material, a bonding sizing material, a composite additive and deionized water; the preparation method of the castable comprises the following steps: S1, carrying out coarse crushing, calcination and fine powder treatment on the light framework material to obtain powder; then adding part of deionized water into the powder, and extruding to obtain a light framework material precursor; and finally, drying and baking the light framework material precursor to obtain the light framework material. S2, calcining and crushing the wear-resistant heat insulating material to obtain a heat-treated material; s3, uniformly mixing the heat-treated material with a bonding sizing material, a composite additive and the rest of deionized water to obtain a premix; s4, stirring and fusing the premix and the light framework material obtained in the S1, and obtaining a casting material; the castable prepared by the method has the advantages of light weight, low thermal conductivity and strong wear resistance, and is suitable for large-scale popularization.

Description

technical field [0001] The invention relates to the technical field of lightweight thermal insulation castables, in particular to a lightweight thermal insulation castable for the lower part of a CFB circulating fluidized bed separator and a preparation method thereof. Background technique [0002] Circulating fluidized bed combustion technology is a new type of coal-fired technology. The materials in the boiler have the characteristics of high heat capacity, strong mixing, and low-temperature combustion. This combustion technology has strong adaptability to fuels. It can not only burn lignite, bituminous coal, Anthracite, coal gangue, gas-making slag, petroleum coke and other low-quality fuels, and multiple types of coal can be burned on the same boiler at the same time; it can also achieve clean combustion of coal, and achieve high-sulfur coal by adding limestone powder or calcium carbide slag The flue gas desulfurization in the furnace is beneficial to the comprehensive u...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/66F23C10/08
CPCC04B35/66F23C10/08C04B2235/3217C04B2235/3225C04B2235/3208C04B2235/3232C04B2235/3418C04B2235/36C04B2235/3826C04B2235/3463C04B2235/3215C04B2235/3229C04B2235/402C04B2235/5216C04B2235/5436C04B2235/77C04B2235/96C04B2235/9607F23C2206/10
Inventor 张卫星张晟王晓杰许英李业清吴俊杰裴一新方贤斌
Owner 宜兴市兴贝耐火保温工程有限公司
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