Aqueous dissociating abrasive cutting fluid used for cutting solar silicon wafer and its preparation method

A technology of solar silicon wafers and free abrasives, applied in lubricating compositions and other directions, can solve the problems of environmental pollution, cost reduction, easy generation of hydrogen, etc., and achieve the effects of improving sand-carrying capacity, reducing production costs, and speeding up cutting speed.

Inactive Publication Date: 2014-07-30
西安通鑫半导体辅料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is currently the most widely used silicon wafer cutting method, but there are still problems such as poor dispersion and suspension of the cutting fluid, high cost of the cutting fluid, poor cooling and lubricity of the cutting fluid, and serious environmental pollution.
The existing water-based cutting fluids used for free abrasive wire cutting of silicon wafers or the water content is still too low to achieve the purpose of effectively reducing costs, or the suspension dispersibility and lubricity are not enough, and few people mention water-based cutting fluids The problem of easy generation of hydrogen gas in the process of wire cutting
[0004] For example, the application number is 201210397124.9, the Chinese patent titled "Water-based cutting fluid for hard and brittle materials and its preparation method" and the application number is 201110176262.X, the invention title is "A water-based cutting fluid for silicon wafer cutting" The water content of the water-based cutting fluid mentioned in the Chinese patents is 40 parts or less, although the production cost is saved to a certain extent, but the range is not large, and the COD value of the cutting fluid is still high due to the low water content, and the It cannot be truly green and environmentally friendly; moreover, in the process of separating the waste mortar after cutting, the organic matter on the surface of SiC is not easy to s

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0041] Example 1

[0042] 1) Add 0.1 part of Tween 80, 0.1 part of coconut oil fatty acid diethanolamide, 1.0 part of fatty alcohol polyoxyethylene ether and 0.2 part of polyethylene glycol 600 monooleate into 91 parts of water, mix , then sequentially add 0.05 parts of dispersant Tamol and 0.01 parts of SRE defoamer to the system, and mix thoroughly to obtain a mixed solution;

[0043] 2) Heat the mixed solution and stir until the solute is completely dissolved to obtain a mixed solution;

[0044] 3) Add 1 part of polyethylene glycol 400 monostearate to the mixed solution obtained in step 2), keep warm while adding the synthetic polymer thickener and keep stirring until the synthetic polymer thickener is completely dissolved to obtain Aqueous free abrasive cutting fluid for cutting solar silicon wafers.

[0045] Its performance indicators are shown in Table 1 below.

Example Embodiment

[0046] Example 2

[0047] 1) Add 0.2 parts of alkylphenol polyoxyethylene ether, 0.3 parts of coconut oil fatty acid diethanolamide, 0.9 parts of fatty alcohol polyoxyethylene ether and 1.5 parts of polyethylene glycol 600 monooleate to 93 parts of In water, after mixing, add 0.1 part of sodium methylene bismethylnaphthalene sulfonate and 0.02 part of one or more of simethicone, simethicone, DE889 defoamer to the system The mixture is fully mixed to obtain a mixed solution; wherein, the alkylphenol polyoxyethylene ether is prepared by adding nonylphenol to 8 molecules of ethylene oxide;

[0048] 2) Heat the mixed solution and stir until the solute is completely dissolved to obtain a mixed solution;

[0049] 3) Add 1.5 parts of polyethylene glycol 400 distearate into the mixed solution obtained in step 2), keep warm while adding the synthetic polymer thickener and keep stirring until the synthetic polymer thickener is completely dissolved to obtain Aqueous free abrasive cutti...

Example Embodiment

[0050] Example 3

[0051] 1) Add 0.3 parts of Tween 80 or alkylphenol ethoxylates, 0.5 parts of AES, 0.8 parts of fatty alcohol ethoxylates and 1.2 parts of polyethylene glycol 600 monooleate into 95 parts of water After mixing, add 0.15 parts of dispersant Tamol and 0.03 parts of a mixture of SRE defoamer and DE889 defoamer to the system in turn, and mix well to obtain a mixed solution;

[0052] 2) Heat the mixed solution and stir until the solute is completely dissolved to obtain a mixed solution;

[0053] 3) Add 2 parts of polyethylene glycol 6000 distearate into the mixed solution obtained in step 2), keep warm while adding the synthetic polymer thickener and keep stirring until the synthetic polymer thickener is completely dissolved to obtain Aqueous free abrasive cutting fluid for cutting solar silicon wafers. Its performance indicators are shown in Table 1 below.

[0054] Table 1

[0055] Numbering

[0056] Wherein, the viscosity is measured under a visco...

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PUM

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Abstract

The invention discloses an aqueous dissociating abrasive cutting fluid used for cutting a solar silicon wafer and its preparation method. The aqueous dissociating abrasive cutting fluid comprises a synthetic polymer thickening agent, a non-ionic surface active agent, a dispersing agent, a defoaming agent and water. The aqueous dissociating abrasive cutting fluid has a moisture content reaching to more than 90 parts, the cutting fluid production cost is greatly reduced, but the performance is greatly improved, the cutting fluid has better dispersion suspension performance on SiC, the cutting fluid has better cooling and lubrication properties; aiming at the problem that a water base cutting fluid is easy to produce hydrogen in an on-line cutting process, the aqueous dissociating abrasive cutting fluid has targeted measures, greatly reduces the hydrogen production amount, makes the production more secure; and at the same time, and because of the low water content and high organic matter content, the aqueous dissociating abrasive cutting fluid is very low in COD (chemical oxygen demand) value, and is a green, environmental-friendly and new water base cutting fluid.

Description

technical field [0001] The invention belongs to the technical field of silicon wafer cutting, and relates to a cutting fluid, in particular to a water-based free abrasive cutting fluid for cutting solar silicon wafers and a preparation method thereof. Background technique [0002] With the continuous development of the solar photovoltaic industry, higher requirements are put forward for photovoltaic conversion efficiency and cost, which requires that every link of the photovoltaic industry must continuously improve the technical level. As silicon wafers are the core components of photovoltaic cells, the improvement of the quality of silicon wafers, the reduction of production costs and the greening of production will provide a stronger impetus for the development of the photovoltaic industry. [0003] Silicon wafer free abrasive wire cutting is to mix the cutting fluid with SiC and spray it between the steel wire and the silicon rod workpiece, so that the silicon rod produce...

Claims

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Application Information

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IPC IPC(8): C10M173/02
Inventor 徐静房忠芳郭小娟李新家
Owner 西安通鑫半导体辅料有限公司
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