Method for preparing papermaking dry strengthening agent
A technology of dry strength agent and conditioner, applied in papermaking, textile and papermaking, fiber raw material processing, etc., can solve the problems of increased equipment and personnel investment, high water retention value, unfavorable energy saving and emission reduction, etc., to improve retention and drainage. The effect of improving the burst resistance index and the sufficient source of raw materials
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Embodiment 1
[0025] The mixture of oxidized starch sodium chlorate and polyanionic cellulose with a total weight of 0.5% is dissolved in pure water and then added to the reaction flask for stirring, adding 8.2 grams of acrylamide, 1.2 acrylic acid, 2.6 carboxylate and 3 grams of acrylonitrile. Copolymerize the mixed monomers, raise the temperature to 30°C, and react at this temperature for 1 hour; add sodium hydroxide solution with a weight concentration of 30%, adjust the pH value to 5.5, and one-step graft copolymerization occurs under this condition Reaction, add sodium sulfate, polyalkylphenol, ethylene glycol, hydrogen peroxide in the process of graft copolymerization reaction, enter into aging reaction process after graft copolymerization reaction, add sodium sulfite in aging reaction process, heat After reaching 65°C, it can be measured and packaged after aging for a period of time.
[0026] The measured paper enhancement effect is shown in the table below
[0027]
Embodiment 2
[0029] Dissolve the mixture of cationic starch and phospholipid starch amphoteric starch and polyanionic cellulose with pure water of 1.5% of the total weight and add to the reaction flask to stir, add 6.1 grams of acrylamide, 1.5 acrylates, 3.2 carboxylic esters and 3.5 gram of acrylonitrile composed of copolymerized mixed monomers, the temperature was raised to 45°C, and reacted at this temperature for 2 hours; adding a mixed solution of potassium hydroxide and rubidium hydroxide with a weight concentration of 30%, adjusted the pH value to 6.5, Under this condition, a one-step graft copolymerization reaction occurs, and sodium chloride, quinone phenols and polyalkylphenols, alcohols and isopropanol, potassium persulfate and ammonium persulfate are added during the graft copolymerization reaction. After the technical copolymerization reaction is completed, it enters the aging reaction process. During the aging reaction process, ethylene glycol amine and triethanolamine are add...
Embodiment 3
[0033] Dissolve the mixture of dextrin and polyanionic cellulose with a total weight of 2.5% in pure water, add it to the reaction flask and stir, add 6.5 grams of acrylamide, 1.8 grams of acrylic acid, 3.5 grams of carboxylate and 2 grams of acrylonitrile. For the monomer, raise the temperature to 60°C, and react at this temperature for 3 hours; add a mixed solution of hydrochloric acid and sulfuric acid with a weight concentration of 30%, adjust the pH value to 7, and under this condition, a one-step graft copolymerization reaction occurs, Add vinylamines and ammonia water, quinone phenols, alkyl mercaptans, benzoyl peroxide and water-soluble azos during the graft copolymerization reaction, and enter the aging reaction process after the graft copolymerization reaction is completed. Sodium bisulfite is added during the aging reaction process, heated to 78°C, and can be measured and packaged after aging for a period of time.
[0034] The measured paper enhancement effect is sh...
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